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    Fiber-reactive dyes containing an aniline radical which carries two different vinylsulfonyl moieties
    1.
    发明授权
    Fiber-reactive dyes containing an aniline radical which carries two different vinylsulfonyl moieties 失效
    含有带有两个不同乙烯基磺酰基部分的苯胺基团的纤维反应性染料

    公开(公告)号：US4929719A

    公开(公告)日：1990-05-29

    申请号：US394302

    申请日：1989-08-10

    申请人： Hansrudolf Schwander ,  Athanassios Tzikas ,  Peter Aeschlimann

    发明人： Hansrudolf Schwander ,  Athanassios Tzikas ,  Peter Aeschlimann

    IPC分类号： C09B62/513 ,  C09B62/44 ,  C09B62/503 ,  C09B62/51

    CPC分类号： C09B62/503 ,  C09B62/4401

    摘要： Reactive dyes which are particularly suitable for dyeing and printing cellulose containing fiber materials by the cold padbatch process and which produce, in high dye yield, dyeings and prints having good fastness properties containing the radical of an amine of the formula ##STR1## in which R is hydrogen, halogen, hydroxyl or sulfo, Z is a radical of the formula --CH.dbd.CH.sub.2 or --CH.sub.2 --CH.sub.2 --Y, Y is a detachable group, R' is hydrogen or C.sub.1 -C.sub.4 alkyl which is unsubstituted or substituted by --COOH, --CN, --OH or --SO.sub.3 H, and E is a radical of the formula ##STR2## in which R' and Z are as defined above, alk, alk' and alk" independently of one another are a C.sub.1 -C.sub.6 alkylene radical, U is hydrogen, halogen, hydroxyl, sulfato, C.sub.1 -C.sub.4 alkanoyloxy, cyano, carboxyl, C.sub.1 -C.sub.4 -alkoxycarbonyl, carbamoyl or a radical --SO.sub.2 --Z in which Z is as defined above, V is hydrogen, substituted or unsubstituted C.sub.1 -C.sub.4 alkyl or a radical of the formula ##STR3## in which Z, alk and U are as defined above, and q, r and s independently of one another are an integer from 1 to 6.

    摘要翻译： 特别适用于通过冷拼接方法对含纤维素纤维材料进行染色和印花的活性染料，其以高染料产率，染色和印刷品具有良好的牢固性能，其含有式（1）的胺基团， 其中R是氢，卤素，羟基或磺基，Z是式-CH = CH 2或-CH 2 -CH 2 -Y的基团，Y是可分离的基团，R'是氢或被未取代或取代的C 1 -C 4烷基 通过-COOH，-CN，-OH或-SO 3 H，并且E是下式的基团：其中R'是（R 1） 和Z如上所定义，烷基，烷基和烷基彼此独立地是C 1 -C 6亚烷基，U是氢，卤素，羟基，硫酸根，C 1 -C 4烷酰氧基，氰基，羧基，C 1 -C 4烷氧基羰基， 氨基甲酰基或其中Z如上定义的基团-SO 2-Z，V是氢，取代或未取代的C 1 -C 4烷基或其中Z，alk和U为 并且q，r和s彼此独立地是1至6的整数。

    Fiber-reactive dioxazine dyes containing two vinylsulfonyl moieties
    3.
    发明授权
    Fiber-reactive dioxazine dyes containing two vinylsulfonyl moieties 失效

    公开(公告)号：US4997937A

    公开(公告)日：1991-03-05

    申请号：US422339

    申请日：1989-10-16

    申请人： Athanassios Tzikas ,  Peter Aeschlimann

    发明人： Athanassios Tzikas ,  Peter Aeschlimann

    IPC分类号： C07D295/18 ,  C07C317/04 ,  C07C317/18 ,  C07C317/28 ,  C07C323/25 ,  C07D498/04 ,  C09B62/503 ,  D06P1/38

    CPC分类号： C09B62/5033 ,  C07C317/04

    摘要： Dyes suitable for dyeing and printing cellulose-containing fiber materials which produce blue dyeings and prints having good fastness properties. These dyes are of the formula ##STR1## wherein R.sub.1 and R.sub.2 are each independently of the other hydrogen, halogen, C.sub.1 -C.sub.4 alkyl, C.sub.1 -C.sub.4 alkoxy, phenoxy, carboxyl carbamoyl or C.sub.1 -C.sub.4 alkanoylamino; R.sub.3 is hydrogen, sulfo, C.sub.1 -C.sub.4 alkyl, C.sub.1 -C.sub.4 alkoxy, halogen, carboxyl, carbamoyl, N-C.sub.1 -C.sub.4 alkylcarbamoyl, N,N-di-C.sub.1 -C.sub.4 alkylcarbamoyl, C.sub.1 -C.sub.4 alkylsulfonyl, sulfamoyl, N-C.sub.1 -C.sub.4 alkylsulfamoyl or N,N-di-C.sub.1 -C.sub.4 alkylsulfamoyl; R.sub.4 is a radical of the formula ##STR2## R.sub.5 and R.sub.6 are independently of each other hydrogen or unsubstituted or hydroxyl-, sulfo-, sulfato-, carboxyl-, cyano-, halogen-, C.sub.1 -C.sub.4 alkoxycarbonyl-, C.sub.1 -C.sub.4 alkanoyloxy- or carbamoyl-substituted and uninterrupted or, except in the case of methyl, --O--, --S-- or --NH--interrupted C.sub.1 -C.sub.6 alkyl; R' is hydrogen or C.sub.1 -C.sub.6 alkyl; t is an integer from 0 to 4; the phenyl radical (a) is unsubstituted or substituted by C.sub.1 -C.sub.4 alkyl, C.sub.1 -C.sub.4 alkyl substituted by hydroxyl-, sulfo or sulfato, C.sub.1 -C.sub.4 alkoxy, halogen, sulfo, carboxyl or hydroxy, and A is a radical of the formula ##STR3## where R' is as defined above, (alk) is C.sub.1 -C.sub.6 alkylene, T is hydrogen, halogen, hydroxyl, sulfato, carboxyl, cyano, C.sub.1 -C.sub.4 alkanoyloxy, C.sub.1 -C.sub.4 alkoxycarbonyl, carbamoyl or a radical --SO.sub.2 --Z, V is hydrogen, substituted or unsubstituted C.sub.1 -C.sub.4 alkyl or a radical of the formula -(alk)--CH.sub.2 --SO.sub.2 --Z, where (alk) is as defined above, Z is a radical of the formula --CH.dbd.CH.sub.2 l or --CH.sub.2 --CH.sub.2 --Y, Y is a leaving group selected from the group consisting of --OSO.sub.3 H, --SSO.sub.3 H, --OCOCH.sub.3, --OCO--C.sub.6 H.sub.5, OPO.sub.3 H.sub.2, --Cl, Br, --F, ##STR4## p, q and r are each independently of the others an integer from 1 to 6.

    Reactive dyes, containing two triazinyl radicals which are bridged via an aliphatic or aromatic bridge member
    4.
    发明授权
    Reactive dyes, containing two triazinyl radicals which are bridged via an aliphatic or aromatic bridge member 失效
    含有两个通过脂族或芳族桥连桥桥连的三嗪基的活性染料

    公开(公告)号：US5717078A

    公开(公告)日：1998-02-10

    申请号：US704425

    申请日：1996-08-22

    申请人： Athanassios Tzikas ,  Peter Aeschlimann

    发明人： Athanassios Tzikas ,  Peter Aeschlimann

    IPC分类号： C07D251/50 ,  C09B62/44 ,  C09B62/503 ,  C09B62/513 ,  C09B62/515 ,  C09B62/09 ,  C09B62/08 ,  C09B62/507 ,  D06P1/38

    CPC分类号： C09B62/4403

    摘要： Reactive dyes of the formula ##STR1## in which R.sub.1, R.sub.2, R.sub.3 and R.sub.4 independently of one another are hydrogen or substituted or unsubstituted C.sub.1 -C.sub.4 alkyl, X.sub.1 and X.sub.2 are halogen, B.sub.1 is an aromatic or aliphatic bridge member, or the radical of the formula --N(R.sub.2)--B.sub.1 --N(R.sub.3)-- is a piperazine radical, A.sub.1 is the radical of a monoazo, polyazo, metal complex azo, anthraquinone, phthalocyanine, formazan or dioxazine chromophore and, A.sub.2 is a radical of the formula ##STR2## in which D.sub.1 is substituted or unsubstituted phenyl or naphthyl, R.sub.5 and R.sub.6 independently of one another are hydrogen or substituted or unsubstituted C.sub.1 -C.sub.4 alkyl, alk is substituted or unsubstituted C.sub.2 -C.sub.6 alkylene and Z is vinyl or a radical --CH.sub.2 --CH.sub.2 --U.sub.1, and U.sub.1 is a leaving group, and the radicals A.sub.1 and A.sub.2 differ from one another, are particularly suitable for dyeing or printing fibre materials containing hydroxyl groups or containing nitrogen. Dyeings with good fastness properties are obtained with a high tinctorial yield.

    摘要翻译： 其中R 1，R 2，R 3和R 4彼此独立地是氢或取代或未取代的C 1 -C 4烷基，X 1和X 2的式（I）的反应性染料是卤素，B1是芳族或脂族桥连构件，或 式-N（R2）-B1-N（R3） - 的基团是哌嗪基，A1是单偶氮，多偶氮，金属络合物偶氮，蒽醌，酞菁，甲an或二恶嗪发色团的基团，A2是 其中D1是取代或未取代的苯基或萘基，R 5和R 6彼此独立的式（II）的基团是氢或取代或未取代的C 1 -C 4烷基，烷基是取代或未取代的C 2 -C 6亚烷基，Z是乙烯基 或基团-CH 2 -CH 2 -U 1，并且U1是离去基团，基团A1和A2彼此不同，特别适用于染色或印刷含有羟基或含氮的纤维材料。 获得具有良好牢度性能的染色，具有高的着色收率。

    Fibre-reactive dyes containing a substituted aminocarbonyl-phenylamino or naphthylamino reactive moiety
    6.
    发明授权
    Fibre-reactive dyes containing a substituted aminocarbonyl-phenylamino or naphthylamino reactive moiety 失效
    含有取代氨基羰基 - 苯基氨基或萘基氨基反应性部分的纤维反应性染料

    公开(公告)号：US5023325A

    公开(公告)日：1991-06-11

    申请号：US191845

    申请日：1988-05-11

    申请人： Athanassios Tzikas ,  Peter Aeschlimann

    发明人： Athanassios Tzikas ,  Peter Aeschlimann

    IPC分类号： C09B62/503 ,  D06P1/384

    CPC分类号： D06P1/384 ,  C09B62/503

    摘要： A reactive dye of the formulaD--U--R).sub.nin which D is the radical of an anthraquinone, phthalocyanine, formazane, azomethine, dioxazine, phenazine, stilbene, triphenylmethane, xanthene, thioxanthone, nitroaryl, naphthoquinone, pyrenequinone or perylenetetracarbimide dye; U is --CO-- or --SO.sub.2 --; R is a radical of the formula ##STR1## Z is sulfatoethyl, .beta.-thiosulfatoethyl, .beta.-phosphatoethyl, .beta.-acetoxyethyl, .beta.-halogenoethyl or vinyl; alk is a polymethylene radical having 1 to 6 C atoms or its branched isomers; Y is hydrogen, chlorine, bromine, fluorine, hydroxyl, sulfato, C.sub.1 -C.sub.4 -alkanoyloxy, cyano, carboxyl, alkoxycarbonyl having 1 to 5 C atoms, carbamoyl or a radical --SO.sub.2 --Z in which Z is as defined above; V is hydrogen or C.sub.1 -C.sub.4 -alkyl which is unsubstituted or substituted by carboxyl, sulfo, C.sub.1 -C.sub.2 -alkoxy, halogen or hydroxyl;or a radical ##STR2## in which Z, alk and Y are as defined above; R.sub.1 is hydrogen or C.sub.1 -C.sub.6 -alkyl; alk', independently of each other, are polymethylene radicals having 2 to 6 C atoms or their branched isomers; n is 1 to 4, m is 1 to 6, p is 1 to 6 and q is 1 to 6; where, when U is --SO.sub.2 --, V must not be hydrogen or D must not be a phthalocyanine dye radical.

    摘要翻译： 式D-U-R）n的活性染料，其中D是蒽醌，酞菁，甲ane烷，偶氮甲碱，二恶嗪，吩嗪，芪，三苯基甲烷，呫吨，噻吨酮，硝基芳基，萘醌，芘醌或苝四甲酰亚胺染料的基团; U是-CO-或-SO 2 - ; R是式（III）的基团，其中Z是硫酸根合，β-硫代乙酰乙基，β-磷酰乙基，β-乙酰氧基乙基，β-卤代乙基或乙烯基; alk是具有1至6个C原子的多亚甲基或其支链异构体; Y是氢，氯，溴，氟，羟基，硫酸根，C 1 -C 4 - 烷酰氧基，氰基，羧基，具有1至5个C原子的烷氧基羰基，氨基甲酰基或-SO 2 -Z基，其中Z如上定义; V是氢或未被取代或被羧基，磺基，C 1 -C 2烷氧基，卤素或羟基取代的C 1 -C 4 - 烷基; 或其中Z，alk和Y如上所定义的基团 R1是氢或C1-C6-烷基; 烷基，彼此独立地是具有2至6个C原子的多亚甲基或其支链异构体; n为1〜4，m为1〜6，p为1〜6，q为1〜6; 其中当U是-SO 2 - 时，V不能是氢或D不能是酞菁染料基团。

    Fibre-reactive dyes containing a substituted sulfonylaminocarbonyl group
    7.
    发明授权
    Fibre-reactive dyes containing a substituted sulfonylaminocarbonyl group 失效
    含有取代的磺酰基氨基羰基的纤维反应性染料

    公开(公告)号：US4968782A

    公开(公告)日：1990-11-06

    申请号：US423710

    申请日：1989-10-13

    申请人： Athanassios Tzikas ,  Peter Aeschlimann

    发明人： Athanassios Tzikas ,  Peter Aeschlimann

    IPC分类号： C09B62/503

    CPC分类号： C09B62/503

    摘要： Reactive dyes of the formula ##STR1## in which D is the radial of an anthraquinone, phthalocyanine, formazan, azomethine, dioxazine, phenazine, triphenylmethane, xanthene, thioxanthone, nitroaryl, naphthoquinone, pyrenequinone or perylenetetracarbimide dye; Q is hydrogen or alkyl which has 1 to 4 carbon atoms and can be substituted by carboxyl, sulfo, cyano, hydroxyl, C.sub.1- C.sub.4 alkoxy or halogen; B is a radical --CH.sub.2n, --O--CH.sub.2n or --NH --CH.sub.2n and n is 1 to 6; R is a radical of the formula ##STR2## Z is .beta.-sulfatoethyl, .beta.-thiosulfatoethyl, .beta.-phosphatoethyl, .beta.-acyloxyethyl, .beta.-halogenoethyl or vinyl; alk is an alkylene radical having 1 to 6 C atoms or branched isomers thereof; Y is hydrogen, chlorine, bromine, flourine, hydroxyl, sulfato, acyloxy having 1 to 4 C atoms, cyano, carboxyl, alkoxycarbonyl having 1 to 5 C atoms, carbamoyl or a radical --SO.sub.2 --Z in which Z is as defined above; V is hydrogen or an alkyl radical which has 1 to 4 C atoms and can be substituted by carboxyl or sulfo groups or by derivatives thereof, alkoxy groups having 1 or 2 C atoms, halogen or hydroxyl; or is a radical ##STR3## in which Z, alk and Y are as defined above; R.sub.1 is hydrogen or C.sub.1 -C.sub.6 alkyl; the alk's independently of one another are polymethylene radicals having 2 to 6 C atoms or branched isomers thereof; m is 1 to 6, p is 1 to 6 and q is 1 to 6; and the benzene or naphthalene radical A can contain further substituents,are particularly suitable for dyeing or printing cellulose-containing fibre materials by the cold pad-batch process, and produce, at a high dye yield, dyeings and prints which have good fastness properties.

    摘要翻译： 式（1）的反应性染料其中D是蒽醌，酞菁，甲an，偶氮甲碱，二恶嗪，吩嗪，三苯甲烷，呫吨，噻吨酮，硝基芳基，萘醌，芘醌或苝四亚甲基亚胺染料的径向。 Q是氢或具有1至4个碳原子并可被羧基，磺基，氰基，羟基，C 1 -C 4烷氧基或卤素取代的烷基; B是基团-CH 2 n，-O-CH 2 n或-NH -CH 2 n，n是1至6; （1a）的化合物（1a）<图像>（1b）（1c）或（1d）Z是β-磺基乙基，β-硫代乙酰乙基，β-磷酰乙基，β-酰氧基乙基， β-卤代乙基或乙烯基; alk是具有1-6个C原子的亚烷基或其支链异构体; Y是氢，氯，溴，芴，羟基，硫酸酯，具有1至4个C原子的酰氧基，氰基，羧基，具有1至5个C原子的烷氧基羰基，氨基甲酰基或-SO 2 -Z基，其中Z如上定义; V是氢或具有1至4个C原子且可被羧基或磺基取代的烷基或其衍生物，具有1或2个C原子的烷氧基，卤素或羟基; 或者是其中Z，alk和Y如上所定义的基本 R1是氢或C1-C6烷基; 烷基彼此独立地是具有2至6个C原子的多亚甲基或其支链异构体; m为1〜6，p为1〜6，q为1〜6; 并且苯或萘基A可以含有其它取代基，特别适用于通过冷垫间歇法染色或印刷含纤维素纤维材料，并以高染料产率生产具有良好牢度性能的染色和印花。

    MIXTURES OF REACTIVE DYES AND THEIR USE IN A METHOD FOR TRICHROMATIC DYEING OR PRINTING
    9.
    发明申请
    MIXTURES OF REACTIVE DYES AND THEIR USE IN A METHOD FOR TRICHROMATIC DYEING OR PRINTING 有权
    反应性染料的混合物及其在三色染色或印刷方法中的应用

    公开(公告)号：US20100077555A1

    公开(公告)日：2010-04-01

    申请号：US12513464

    申请日：2007-10-30

    申请人： Georg Roentgen ,  Athanassios Tzikas ,  Hubert Jean Luc Christnacher

    发明人： Georg Roentgen ,  Athanassios Tzikas ,  Hubert Jean Luc Christnacher

    IPC分类号： C09B62/095 ,  C09B62/012

    CPC分类号： C09B62/4407 ,  C09B62/4413 ,  C09B62/4415 ,  C09B67/005 ,  C09B67/0059

    摘要： Dye mixtures, comprising at least one dye of formula and at least one dye from the group of formulae wherein Q1 is C1-C4alkyl, halogen or a radical —SO2—Z, Q2 and Q3 are each independently of the other C1-C4alkoxy, Q4 is C1-C4alkoxy, C1-C4alkyl, halogen or sulfo, Q5 is C1-C4alkoxy, C1-C4alkyl, C1-C4alkanoylamino, ureido, halogen or sulfo, R1, R2 and R3 are each independently of the others hydrogen or unsubstituted or substituted C1-C4alkyl, k and q are each independently of the other the number 0 or 1, n and p are each independently of the other the number 0, 1 or 2, m is the number 0, 1, 2 or 3, t is the number 1, 2 or 3, X1, X2 and X3 are each independently of the others halogen, 3-carboxypyridin-1-yl, 3-carbamoylpyridin-1-yl or a non-fibre-reactive substituent, and T1, T2 and T3 are each independently of the others a non-fibre-reactive substituent or a fibre-reactive radical of formula wherein (R4)0-2 denotes from 0 to 2 identical or different substituents from the group halogen, C1-C4alkyl, C1-C4alkoxy and sulfo, Z is vinyl or a radical —CH2—CH2—U and U is a group removable under alkaline conditions, Q is a group —CH(Hal)-CH2-Hal or —C(Hal)=CH2, and Hal is halogen, are suitable especially for the dichromatic or trichromatic dyeing or printing of cellulosic fibre materials and yield dyeings or prints having good reproducibility and good all-round fastness properties.

    摘要翻译： 染料混合物，其包含至少一种下式的染料和至少一种下式基团的染料，其中Q 1是C 1 -C 4烷基，卤素或基团-SO 2 -Z，Q 2和Q 3各自独立地为C 1 -C 4烷氧基，Q 4 C1-C4烷氧基，C1-C4烷基，卤素或磺基，Q5是C1-C4烷氧基，C1-C4烷基，C1-C4烷酰基氨基，脲基，卤素或磺基，R1，R2和R3各自独立地是氢或未取代的或取代的C1 -C 1-4烷基，k和q各自独立于数字0或1中的另一个，n和p各自独立于数字0,1或2中的另一个，m是数字0,1,2或3，t是 1,2或3个，X1，X2和X3各自独立地为卤素，3-羧基吡啶-1-基，3-氨基甲酰基吡啶-1-基或非纤维反应性取代基，T1，T2和T3 各自独立地为非纤维反应性取代基或具有下式的纤维反应性基团其中（R4）0-2表示0至2个相同或不同的取代基，基团卤素 ，C 1 -C 4烷基，C 1 -C 4烷氧基和磺基，Z是乙烯基或基团-CH 2 -CH 2 -U，U是在碱性条件下可除去的基团，Q是基团-CH（Hal）-CH 2 - Hal或-C（ Hal）= CH2，Hal是卤素，特别适用于纤维素纤维材料的二色或三色染色或印花，并且具有良好的再现性和良好的全面牢固性的产量染色或印花。

    Mixtures of reactive dyes and their use
    10.
    发明授权
    Mixtures of reactive dyes and their use 失效
    活性染料的混合物及其用途

    公开(公告)号：US07641724B2

    公开(公告)日：2010-01-05

    申请号：US10579364

    申请日：2004-11-08

    申请人： Athanassios Tzikas ,  Georg Roentgen

    发明人： Athanassios Tzikas ,  Georg Roentgen

    IPC分类号： C09D11/00 ,  C09B62/006 ,  C09B62/08

    CPC分类号： C09B67/005

    摘要： Dye mixtures comprising at least one dye of formula (I) together with at least one dye of formula (II) wherein the radicals are as defined in the claim, are suitable for dyeing or printing cellulosic fiber materials, while having a good build-up behavior, and yield dyeings of a deep shade having good fastness properties.

    摘要翻译： 包含至少一种式（I）染料与至少一种式（II）染料的染料混合物，其中基团如权利要求中所定义，适用于染色或印刷纤维素纤维材料，同时具有良好的聚集性 行为和屈服染色，具有良好的牢度特性。