摘要:
TO LOWER THE CONTENT OF CHLORINE-CONTAINING BY-PRODUCTS IN THE CRUDE CIS,TRANS,TRANS-CYCLODODECATRIENE-1,5,9 OBTAINED FROM THE TRIMERIZATION OF 1,3-BUTADIENE IN THE PRESENCE OF TITANIUM HALOGENIDES AND ALKYL ALUMINUM HALIDES IN AN INERT SOLVENT, AFTER THE TRIMERIZATION IS COMPLETED, THERE IS ADDED AMMONIA WHICH SUPRESSES THE FORMATION OF CHLORINE-CONTAINING COMPOUNDS, AND THEREAFTER WATER WHICH RESULTS IN THE CATALYST RESIDUE PRECIPITATING IN LARGE GRANULES, FACILITATING A DECANTING OR FILTRATION STEP.