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    Process for the preparation of 3-hydrazino-1,2-benz-isothiazole 1,1-dioxides
    2.
    发明授权
    Process for the preparation of 3-hydrazino-1,2-benz-isothiazole 1,1-dioxides 失效
    3-肼基-1,2-苯并异噻唑1,1-二氧化物的制备方法

    公开(公告)号：US4667041A

    公开(公告)日：1987-05-19

    申请号：US706577

    申请日：1985-02-28

    申请人： Herbert Salzburg ,  Manfred Hajek ,  Gerd Hanssler

    发明人： Herbert Salzburg ,  Manfred Hajek ,  Gerd Hanssler

    IPC分类号： A01N43/80 ,  C07D275/06

    CPC分类号： C07D275/06 ,  A01N43/80

    摘要： A process for the preparation of a 3-hydrazino-1, 2-benzisothiazole 1,1-dioxide of the formula ##STR1## in which R.sup.1 and R.sup.2 each independently is hydrogen, alkyl, halogen, amino, hydroxyl or carboxyl, andR.sup.3 and R.sup.4 each independently is hydrogen, alkyl, cycloalkyl or aryl,comprising reacting a 3-keto-2H,3H-1,2-benzisothiazole 1,1-dioxide of the formula ##STR2## with a hydrazine of the formula ##STR3## in a molar ratio of 1:1 to 1:50, in an inert solvent, at a temperature between 75.degree. C. and 200.degree. C. and for a reaction time of 15 to 40 hours. The products, some of which are known, are fungicidally active and can also be used as intermediates.

    摘要翻译： 制备式“IMAGE”的3-肼基-1,2-苯并异噻唑1,1-二氧化物的方法，其中R 1和R 2各自独立地为氢，烷基，卤素，氨基，羟基或羧基，以及R 3和 R 4各自独立地是氢，烷基，环烷基或芳基，包括使式IMAGE的3-酮基-2H，3H-1,2-苯并异噻唑1,1-二氧化物与式IMAMA的肼反应 摩尔比为1:1至1:50，在惰性溶剂中，在75℃至200℃之间，反应时间为15至40小时。 其中一些已知的产品是杀真菌活性的并且也可以用作中间体。

    3-hydrazono-benzisothiazole 1,1-dioxide fungicides
    3.
    发明授权
    3-hydrazono-benzisothiazole 1,1-dioxide fungicides 失效
    3-肼基 - 苯并异噻唑1,1-二氧化物杀真菌剂

    公开(公告)号：US4666930A

    公开(公告)日：1987-05-19

    申请号：US707361

    申请日：1985-03-01

    申请人： Herbert Salzburg ,  Manfred Hajek ,  Gerd Hanssler

    发明人： Herbert Salzburg ,  Manfred Hajek ,  Gerd Hanssler

    IPC分类号： A01N43/80 ,  A01N47/24 ,  A01N47/34 ,  C07D275/06 ,  C07D417/12

    CPC分类号： C07D275/06 ,  A01N43/80 ,  A01N47/24 ,  A01N47/34 ,  C07D417/12

    摘要： Compounds of the formula ##STR1## in which R.sup.1 is alkyl, cycloalkyl, aryl or hydrogen,R.sup.2 is --CO--R.sup.3,R.sup.3 is alkyl, alkenyl or cycloalkyl, or is phenyl which is optionally substituted, or is alkoxy or benzyl, or is phenoxy which is optionally substituted, or is phenoxymethyl, alkylamino, cycloalkylamino or phenylamino, orR.sup.1 and R.sup.2 together are a ##STR2## group, R.sup.4 and R.sup.5 each independently is hydrogen, alkyl, cycloalkenyl or phenylalkenyl, or is phenyl which is optionally substituted by alkyl, halogen and/or alkoxy, or is furyl, orR.sup.4 and R.sup.5 together are alkylene having 4 to 6 carbon atoms,are fungicidally active. Those compounds wherein R.sup.3 is alkylamino, cycloalkylamino or phenylamino, with the exception of the compound in which R.sup.1 is hydrogen and R.sup.6 is phenylamino, are new.

    摘要翻译： 式中，R 1为烷基，环烷基，芳基或氢的化合物，R 2为-CO-R 3，R 3为烷基，烯基或环烷基，或为任选取代的苯基，或为烷氧基或苄基，或为 任选被取代的苯氧基，或者是苯氧基甲基，烷基氨基，环烷基氨基或苯基氨基，或者R 1和R 2一起是一个基团，R 4和R 5各自独立地是氢，烷基，环烯基或苯基烯基，或者是任选地被 烷基，卤素和/或烷氧基，或是呋喃基，或R4和R5一起是具有4-6个碳原子的亚烷基，是杀真菌活性的。 其中R 3是烷基氨基，环烷基氨基或苯基氨基的那些化合物，除了其中R 1是氢和R 6是苯基氨基的化合物外，是新的。

    Salts of 2-keto-2H, 3H-1,2-benzisothiazole 1,1-dioxide as microbicides
    4.
    发明授权
    Salts of 2-keto-2H, 3H-1,2-benzisothiazole 1,1-dioxide as microbicides 失效

    公开(公告)号：US4683233A

    公开(公告)日：1987-07-28

    申请号：US704439

    申请日：1985-02-22

    申请人： Herbert Salzburg ,  Manfred Hajek ,  Gerd Hanssler ,  Varl-Heinz Kuck

    发明人： Herbert Salzburg ,  Manfred Hajek ,  Gerd Hanssler ,  Varl-Heinz Kuck

    IPC分类号： A01N47/44 ,  A01N20060101 ,  A01N37/44 ,  A01N43/16 ,  A01N43/40 ,  A01N43/50 ,  A01N43/54 ,  A01N43/56 ,  A01N43/60 ,  A01N43/653 ,  A01N43/76 ,  A01N43/80 ,  A01N43/84 ,  A01N43/90 ,  A01N47/42

    CPC分类号： A01N43/56 ,  A01N37/44 ,  A01N43/16 ,  A01N43/40 ,  A01N43/50 ,  A01N43/54 ,  A01N43/60 ,  A01N43/653 ,  A01N43/76 ,  A01N43/80 ,  A01N43/84 ,  A01N43/90 ,  A01N47/44

    摘要： A method of combating fungi and bacteria which comprises applying to such fungi, bacteria or a habitat thereof, a fungicidally or bactericidally effective amount of at least one salt of 3-keto-2-, 3H-1,2-benzisothiazole 1,1-dioxide of the formula ##STR1## in which R.sup.1 represents hydrogen, alkyl having 1 to 18 carbon atoms, or alkyl which has 1 to 6 carbon atoms and is optionally monosubstituted to trisubstituted by hydroxyl and/or monosubstituted to trisubstituted by amino, or represents carboxyl-substituted alkyl having 1 to 4 carbon atoms, or phenyl which is optionally monosubstituted to trisubstituted by identical or different substituents from amongst nitro and chlorine, or represents cycloalkyl having 5 or 6 carbon atoms, or represents heterocyclic structures which are optionally saturated or unsaturated, are optionally monosubstituted to tetrasubstituted by alkyl having 1 to 4 carbon atoms or hydroxyl, and have 1 to 3 identical or different heteroatoms, and a total of 5 or 6 ring members,R.sup.2 represents alkyl having 1 to 18 atoms, or alkyl which has 1 to 6 carbon atoms and is optionally monosubstituted to trisubstituted by hydroxyl and/or monosubstituted to trisubstituted by amino, or represents carboxyl-substituted alkyl having 1 to 4 carbon atoms, or phenyl which is optionally monosubstituted to trisubstituted by identical or different substituents from amongst nitro and chlorine, or represent cycloalkyl having 5 or 6 carbon atoms, or represents heterocyclic structures which are optionally saturated or unsaturated, are optionally monosubstituted to tetrasubstituted by alkyl having 1 to 4 carbon atoms or hydroxyl, and have 1 to 3 identical or different heteroatoms, and a total of 5 or 6 ring members, andR.sup.3 represents hydrogen, alkyl, having 1 to 6 carbon atoms, NH.sub.2, ##STR2## benzyl, or hydroxyalkyl having 1 to 3 carbon atoms, with the exception of the mono-, di- and triethanolamine compounds, orR.sup.1 and R.sup.2 together with the nitrogen atom at which they are located, form a 5-membered or 6-membered ring which can optionally contain further heteroatoms, and can optionally be substituted by keto groups or fused-on 5-membered or 6-membered rings and/or alkyl having 1 to 4 carbon atoms, with the exception of the pyridine ring which is optionally mono- or disubstituted by methyl.

    Process for the production of dianhydrohexitol mixtures and the production of polymers from such mixtures
    5.
    发明授权
    Process for the production of dianhydrohexitol mixtures and the production of polymers from such mixtures 失效
    用于制备二羟基己糖醇混合物的方法和由这些混合物生产聚合物

    公开(公告)号：US4564645A

    公开(公告)日：1986-01-14

    申请号：US689357

    申请日：1985-01-07

    申请人： Herbert Salzburg ,  Manfred Hajek ,  Holger Meyborg

    发明人： Herbert Salzburg ,  Manfred Hajek ,  Holger Meyborg

    IPC分类号： C07D493/04 ,  C08G18/32 ,  C08G18/30

    CPC分类号： C07D493/04 ,  C08G18/3218

    摘要： Liquid dianhydrohexitol mixtures are prepared from diacylation products of hexitols and compounds such as organic carboxylic acids, carboxylic acid anhydrides, carboxylic acid halides, ketene and carbonic acid ester derivatives. More specifically, such diacylation products are simultaneously dehydrated and isomerized by subjecting them to a temperature of at least 130.degree. C. in the presence of a strong acid to yield diacylated dianhydro-hexitol isomer mixtures. These isomer mixtures are then converted to dianhydro-hexitol isomer mixtures by hydrolysis or transesterification. Suitable strong acids include proton acids, Lewis acids and heterogeneous acid catalysts (e.g., ion exchange resins). The mixtures of the present invention are characterized by a minimal tendency towards crystallization. These mixtures are particularly useful as chain extending agents in the production of polyurethanes.

    摘要翻译： 液体二脱水己糖醇混合物由己醇的二酰化产物和有机羧酸，羧酸酐，羧酸卤化物，乙烯酮和碳酸酯衍生物等化合物制备。 更具体地说，这样的二酰化产物通过在强酸存在下使其至少130℃的温度同时进行脱水和异构化，得到二酰化二脱氢 - 己糖醇异构体混合物。 然后通过水解或酯交换将这些异构体混合物转化为二脱氢己糖醇异构体混合物。 合适的强酸包括质子酸，路易斯酸和多相酸催化剂（如离子交换树脂）。 本发明的混合物的特征在于最小的结晶倾向。 这些混合物特别可用作聚氨酯生产中的扩链剂。

    Process for the production of dianhydrohexitol mixtures and liquid mixture of dianhydrohexitols
    6.
    发明授权
    Process for the production of dianhydrohexitol mixtures and liquid mixture of dianhydrohexitols 失效
    二脱水己醇混合物的生产方法和二脱水己醇的液体混合物

    公开(公告)号：US4506086A

    公开(公告)日：1985-03-19

    申请号：US515411

    申请日：1983-07-20

    申请人： Herbert Salzburg ,  Manfred Hajek ,  Holger Meyborg

    发明人： Herbert Salzburg ,  Manfred Hajek ,  Holger Meyborg

    IPC分类号： C07D493/04 ,  C08G18/32

    CPC分类号： C07D493/04 ,  C08G18/3218

    摘要： Liquid dianhydrohexitol mixtures are prepared from diacylation products of hexitols and compounds such as organic carboxylic acids, carboxylic acid anhydrides, carboxylic acid halides, ketene and carbonic acid ester derivatives. More specifically, such diacylation products are simultaneously dehydrated and isomerized by subjecting them to a temperature of at least 130.degree. C. in the presence of a strong acid to yield diacylated dianhydrohexitol isomer mixtures. These isomer mixtures are then converted to dianhydrohexitol isomer mixtures by hydrolysis or transesterification. Suitable strong acids include proton acids, Lewis acids and heterogeneous acid catalysts (e.g., ion exchange resins). The mixtures of the present invention are characterized by a minimal tendency towards crystallization. These mixtures are particularly useful as chain extending agents in the production of polyurethanes.

    摘要翻译： 液体二脱水己糖醇混合物由己醇的二酰化产物和有机羧酸，羧酸酐，羧酸卤化物，乙烯酮和碳酸酯衍生物等化合物制备。 更具体地说，这样的二酰化产物通过在强酸存在下经受至少130℃的温度同时进行脱水和异构化，得到二酰基二脱水己糖异构体混合物。 然后通过水解或酯交换将这些异构体混合物转化成二羟基己糖异构体混合物。 合适的强酸包括质子酸，路易斯酸和多相酸催化剂（如离子交换树脂）。 本发明的混合物的特征在于最小的结晶倾向。 这些混合物特别可用作聚氨酯生产中的扩链剂。

    Polyamines
    7.
    发明授权
    Polyamines 失效
    多胺

    公开(公告)号：US4642344A

    公开(公告)日：1987-02-10

    申请号：US690445

    申请日：1985-01-11

    申请人： Manfred Hajek ,  Herbert Salzburg ,  Heinz Ziemann

    发明人： Manfred Hajek ,  Herbert Salzburg ,  Heinz Ziemann

    IPC分类号： C07D251/70

    CPC分类号： C07D251/70

    摘要： The present invention relates to new polyamines corresponding to the formula ##STR1## in which R.sup.1 represents an alkyl, cycloalkyl or aryl group andR.sup.2 represents hydrogen or an alkyl group.The present invention is also directed to a process for the preparation of these amines by hydrogenating the corresponding trinitriles.

    摘要翻译： 本发明涉及对应于式“IMAGE”的新的多胺，其中R 1表示烷基，环烷基或芳基，R 2表示氢或烷基。 本发明还涉及通过氢化相应的三腈来制备这些胺的方法。