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公开(公告)号：US4061684A
公开(公告)日：1977-12-06
申请号：US736939
申请日：1976-10-29
IPC分类号： C08G65/334 , C07C43/00 , C10M7/16
CPC分类号： C08G65/3344
摘要： Highly branched polyether polyols of high molecular weight (such as over 12,000) are made by coupling an alkoxylated polyglycerol, by reaction of the sodium alcoholate of the oxyalkylated polyglycerol with a dibenzenesulfo or ditoluenesulfo ester of a diol containing 2 to 6 carbon atoms. Products obtained are viscous resinous products which are particularly suitable for use as hydrophilic water-swellable gels and other purposes.
摘要翻译： 通过使烷氧基化聚甘油的醇钠与含有2至6个碳原子的二醇的二苯磺酸或二甲苯磺酸酯的反应，通过偶联烷氧基化聚甘油来制备高分子量的高支化聚醚多元醇（如12,000以上）。 获得的产品是特别适合用作亲水性水溶胀性凝胶和其它目的的粘性树脂产品。
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公开(公告)号：US4113785A
公开(公告)日：1978-09-12
申请号：US736959
申请日：1976-10-29
IPC分类号： C08G65/26 , C08G65/28 , C08G65/321 , C08G65/331 , C07C41/02 , C07C43/10
CPC分类号： C08G65/3312 , C08G65/26 , C08G65/321 , Y10S516/01
摘要： New polyether polyols of predetermined structure are prepared by reacting polyether bis alcoholates with selected bis epoxides. Specifically, a polyoxyalkylene glycol is converted to the bis alcoholate, and then the bis alcoholate is reacted with an equivalent amount of a glycol bis glycidyl ether, with the reactants being mixed together all at once. The polyether polyalcoholate thus obtained is converted to a high molecular weight polyether polyol by acid neutralization or ion exchange.
摘要翻译： 通过聚醚双醇酯与选择的双环氧化物反应制备具有预定结构的新型聚醚多元醇。 具体地说，将聚氧化亚烷基二醇转化成双醇化物，然后使双醇化物与等量的二醇双缩水甘油醚反应，同时将反应物全部混合在一起。 由此获得的聚醚多元醇酸通过酸中和或离子交换转化为高分子量聚醚多元醇。
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公开(公告)号：US4077894A
公开(公告)日：1978-03-07
申请号：US754562
申请日：1976-12-27
CPC分类号： C09K5/20 , B01D19/0404
摘要： A glycol-based antifreeze formulation containing as a defoaming agent, from 0.001% to about 1.0% by weight of a mixture containing a compound of the formula ##STR1## WHEREIN R is an alkyl, alkoxyalkyl, hydroxyalkyl, or dihydroxyalkyl group having from 1 to 6 carbon atoms, R.sup.1 is hydrogen, methyl or ethyl, R.sup.2 is an alkyl group having 1 to 8 carbon atoms, p is an integer from 1 to 20, and n is an integer from 1 to 14; and a compound of the formulaRO--(C.sub.6 H.sub.10 O.sub.5).sub.p --Hwherein R and p are as defined above.
摘要翻译： 含有作为消泡剂的二醇类防冻剂配方，其含有0.001％至约1.0％重量的含有下式化合物的混合物是具有1至1个碳原子的烷基，烷氧基烷基，羟基烷基或二羟基烷基， 6个碳原子，R 1是氢，甲基或乙基，R 2是具有1至8个碳原子的烷基，p是1至20的整数，n是1至14的整数; 和式RO-（C6H10O5）p-H的化合物，其中R和p如上所定义。
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公开(公告)号：US4077895A
公开(公告)日：1978-03-07
申请号：US756177
申请日：1977-01-03
CPC分类号： C09K5/20 , B01D19/0404
摘要： A glycol-based antifreeze formulation containing as a defoaming agent, from 0.001% to about 1.0% by weight of the reaction product of a polyglycerol having from 5 to 30 glycerol units, and a glycidyl ether having the formula ##STR1## wherein n is an integer from 1 to 20, R is hydrogen, methyl or ethyl, and Z is an alkyl group having from 1 to 8 carbon atoms or the group having the formula ##STR2##
摘要翻译： 含有作为消泡剂的二醇类防冻剂配方，含有5-30个甘油单元的聚甘油的反应产物的0.001重量％至约1.0重量％，以及具有下式的缩水甘油醚：其中n为 1至20的整数，R是氢，甲基或乙基，Z是具有1至8个碳原子的烷基或具有式“IMAGE”
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公开(公告)号：US4086279A
公开(公告)日：1978-04-25
申请号：US720952
申请日：1976-09-07
CPC分类号： C08G65/2609 , C08G65/34 , C08G65/48 , C08L71/00 , C11D1/721 , Y10S516/01
摘要： Nonionic surfactant compositions are made by reacting a 3 to 30-unit polyglycerol as hydrophile with a hydrophobic glycidyl ether in sufficient quantity to substitute 4 to 25% of the hydroxy groups of the polyglycerol. By using glycidyl ethers (which can be made conveniently by reaction of hydrophobic alcohol with epichlorohydrin) it becomes possible to avoid the expense of working with long-chain 1,2-epoxides. The surfactant compositions obtained have solubility and stability in a variety of concentrated ionic solutions, and especially in basic media.
摘要翻译： 非离子表面活性剂组合物通过使3至30单元的亲水性聚甘油与足够量的疏水性缩水甘油醚反应来代替聚甘油4至25％的羟基。 通过使用缩水甘油醚（可以通过疏水性醇与表氯醇的反应方便地制备），可以避免与长链1,2-环氧化物的加工成本。 获得的表面活性剂组合物在各种浓缩的离子溶液中，特别是在碱性介质中具有溶解性和稳定性。
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