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公开(公告)号：US4594185A
公开(公告)日：1986-06-10
申请号：US624322
申请日：1984-06-25
IPC分类号： C07C305/04 , C11D1/14 , C11D1/29 , C07C141/02
CPC分类号： C07C305/00 , C11D1/29 , Y10S516/03
摘要： Alkoxylated ether sulfate anionic surfactants of this invention are prepared by conventional procedures, e.g., oxyalkylation with propylene oxide or 1,2-butylene oxide of a straight chain plasticizer range alcohol; optionally followed by oxyalkylation with ethylene oxide or with a mixture of ethylene oxide and higher alkylene oxide; sulfation of the alkoxylated product; and neutralization of the sulfated derivative. The alkoxylated ether sulfate anionic surfactants of the present invention are liquids which exhibit superior detergency to polyester fabrics, excellent hard water stability, organic solubility, low foaming, low odor, and exhibit excellent compatibility with non-ionic and other surfactants in detergent formulations.
摘要翻译： 通过常规方法制备本发明的烷氧基化醚硫酸盐阴离子表面活性剂，例如用环氧丙烷或直链增塑剂范围醇的1,2-环氧丁烷进行烷氧基化; 随后用环氧乙烷或与环氧乙烷和更高级烯化氧的混合物进行烷氧基化; 烷氧基化产物的硫酸化; 并中和硫酸化衍生物。 本发明的烷氧基化醚硫酸盐阴离子表面活性剂是对涤纶织物具有优异的去污力，优异的硬水稳定性，有机溶解性，低起泡性，低气味，并且与洗涤剂配方中的非离子表面活性剂和其它表面活性剂具有优异相容性的液体。
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2.发明授权Alkoxylated ether sulfate anionic surfactants from branched chain plasticizer alcohols 失效来自支链增塑剂醇的烷氧基醚硫酸盐阴离子表面活性剂
公开(公告)号：US4608197A
公开(公告)日：1986-08-26
申请号：US624323
申请日：1984-06-25
IPC分类号： C07C305/06 , C11D1/14 , C11D1/29 , C07C141/02
CPC分类号： C07C305/00 , C11D1/29 , Y10S516/03
摘要： Alkoxylated ether sulfate anionic surfactants of this invention are prepared by conventional procedures, e.g., oxyalkylation with propylene oxide or 1,2-butylene oxide of a branched chain alcohol; optionally followed by oxyalkylation with ethylene oxide or with a mixture of ethylene oxide and higher alkylene oxide; sulfation of the alkoxylated product; and neutralization of the sulfated derivative. The alkoxylated ether sulfate anionic surfactants of the present invention are liquids which exhibit superior detergency to polyester fabrics, excellent hard water stability, low foaming, low odor, and exhibit excellent compatibility with non-ionic and other surfactants in detergent formulations.
摘要翻译： 通过常规方法制备本发明的烷氧基化醚硫酸盐阴离子表面活性剂，例如用环氧丙烷或支链醇的1,2-环氧丁烷进行烷氧基化; 随后用环氧乙烷或与环氧乙烷和更高级烯化氧的混合物进行烷氧基化; 烷氧基化产物的硫酸化; 并中和硫酸化衍生物。 本发明的烷氧基化醚硫酸盐阴离子表面活性剂是对涤纶织物具有优异洗涤性，优异的硬水稳定性，低起泡性，低气味和与洗涤剂配方中的非离子型和其它表面活性剂的相容性优异的液体。
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3.发明授权Alkoxylated ether sulfate anionic surfactants from plasticizer alcohol mixtures 失效来自增塑剂醇混合物的烷氧基醚硫酸盐阴离子表面活性剂
公开(公告)号：US4592875A
公开(公告)日：1986-06-03
申请号：US624324
申请日：1984-06-25
IPC分类号： C07C305/04 , C11D1/14 , C11D1/29 , C07C141/02
CPC分类号： C07C305/00 , C11D1/29 , Y10S516/03
摘要： Mixtures of alkoxylated ether sulfate anionic surfactants of this invention are prepared by conventional procedures, e.g., oxyalkylation with propylene oxide or 1,2-butylene oxide of a plasticizer range linear or branched "oxo" alcohol; optionally followed by oxyalkylation with ethylene oxide or with a mixture of ethylene oxide and higher alkylene oxide; sulfation of the alkoxylated product; and neutralization of the sulfated derivative. The alkoxylated ether sulfate anionic surfactant compositions of the present invention are liquids which exhibit superior detergency to polyester fabrics, excellent hard water stability, low foaming, low odor, and exhibit excellent compatibility with non-ionic and other surfactants in detergent formulations. The compositions of the invention are prepared as concentrates containing high proportions of active ingredients which are capable of being diluted with water without formation of a gel phase or lumps and as surfactants exhibit properties comparable to commercial surfactants prepared from "detergent" range alcohols.
摘要翻译： 通过常规方法制备本发明的烷氧基化醚硫酸盐阴离子表面活性剂的混合物，例如用环氧丙烷进行烷氧基化或直链或支链“氧代”醇的增塑剂范围的1,2-环氧丁烷; 随后用环氧乙烷或与环氧乙烷和更高级烯化氧的混合物进行烷氧基化; 烷氧基化产物的硫酸化; 并中和硫酸化衍生物。 本发明的烷氧基化醚硫酸盐阴离子表面活性剂组合物是对涤纶织物具有优异的去污力，优异的硬水稳定性，低起泡性，低气味，并且与洗涤剂配方中的非离子表面活性剂和其它表面活性剂的相容性优异的液体。 本发明的组合物制备为含有高比例活性成分的浓缩物，其能够用水稀释而不形成凝胶相或团块，并且表面活性剂表现出与“洗涤剂”范围醇制备的市售表面活性剂相当的性能。
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公开(公告)号：US4026830A
公开(公告)日：1977-05-31
申请号：US605796
申请日：1975-08-18
申请人： Hyman D. Gillman , James P. King
发明人： Hyman D. Gillman , James P. King
CPC分类号： C07F9/02 , C07F9/304 , C08G79/14 , C08K5/5313
摘要： Tantalum phosphinates of the general formula: [Ta(OPRR'O).sub.p (Z).sub.5b.-p ].sub.n wherein 1.ltoreq.p.ltoreq.3; R and R' are aryl groups; Z may be a halo, alkoxy, or aryloxy group or a mixture thereof; and n may be any number. The preparation thereof is based on the reaction of a tantalum pentavalent compound (TaZ.sub.5) with a phosphinic acid (RR'P(O)OH) in a dry inert solvent at reflux temperature. Such compounds are useful in high temperature laminates as fillers. Oxide hydrates of these compounds may be prepared by hydrolysis and are similarly useful in high temperature laminates as fillers.
摘要翻译： 具有以下通式的钽亚磷酸盐：[Ta（OPRR'O）p（Z）5-p] n其中1≤n≤3; R和R'是芳基; Z可以是卤素，烷氧基或芳氧基或其混合物; n可以是任何数字。 其制备方法是基于钽酸五价化合物（TaZ5）与次膦酸（RR'P（O）OH）在回流温度下在干惰性溶剂中的反应。 这些化合物可用作高温层压材料作为填料。 这些化合物的氧化物水合物可以通过水解制备，并且类似地用作高温层压体作为填料。
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公开(公告)号：US06248228B1
公开(公告)日：2001-06-19
申请号：US09272550
申请日：1999-03-19
IPC分类号： C25D302
摘要： The use of alkali metal, alkaline earth metal, ammonium and substituted ammonium salts of alkyl and alkanol sulfonic acids as additives in pure metal and metal alloy halide electroplating baths has a number of unexpected benefits including wider useful current density range and improved appearance. The metals and metal alloys include but are not limited to tin, lead, copper, nickel, zinc, cadmium, tin/zinc, zinc/nickel and tin/nickel.
摘要翻译： 在纯金属和金属合金卤化物电镀浴中使用烷基和链烷醇磺酸的碱金属，碱土金属，铵和取代铵盐作为添加剂具有许多意想不到的优点，包括更宽的有用电流密度范围和改进的外观。 金属和金属合金包括但不限于锡，铅，铜，镍，锌，镉，锡/锌，锌/镍和锡/镍。
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公开(公告)号：US4692535A
公开(公告)日：1987-09-08
申请号：US944896
申请日：1986-12-22
申请人： Harold V. Larson , Hyman D. Gillman
发明人： Harold V. Larson , Hyman D. Gillman
IPC分类号： C07D301/32 , C07D303/04 , C08G18/48
CPC分类号： C07D301/32
摘要： Process for improving the quality of propylene oxide contaminated with minute quantities of high molecular weight poly(propylene oxide) by contacting liquid propylene oxide with certain solid adsorbents, such as activated carbon and attapulgite, thereby obtaining a substantially pure oxide product essentially free of high molecular weight poly(propylene oxide) suitable for conversion of polyether polyols capable of producing high resilient flexible polyurethane foams exhibiting high rise and substantially free of blow hole formation.
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公开(公告)号：US06562220B2
公开(公告)日：2003-05-13
申请号：US09862166
申请日：2001-05-21
IPC分类号： C25D302
摘要： The use of alkali metal, alkaline earth metal, ammonium and substituted ammonium salts of alkyl and alkanol sulfonic acids as additives in pure metal and metal alloy sulfate electroplating baths has a number of unexpected benefits including wider useful current density range, improved appearance and in the case of tin improved oxidative stability. The metals and alloys include but are not limited to tin, nickel, copper, chromium, cadmium, iron, rhodium, ruthenium, iron/zinc and tin/zinc.
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公开(公告)号：US06183619B2
公开(公告)日：2001-02-06
申请号：US09272551
申请日：1999-03-19
IPC分类号： C25D302
摘要： The use of alkali metal, alkaline earth metal, ammonium and substituted ammonium salts of alkyl and alkanol sulfonic acids as additives in pure metal and metal alloy sulfonic acid electroplating baths has a number of unexpected benefits including wider useful current density range, improved appearance and in the case of tin improved oxidative stability. An additional significant appearance is to reduce the overall costs of this type of bath with the more economical salts of alkyl and alkanol sulfonic acids. The metals and metal alloys include but are not limited to tin, lead, copper, nickel, zinc, tin/lead, tin/lead/copper, tin/zinc and zinc/nickel.
摘要翻译： 在纯金属和金属合金磺酸电镀浴中使用烷基和链烷醇磺酸的碱金属，碱土金属，铵和取代的铵盐作为添加剂具有许多意想不到的优点，包括更广泛的有用电流密度范围，改进的外观和 锡的情况改善了氧化稳定性。 另外一个显着的外观是用更经济的烷基和链烷醇磺酸盐降低这种类型的浴的总体成本。 金属和金属合金包括但不限于锡，铅，铜，镍，锌，锡/铅，锡/铅/铜，锡/锌和锌/镍。
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公开(公告)号：US06179985B2
公开(公告)日：2001-01-30
申请号：US09273119
申请日：1999-03-19
IPC分类号： C25D300
摘要： The use of alkali metal, alkaline earth metal, ammonium and substituted ammonium salts of alkyl and alkanol sulfonic acids as additives in pure metal and metal alloy fluoroborate electroplating baths has a number of unexpected benefits including wider useful current density range and improved appearance. The metals and metal alloys include but are not limited to tin, lead, copper, cadmium, indium, iron, tin/lead and tin/lead copper.
摘要翻译： 在纯金属和金属合金氟硼酸盐电镀浴中使用烷基和链烷醇磺酸的碱金属，碱土金属，铵和取代的铵盐作为添加剂具有许多意想不到的优点，包括更宽的有用电流密度范围和改善的外观。 金属和金属合金包括但不限于锡，铅，铜，镉，铟，铁，锡/铅和锡/铅铜。
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公开(公告)号：US06251253B1
公开(公告)日：2001-06-26
申请号：US09272800
申请日：1999-03-19
IPC分类号： C25D302
摘要： The use of alkali metal, alkaline earth metal, ammonium and substituted ammonium salts of alkyl and alkanol sulfonic acids as additives in pure metal and metal alloy sulfate electroplating baths has a number of unexpected benefits including wider useful current density range, improved appearance and in the case of tin improved oxidative stability. The metals and alloys include but are not limited to tin, nickel, copper, chromium, cadmium, iron, rhodium, ruthenium, iron/zinc and tin/zinc.
摘要翻译： 在纯金属和金属合金硫酸盐电镀浴中使用烷基和链烷醇磺酸的碱金属，碱土金属，铵和取代的铵盐作为添加剂具有许多意想不到的优点，包括更宽的有用电流密度范围，改进的外观和 锡的情况改善了氧化稳定性。 金属和合金包括但不限于锡，镍，铜，铬，镉，铁，铑，钌，铁/锌和锡/锌。
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