公开(公告)号：US20160252485A1

公开(公告)日：2016-09-01

申请号：US15028242

申请日：2014-10-08

Applicant: HTE GMBH THE HIGH THROUGHPUT EXPERIMENTATION COMPANY

Inventor： Armin LANGE DE OLIVEIRA ,  Nadine BREM ,  Mario SOORHOLTZ ,  Johannes LIEBERKNECHT

IPC: G01N31/10 ,  B01J19/00

CPC classification number: G01N31/10 ,  B01J19/0046 ,  B01J2219/00281 ,  B01J2219/00286 ,  B01J2219/00477 ,  B01J2219/00479 ,  B01J2219/00704 ,  B01J2219/00707 ,  B01J2219/00747 ,  C40B30/08 ,  C40B60/12

Abstract: The invention relates to an apparatus and a method for investigating solid catalysts and processes in which discontinuous fluid streams arise. The apparatus according to the invention which is preferably configured for parallel investigation of a plurality of catalysts comprises at least one reaction space, wherein every reaction space has one or more fluid mixing spaces connected downstream of it. The outlet line of the fluid mixing space or else the outlet line of a sequence of fluid mixing spaces is operatively connected to a throttle element (11), wherein the throttle element (11) is operatively connected to an analyzer and an outlet line and the outlet line comprises a control means. The method according to the invention is operated in a cyclic mode in which at least one product fluid is supplied into the at least one fluid mixing space in a controlled manner, the product fluid stream is commixed in the mixing space and the at least one commixed product fluid stream is supplied to the outlet line and the analyzer. One cycle has a duration in the range from 0.2 to 7200 seconds and can comprise two or more phases of different compositions. The method can comprise a plurality of cycles.

Abstract translation: 本发明涉及一种用于研究固体催化剂的装置和方法，其中产生不连续流体流。 根据本发明的装置优选地被配置用于多个催化剂的并行研究包括至少一个反应空间，其中每个反应空间具有连接在其下游的一个或多个流体混合空间。 流体混合空间的出口管线或一系列流体混合空间的出口管线可操作地连接到节流元件（11），其中节流元件（11）可操作地连接到分析器和出口管线，并且 出口管线包括控制装置。 根据本发明的方法以循环模式操作，其中以受控的方式将至少一种产品流体供应到至少一个流体混合空间中，产物流体流在混合空间中并入，并且至少一个混合 产品流体流被输送到出口管线和分析器。 一个周期的持续时间在0.2至7200秒的范围内，并且可以包括两个或更多个不同组成的相。 该方法可以包括多个周期。