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    Preparation of fluoromethylthiobenzoyl fluorides
    3.
    发明授权
    Preparation of fluoromethylthiobenzoyl fluorides 失效
    氟甲硫基苯甲酰氟的制备

    公开(公告)号：US4590016A

    公开(公告)日：1986-05-20

    申请号：US589305

    申请日：1984-03-14

    申请人： Juergen Varwig ,  Gerhard Hamprecht

    发明人： Juergen Varwig ,  Gerhard Hamprecht

    IPC分类号： C07C319/20 ,  C07C51/58 ,  C07C67/00 ,  C07C313/00 ,  C07C323/62

    CPC分类号： C07C323/00

    摘要： Novel fluoromethylthiobenzoyl fluorides are prepared by reacting a trichloromethylthiobenzoyl chloride with hydrogen fluoride at from 10.degree. to 130.degree. C., and are useful starting materials for the preparation of crop protection agents. The process of the invention is selective in permitting the optional production of either a trifluoromethylthiobenzoyl fluoride or a difluoromonochloromethylthiobenzoyl fluoride, depending upon the temperature employed.

    摘要翻译： 新的氟甲硫基苯甲酰氟通过三氯甲硫基苯甲酰氯与氟化氢在10°至130℃下反应制备，并且是用于制备作物保护剂的有用起始材料。 根据所用的温度，本发明的方法是选择性地允许任选地生产三氟甲硫基苯甲酰氟或二氟单氯氯甲硫基苯甲酰氟。

    Preparation of substituted 2-phenyl-4H-3,1-benzoxazin-4-ones
    4.
    发明授权
    Preparation of substituted 2-phenyl-4H-3,1-benzoxazin-4-ones 失效
    取代的2-苯基-4H-3,1-苯并恶嗪-4-酮的制备

    公开(公告)号：US4673740A

    公开(公告)日：1987-06-16

    申请号：US842995

    申请日：1986-03-24

    申请人： Gerhard Hamprecht ,  Wolfgang Rohr ,  Juergen Varwig

    发明人： Gerhard Hamprecht ,  Wolfgang Rohr ,  Juergen Varwig

    IPC分类号： C07D265/22 ,  C07D265/36

    CPC分类号： C07D265/22

    摘要： 2-Phenyl-4H-3,1-benzoxazin-4-ones of the general formula I ##STR1## where R.sup.1 and R.sup.2 are each hydrogen or halogen, R.sup.1 may furthermore be methyl or methoxy and R.sup.2 may furthermore be haloalkyl, haloalkoxy, haloalkylmercapto or haloalkylsulfonyl, each of 1 to 3 carbon atoms, are prepared by reacting an appropriate anthranilic acid with an appropriate benzoyl halide in the presence of a base (acylation) and effecting ring closure by removal of water (cyclization), the process being carried out in a suspending agent which is immiscible with aqueous alkali metal hydroxide solution and in the presence of a phase-transfer catalyst.

    摘要翻译： 其中R 1和R 2各自为氢或卤素的通式I（I）的2-苯基-4H-3,1-苯并恶嗪-4-酮，R 1还可以是甲基或甲氧基，R 2还可以是卤代烷基， 通过在碱（酰化）存在下使合适的苯甲酰卤与适当的苯甲酰卤反应并通过除去水（环化）进行闭环来制备具有1至3个碳原子的卤代烷氧基，卤代烷基巯基或卤代烷基磺酰基， 在与碱金属氢氧化物水溶液不混溶并在相转移催化剂存在下的悬浮剂中进行。

    Preparation of fluorophthalic anhydrides
    6.
    发明授权
    Preparation of fluorophthalic anhydrides 失效
    氟代邻苯二甲酸酐的制备

    公开(公告)号：US4514572A

    公开(公告)日：1985-04-30

    申请号：US572949

    申请日：1984-01-23

    申请人： Gerhard Hamprecht ,  Juergen Varwig ,  Wolfgang Rohr

    发明人： Gerhard Hamprecht ,  Juergen Varwig ,  Wolfgang Rohr

    IPC分类号： C07C51/567 ,  C07D307/89

    CPC分类号： C07C51/567 ,  C07D307/89

    摘要： Fluorophthalic anhydrides containing 1 or 2 fluorine atoms are prepared by a process in which a chlorophthalic anhydride containing 1 or 2 chlorine atoms is treated with an acid chloride of sulfurous acid or of carbonic acid in the presence of an aliphatic sulfone, and the reaction mixture is then reacted with potassium fluoride.

    摘要翻译： 含有1或2个氟原子的氟代邻苯二甲酸酐通过在脂族砜存在下用亚硫酸或碳酸的酰氯处理含有1或2个氯原子的氯代邻苯二甲酸酐的方法制备，反应混合物为 然后与氟化钾反应。

    Preparation of fluorophthalimides
    7.
    发明授权
    Preparation of fluorophthalimides 失效
    氟代邻苯二甲酰亚胺的制备

    公开(公告)号：US4680412A

    公开(公告)日：1987-07-14

    申请号：US615806

    申请日：1984-05-31

    申请人： Gerhard Hamprecht ,  Juergen Varwig ,  Wolfgang Rohr

    发明人： Gerhard Hamprecht ,  Juergen Varwig ,  Wolfgang Rohr

    IPC分类号： C07D209/48

    CPC分类号： C07D209/48

    摘要： Fluorophthalimides are prepared by a process in which a fluorophthalic anhydride is reacted, in the presence of an aliphatic sulfone, with from 0.4 to 0.8 mole of urea per mole of fluorophthalic anhydride, and the reaction is carried out first at 110.degree.-140.degree. C. and then at 150.degree.-170.degree. C.

    摘要翻译： 氟代邻苯二酰亚胺通过在脂肪族砜存在下使氟代邻苯二甲酸酐与每摩尔氟代邻苯二甲酸酐为0.4至0.8摩尔的尿素反应的方法制备，首先在110-140℃下进行反应 然后在150℃-170℃

    Pyridine derivatives and their use for controlling undesirable plant growth
    8.
    发明授权
    Pyridine derivatives and their use for controlling undesirable plant growth 失效
    吡啶衍生物及其用于控制​​不希望的植物生长的用途

    公开(公告)号：US5262384A

    公开(公告)日：1993-11-16

    申请号：US825793

    申请日：1992-01-21

    申请人： Gerhard Hamprecht ,  Norbert Goetz ,  Bruno Wuerzer ,  Karl-Otto Westphalen

    发明人： Gerhard Hamprecht ,  Norbert Goetz ,  Bruno Wuerzer ,  Karl-Otto Westphalen

    IPC分类号： A01N43/40 ,  A01N43/90 ,  C07D213/81 ,  C07D213/82 ,  C07D471/04 ,  C07D47/04

    CPC分类号： C07D213/81 ,  A01N43/40 ,  A01N43/90 ,  C07D213/82 ,  C07D471/04

    摘要： Pyridine derivatives of the formulae ##STR1## where W, X, Y and Z are each C--R.sup.4, N or N.fwdarw.O, with the proviso that the ring contains only one heteroatom, and the substituents R.sup.1, R.sup.2 and R.sup.3 have the following meanings:R.sup.1 is alkoxy, substituted or unsubstituted alkyl, substituted or unsubstituted cycloalkyl, substituted or unsubstituted alkenyl, or substituted or unsubstituted alkynyl,R.sup.2 is hydrogen,R.sup.3 is formyl, 4,5-dihydrooxazol-2-yl or --CO--A--R.sup.5 or --CO--NR.sup.6 R.sup.7,whereR.sup.4 is halogen, nitro, cyano, substituted or unsubstituted alkyl, substituted or unsubstituted benzyl, substituted or unsubstituted cycloalkyl, substituted or unsubstituted alkenyl, substituted or unsubstituted alkynyl, alkoxy, alkylthio, haloalkoxy, haloalkylthio, alkenyloxy, alkynyloxy, alkylsulfinyl, alkylsulfonyl, haloalkylsulfonyl, substituted or unsubstituted phenoxy or phenylthio, a substituted or unsubstituted 5- or 6-membered heterocyclic radical having one or two heteroatoms selected from the group consisting of oxygen, sulfur and nitrogen, or is substituted or unsubstituted phenylA is oxygen or sulfur,R.sup.5 is hydrogen, substituted or unsubstituted alkyl, substituted or unsubstituted benzyl, cycloalkyl, substituted or unsubstituted phenyl,one equivalent of a cation or the radical --N.dbd.CR.sup.8 R.sup.9 andR.sup.6 and R.sup.7 are hydrogen or alkyl or together denote a methylene chain having 4 or 5 members,their agriculturally utilizable salts, and their use for controlling unwanted plant growth.

    摘要翻译： 其中W，X，Y和Z各自为C-R 4，N或N-> O，条件是环仅含有一个杂原子，并且 取代基R 1，R 2和R 3具有以下含义：R 1是烷氧基，取代或未取代的烷基，取代或未取代的环烷基，取代或未取代的链烯基或取代或未取代的炔基，R 2是氢，R 3是甲酰基，4,5-二氢恶唑 -2-基或-CO-A-R5或-CO-NR6R7，其中R4是卤素，硝基，氰基，取代或未取代的烷基，取代或未取代的苄基，取代或未取代的环烷基，取代或未取代的烯基，取代或未取代的炔基 烷氧基，烷硫基，卤代烷氧基，卤代烷硫基，烯氧基，炔氧基，烷基亚磺酰基，烷基磺酰基，卤代烷基磺酰基，取代或未取代的苯氧基或苯硫基，取代或未取代的具有一个或两个选自t 由氧，硫和氮组成的组，或者是取代或未取代的苯基A是氧或硫，R5是氢，取代或未取代的烷基，取代或未取代的苄基，环烷基，取代或未取代的苯基，1当量的阳离子或 基团-N = CR 8 R 9和R 6和R 7是氢或烷基或一起表示具有4或5个成员的亚甲基链，它们的农业上可利用的盐，以及它们用于控制不想要的植物生长的用途。

    Agents for defoliating cotton
    9.
    发明授权
    Agents for defoliating cotton 失效
    棉花脱叶剂

    公开(公告)号：US5171352A

    公开(公告)日：1992-12-15

    申请号：US561611

    申请日：1990-08-02

    申请人： Klaus Grossmann ,  Wilhelm Rademacher ,  Gerhard Hamprecht ,  Karl-Otto Westphalen ,  Bruno Wuerzer

    发明人： Klaus Grossmann ,  Wilhelm Rademacher ,  Gerhard Hamprecht ,  Karl-Otto Westphalen ,  Bruno Wuerzer

    IPC分类号： A01N47/36

    CPC分类号： A01N47/36

    摘要： Cotton plants are defoliated by the action of an amount, having a defoliant effect, of a phenylsulfonylurea Ia or Ib ##STR1## where R.sup.1 is C.sub.1 -C.sub.4 -alkyl or C.sub.3 -C.sub.5 -alkoxyalkyl, and these radicals may each carry from 1 to 3 halogen atoms, or C.sub.3 - or C.sub.4 -alkenyl or C.sub.3 - or C.sub.4 -alkynyl, R.sup.2 is F, Cl or Br, R.sup.2' is H, F, Cl or Br, R.sup.3 is H, CH.sub.3 or C.sub.2 H.sub.5, R.sup.4 is halogen, CH.sub.3 or OCH.sub.3, R.sup.5 is CH.sub.3 or OCH.sub.3, R.sup.6 is halogen, C.sub.1 - or C.sub.2 -alkyl, C.sub.1 - or C.sub.2 -alkoxy, C.sub.1 - or C.sub.2 -alkylthio or C.sub.1 - or C.sub.2 -alkylamino and Z is CH or N, or of an alkali metal or alkaline earth metal salt of a compound Ia or Ib.

    摘要翻译： 通过具有脱叶效应的量的苯基磺酰脲Ia或其中R 1是C 1 -C 4 - 烷基或C 3 -C 5 - 烷氧基烷基的苯基磺酰脲Ia或Ib，其中这些基团可各自脱落， 携带1至3个卤素原子，或C3-或C4-烯基或C3-或C4-炔基，R2是F，Cl或Br，R2'是H，F，Cl或Br，R3是H，CH3或C2H5， R4是卤素，CH3或OCH3，R5是CH3或OCH3，R6是卤素，C1-或C2-烷基，C1-或C2-烷氧基，C1-或C2-烷硫基或C1-或C2-烷基氨基，Z是CH或 N，或化合物Ia或Ib的碱金属或碱土金属盐。

    Herbicidal sulfonamides and their use to influence plant growth
    10.
    发明授权
    Herbicidal sulfonamides and their use to influence plant growth 失效
    除草剂磺酰胺及其用于影响植物生长的因素

    公开(公告)号：US5104441A

    公开(公告)日：1992-04-14

    申请号：US618587

    申请日：1990-11-28

    申请人： Gerhard Hamprecht ,  Helmut Hagen ,  Thomas Liese-Sauer ,  Norbert Meyer ,  Bruno Wuerzer

    发明人： Gerhard Hamprecht ,  Helmut Hagen ,  Thomas Liese-Sauer ,  Norbert Meyer ,  Bruno Wuerzer

    IPC分类号： A01N47/36 ,  C07D521/00

    CPC分类号： C07D521/00 ,  A01N47/36

    摘要： Substituted sulfonylureas of the formula I ##STR1## where R.sup.1 is hydrogen, C.sub.1 -C.sub.4 -alkyl, C.sub.3 -C.sub.4 -alkenyl or alkynyl, C.sub.1 -C.sub.4 -haloalkyl, C.sub.3 -C.sub.6 -alkoxyalkyl, C.sub.4 -C.sub.6 -haloalkoxyalkyl or C.sub.5 -C.sub.6 -cycloalkyl,R.sup.2 is hydrogen, methyl or ethyl,R.sup.3 is hydrogen, halogen, methyl or methoxy,R.sup.4 is hydrogen, methyl or methoxy,X is N or C--H,and Hal is fluorine, chlorine or bromine, and alkali metal or alkaline earth metal salts thereof, with the proviso that R.sup.1 is not methyl when Hal is chlorine and X is N, a process for the manufacture of sulfonylureas of the formula I and their use as herbicides.

    摘要翻译： 取代的式I的磺酰脲其中R 1是氢，C 1 -C 4 - 烷基，C 3 -C 4 - 烯基或炔基，C 1 -C 4卤代烷基，C 3 -C 6 - 烷氧基烷基，C 4 -C 6 - 卤代烷氧基烷基或C 5 -C 6 环烷基，R 2是氢，甲基或乙基，R 3是氢，卤素，甲基或甲氧基，R 4是氢，甲基或甲氧基，X是N或CH，Hal是氟，氯或溴，以及碱金属或碱土 金属盐，条件是当Hal为氯且X为N时，R1不是甲基，制备式I磺酰脲的方法及其作为除草剂的用途。