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    Process and catalyst for dehydrogenating primary alcohols to make carboxylic acid salts
    3.
    发明授权
    Process and catalyst for dehydrogenating primary alcohols to make carboxylic acid salts 有权
    用于使伯醇脱氢以制备羧酸盐的方法和催化剂

    公开(公告)号：US06376708B1

    公开(公告)日：2002-04-23

    申请号：US09547373

    申请日：2000-04-11

    申请人： David A. Morgenstern ,  Juan P. Arhancet ,  Howard C. Berk ,  William L. Moench, Jr. ,  James C. Peterson

    发明人： David A. Morgenstern ,  Juan P. Arhancet ,  Howard C. Berk ,  William L. Moench, Jr. ,  James C. Peterson

    IPC分类号： C07C5116

    CPC分类号： C07F9/3813 ,  B01J23/70 ,  B01J23/72 ,  B01J23/80 ,  B01J23/835 ,  B01J35/04 ,  B01J37/348 ,  C07C51/235 ,  C07C227/02 ,  C07C229/16

    摘要： This invention is directed to a process for making a salt of a carboxylic acid. The process comprises contacting a catalyst with an alkaline mixture comprising a primary alcohol. In one embodiment, for example, the catalyst comprises a metal support (preferably a metal sponge support) coated with copper. The support comprises at least about 10% (by weight) non-copper metal, and the copper-containing coating comprises from about 0.005 to about 0.5 grams of copper (per gram of said metal support). In another embodiment, the catalyst comprises a metal support (preferably a metal sponge support) coated with silver. The support comprises at least about 10% (by weight) non-silver metal, and the silver-containing coating comprises from about 0.005 to about 0.5 grams of copper (per gram of said metal support). In another embodiment, the catalyst comprises at least about 15% (by weight) non-copper metal, and at least about 10% (by weight) copper. In yet another embodiment, the catalyst comprises at least about 15% (by weight) non-silver metal, and at least about 10% (by weight) silver. In both these embodiments, it is particularly preferable for the catalyst to be in the form of a metal sponge. This invention is also directed to copper-containing and silver-containing catalysts which may, for example, be used in the above process. This invention is further directed to processes for making such catalysts.

    摘要翻译： 本发明涉及一种制备羧酸盐的方法。 该方法包括使催化剂与包含伯醇的碱性混合物接触。在一个实施方案中，例如，催化剂包含涂覆有铜的金属载体（优选金属海绵载体）。 载体包含至少约10％（重量）的非铜金属，并且含铜涂层包含约0.005至约0.5克铜（每克所述金属载体）。在另一个实施方案中，催化剂包含 金属支撑体（优选金属海绵支撑体）涂覆银。 载体包含至少约10％（重量）的非银金属，并且含银涂层包含约0.005至约0.5克铜（每克所述金属载体）。在另一个实施方案中，催化剂包含 至少约15％（重量）的非铜金属和至少约10％（重量）的铜。 在另一个实施方案中，催化剂包含至少约15％（重量）的非银金属和至少约10％（重量）的银。 在这两个实施方案中，特别优选催化剂为金属海绵形式。本发明还涉及可以在上述方法中使用的含铜和含银催化剂。 本发明还涉及制备这种催化剂的方法。

    Aqueous concentrate formulations having reduced eye irritancy
    10.
    发明授权
    Aqueous concentrate formulations having reduced eye irritancy 失效
    具有降低眼睛刺激性的浓缩水配方

    公开(公告)号：US5389598A

    公开(公告)日：1995-02-14

    申请号：US169693

    申请日：1993-12-17

    申请人： Howard C. Berk ,  James W. Kassebaum

    发明人： Howard C. Berk ,  James W. Kassebaum

    IPC分类号： A01N25/02 ,  A01N25/30 ,  A01N25/32 ,  A01N33/08 ,  A01N37/02 ,  A01N37/06 ,  A01N57/20 ,  A01N63/02 ,  A01N57/04 ,  A01N28/30

    CPC分类号： A01N25/32 ,  A01N57/20

    摘要： Disclosed are storage-stable aqueous concentrate formulations of pesticides or plant growth modifying agents containing sufficient amounts of an alkoxylated alkylamine surfactant to insure a high degree of pesticidal or plant growth modifying efficacy, wherein irritancy to eyes resulting from the presence of said surfactant is reduced by the presence of an effective amount of a C.sub.6-22 saturated or unsaturated alkyl monocarboxylic or dicarboxylic acid or mixture of such acids.

    摘要翻译： 公开了含有足够量的烷氧基化烷基胺表面活性剂的农药或植物生长调节剂的储存稳定含水浓缩物制剂，以确保高度的杀虫剂或植物生长调节效力，其中由所述表面活性剂的存在引起的对眼睛的刺激性由 存在有效量的C6-22饱和或不饱和烷基单羧酸或二羧酸或这些酸的混合物。