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公开(公告)号：US08097663B2
公开(公告)日：2012-01-17
申请号：US12441718
申请日：2007-10-01
IPC分类号： C08G63/60 , C08G67/02 , C08G69/26 , C08J3/00 , C08K5/34 , C08K5/48 , C08L67/00 , C08L73/00 , C08L77/00 , C08L79/00 , C09B67/00 , C09D5/00 , C09D11/00
CPC分类号： C09D11/36 , C09D11/326
摘要： A non-aqueous inkjet ink containing a pigment includes C.I. Pigment Violet 19 and a polymeric dispersant according to Formula (I): wherein, T represents hydrogen or a polymerization terminating group; Z represents the residue of polyethyleneimine having a number-average molecular weight of at least 100; A represents an oxyalkylene carbonyl group; T-C(O)An- represents a TPOAC-chain which is bound to Z through an amide bond; and n and m are integers wherein m is at least 2 and n is from 2 to 100; wherein the polymeric dispersant fulfills the conditions of: WTPOAC>57 and NAmide≧65 mol % with WTPOAC representing the ratio of the weight percentage of TPOAC-chains over the weight percentage of amide bonds in the polymeric dispersant; NAmide representing the mol % of amide bonds based on the total nitrogen content of the polymeric dispersant; and wherein the values of WTPOAC and NAmide are calculated from the total nitrogen content determined by dry combustion of the polymeric dispersant and from the amine content determined through potentiometric titration in a mixture of CH3COOH:THF (14.5:0.5) with 0.1N aqueous perchloric acid.
摘要翻译： 含有颜料的非水性喷墨油墨包括C.I. 颜料紫19和根据式（I）的聚合物分散剂：其中T表示氢或聚合终止基团; Z表示数均分子量为100以上的聚乙烯亚胺的残基; A表示氧化烯羰基; T-C（O）An-表示通过酰胺键与Z结合的TPOAC-链; 并且n和m是其中m为至少2且n为2至100的整数; 其中所述聚合物分散剂满足以下条件：WTPOAC> 55和NAmide≥65mol％，其中WTPOAC表示TPOAC链的重量百分比与聚合物分散剂中酰胺键的重量百分比的比率; 基于聚合物分散剂的总氮含量，NAmide代表酰胺键的摩尔％; 并且其中WTPOAC和NAmide的值根据通过聚合物分散剂的干燃烧确定的总氮含量和通过在CH 3 COOH:THF（14.5:0.5）与0.1N高氯酸盐的混合物中的电位滴定测定的胺含量来计算。 。
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公开(公告)号：US20090312463A1
公开(公告)日：2009-12-17
申请号：US12441718
申请日：2007-10-01
IPC分类号： C09D11/10
CPC分类号： C09D11/36 , C09D11/326
摘要： A non-aqueous inkjet ink containing a pigment includes C.I. Pigment Violet 19 and a polymeric dispersant according to Formula (I): wherein, T represents hydrogen or a polymerization terminating group; Z represents the residue of polyethyleneimine having a number-average molecular weight of at least 100; A represents an oxyalkylene carbonyl group; T-C(O)An- represents a TPOAC-chain which is bound to Z through an amide bond; and n and m are integers wherein m is at least 2 and n is from 2 to 100; wherein characterized in that the polymeric dispersant fulfills the conditions of: WTPOAC>57 and NAmide≧65 mol % with WTPOAC representing the ratio of the weight percentage of TPOAC-chains over the weight percentage of amide bonds in the polymeric dispersant; NAmide representing the mol % of amide bonds based on the total nitrogen content of the polymeric dispersant; and wherein the values of WTPOAC and NAmide are calculated from the total nitrogen content determined by dry combustion of the polymeric dispersant and from the amine content determined through potentiometric titration in a mixture of CH3COOH:THF (14.5:0.5) with 0.1N aqueous perchloric acid.
摘要翻译： 含有颜料的非水性喷墨油墨包括C.I. 颜料紫19和根据式（I）的聚合物分散剂：其中T表示氢或聚合终止基团; Z表示数均分子量为100以上的聚乙烯亚胺的残基; A表示氧化烯羰基; T-C（O）An-表示通过酰胺键与Z结合的TPOAC-链; 并且n和m是其中m为至少2且n为2至100的整数; 其特征在于，聚合物分散剂满足以下条件：WTPOAC> 55和NAmide> = 65mol％，WTPOAC代表TPOAC链的重量百分比与聚合物分散剂中酰胺键的重量百分比的比率; 基于聚合物分散剂的总氮含量，NAmide代表酰胺键的摩尔％; 并且其中WTPOAC和NAmide的值根据通过聚合物分散剂的干燃烧确定的总氮含量和通过在CH 3 COOH:THF（14.5:0.5）与0.1N高氯酸盐的混合物中的电位滴定测定的胺含量来计算。 。
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公开(公告)号：US20090270537A1
公开(公告)日：2009-10-29
申请号：US12441719
申请日：2007-10-02
IPC分类号： C09D11/10 , C08K5/3492
CPC分类号： C09D11/101
摘要： A non-aqueous inkjet ink includes C.I. Pigment Yellow 150 and a polymeric dispersant according to Formula (I): wherein, T represents hydrogen or a polymerization terminating group; Z represents the residue of polyethyleneimine having a number-average molecular weight of at least 100; A represents an oxyalkylene carbonyl group; T-C(O)An- represents a TPOAC-chain which is bound to Z through an amide bond; and n and m are integers wherein m is at least 2 and n is from 2 to 100; the polymeric dispersant fulfills the conditions of: WTPOAC>57 and NAmide≧65 mol % wherein WTPOAC represents the ratio of the weight percentage of TPOAC-chains over the weight percentage of amide bonds in the polymeric dispersant; NAmide represents the mol % of amide bonds based on the total nitrogen content of the polymeric dispersant; and the values of WTPOAC and NAmide are calculated from the total nitrogen content determined by dry combustion of the polymeric dispersant and from the amine content determined through potentiometric titration in a mixture of CH3COOH:THF (14.5:0.5) with 0.1N aqueous perchloric acid.
摘要翻译： 非水性喷墨油墨包括C.I. 颜料黄150和根据式（I）的聚合物分散剂：其中，T表示氢或聚合终止基团; Z表示数均分子量为100以上的聚乙烯亚胺的残基; A表示氧化烯羰基; T-C（O）An-表示通过酰胺键与Z结合的TPOAC-链; 并且n和m是其中m为至少2且n为2至100的整数; 聚合物分散剂满足以下条件：WTPOAC> 57和NAmide> = 65mol％，其中WTPOAC表示TPOAC链的重量百分比与聚合物分散剂中酰胺键的重量百分比的比率; 基于聚合物分散剂的总氮含量，NAmide表示酰胺键的摩尔％; 并且从通过聚合物分散剂的干燃烧确定的总氮含量和通过在CH 3 COOH:THF（14.5:0.5）与0.1N高氯酸的混合物中的电位滴定测定的胺含量计算WTPOAC和NAmide的值。
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公开(公告)号：US20100029813A1
公开(公告)日：2010-02-04
申请号：US12441725
申请日：2007-10-01
IPC分类号： C09D11/10
CPC分类号： C09D11/101
摘要： A non-aqueous inkjet ink includes a benzimidazolone pigment and a polymeric dispersant according to Formula (I): wherein, T represents hydrogen or a polymerization terminating group; Z represents the residue of polyethyleneimine having a number-average molecular weight of at least 100; A represents an oxyalkylene carbonyl group; T-C(O)An- represents a TPOAC-chain which is bound to Z through an amide bond; and n and m are integers wherein m is at least 2 and n is from 2 to 100; the polymeric dispersant fulfills the conditions of: WTPOAC>57 and NAmide≧65 mol % wherein WTPOAC represents the ratio of the weight percentage of TPOAC-chains over the weight percentage of amide bonds in the polymeric dispersant; NAmide represents the mol % of amide bonds based on the total nitrogen content of the polymeric dispersant; and the values of WTPOAC and NAmide are calculated from the total nitrogen content determined by dry combustion of the polymeric dispersant and from the amine content determined through potentiometric titration in a mixture of CH3COOH:THF (14.5:0.5) with 0.1N aqueous perchloric acid.
摘要翻译： 非水性喷墨油墨包括苯并咪唑酮颜料和根据式（I）的聚合物分散剂：其中T表示氢或聚合终止基团; Z表示数均分子量为100以上的聚乙烯亚胺的残基; A表示氧化烯羰基; T-C（O）An-表示通过酰胺键与Z结合的TPOAC-链; 并且n和m是其中m为至少2且n为2至100的整数; 聚合物分散剂满足以下条件：WTPOAC> 57和NAmide> = 65mol％，其中WTPOAC表示TPOAC链的重量百分比与聚合物分散剂中酰胺键的重量百分比的比率; 基于聚合物分散剂的总氮含量，NAmide表示酰胺键的摩尔％; 并且从通过聚合物分散剂的干燃烧确定的总氮含量和通过在CH 3 COOH:THF（14.5:0.5）与0.1N高氯酸的混合物中的电位滴定测定的胺含量计算WTPOAC和NAmide的值。
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公开(公告)号：US08138238B2
公开(公告)日：2012-03-20
申请号：US12441719
申请日：2007-10-02
IPC分类号： C07D243/08 , C08G63/60 , C08G67/02 , C08G69/26 , C08J3/00 , C08K5/34 , C08K5/48 , C08L67/00 , C08L73/00 , C08L77/00 , C08L79/00 , C09D5/00 , C09D11/00
CPC分类号： C09D11/101
摘要： A non-aqueous inkjet ink includes C.I. Pigment Yellow 150 and a polymeric dispersant according to Formula (I): wherein, T represents hydrogen or a polymerization terminating group; Z represents the residue of polyethyleneimine having a number-average molecular weight of at least 100; A represents an oxyalkylene carbonyl group; T-C(O)An- represents a TPOAC-chain which is bound to Z through an amide bond; and n and m are integers wherein m is at least 2 and n is from 2 to 100; the polymeric dispersant fulfills the conditions of: WTPOAC>57 and NAmide≧65 mol % wherein WTPOAC represents the ratio of the weight percentage of TPOAC-chains over the weight percentage of amide bonds in the polymeric dispersant; NAmide represents the mol % of amide bonds based on the total nitrogen content of the polymeric dispersant; and the values of WTPOAC and NAmide are calculated from the total nitrogen content determined by dry combustion of the polymeric dispersant and from the amine content determined through potentiometric titration in a mixture of CH3COOH:THF (14.5:0.5) with 0.1N aqueous perchloric acid.
摘要翻译： 非水性喷墨油墨包括C.I. 颜料黄150和根据式（I）的聚合物分散剂：其中，T表示氢或聚合终止基团; Z表示数均分子量为100以上的聚乙烯亚胺的残基; A表示氧化烯羰基; T-C（O）An-表示通过酰胺键与Z结合的TPOAC-链; 并且n和m是其中m为至少2且n为2至100的整数; 聚合物分散剂满足以下条件：WTPOAC> 57和NAmide≥65mol％其中WTPOAC表示TPOAC链的重量百分比与聚合物分散剂中酰胺键的重量百分比的比率; 基于聚合物分散剂的总氮含量，NAmide表示酰胺键的摩尔％; 并且从通过聚合物分散剂的干燃烧确定的总氮含量和通过在CH 3 COOH:THF（14.5:0.5）与0.1N高氯酸的混合物中的电位滴定测定的胺含量计算WTPOAC和NAmide的值。
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公开(公告)号：US08093312B2
公开(公告)日：2012-01-10
申请号：US12441725
申请日：2007-10-01
IPC分类号： C08G63/60 , C08G67/02 , C08G69/26 , C08J3/00 , C08K5/00 , C08K5/23 , C08L67/00 , C08L73/00 , C08L77/00 , C08L79/00 , C09B67/00 , C09D5/00 , C09D11/00
CPC分类号： C09D11/101
摘要： A non-aqueous inkjet ink includes a benzimidazolone pigment and a polymeric dispersant according to Formula (I): wherein, T represents hydrogen or a polymerization terminating group; Z represents the residue of polyethyleneimine having a number-average molecular weight of at least 100; A represents an oxyalkylene carbonyl group; T-C(O)An- represents a TPOAC-chain which is bound to Z through an amide bond; and n and m are integers wherein m is at least 2 and n is from 2 to 100; the polymeric dispersant fulfills the conditions of: WTPOAC>57 and NAmide≧65 mol % wherein WTPOAC represents the ratio of the weight percentage of TPOAC-chains over the weight percentage of amide bonds in the polymeric dispersant; NAmide represents the mol % of amide bonds based on the total nitrogen content of the polymeric dispersant; and the values of WTPOAC and NAmide are calculated from the total nitrogen content determined by dry combustion of the polymeric dispersant and from the amine content determined through potentiometric titration in a mixture of CH3COOH:THF (14.5:0.5) with 0.1N aqueous perchloric acid.
摘要翻译： 非水性喷墨油墨包括苯并咪唑酮颜料和根据式（I）的聚合物分散剂：其中T表示氢或聚合终止基团; Z表示数均分子量为100以上的聚乙烯亚胺的残基; A表示氧化烯羰基; T-C（O）An-表示通过酰胺键与Z结合的TPOAC-链; 并且n和m是其中m为至少2且n为2至100的整数; 聚合物分散剂满足以下条件：WTPOAC> 57和NAmide≥65mol％其中WTPOAC表示TPOAC链的重量百分比与聚合物分散剂中酰胺键的重量百分比的比率; 基于聚合物分散剂的总氮含量，NAmide表示酰胺键的摩尔％; 并且从通过聚合物分散剂的干燃烧确定的总氮含量和通过在CH 3 COOH:THF（14.5:0.5）与0.1N高氯酸的混合物中的电位滴定测定的胺含量计算WTPOAC和NAmide的值。
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7.发明授权Antihalation dye for photothermographic recording material and a recording process therefor 失效用于光热敏记录材料的抗晕染染料及其记录方法
公开(公告)号：US5945263A
公开(公告)日：1999-08-31
申请号：US862812
申请日：1997-05-30
CPC分类号： G03C1/49872 , G03C1/49854 , Y10S430/145
摘要： A photothermographic recording material comprising a support; a photo-addressable thermally developable element comprising a substantially light-insensitive organic silver salt, photosensitive silver halide in catalytic association with the substantially light-insensitive organic silver salt spectrally sensitized to the infrared region of the electromagnetic spectrum and a binder; and in a hydrophobic layer an antihalation dye according to the general formula (I): ##STR1## wherein R.sup.1 and R.sup.15 independently represent an alkyl group or an alkyl group substituted with at least one fluorine, chlorine, bromine or an alkoxy-, aryloxy- or ester-group; R.sup.2, R.sup.3, R.sup.16 and R.sup.17 independently represent an alkyl group; R.sup.4, R.sup.5, R.sup.6, R.sup.7, R.sup.18, R.sup.19, R.sup.20 and R.sup.21 independently represent hydrogen, chlorine, bromine, fluorine or a keto-, sulfo-, carboxy-, ester-, sulfonamide-, amide-, dialkylamino-, nitro-, cyano-, alkyl-, alkenyl-, aryl-, alkoxy- or aryloxy-group; or each of R.sup.4 together with R.sup.5, R.sup.5 together with R.sup.6, R.sup.6 together with R.sup.7, R.sup.18 together with R.sup.19, R.sup.19 together with R.sup.20 or R.sup.20 together with R.sup.21 may independently constitute the atoms necessary to complete a benzene ring; R.sup.8, R.sup.9, R.sup.10 and R.sup.11 independently represent hydrogen, an alkyl group or each of R.sup.1 together with R.sup.8, R.sup.8 together with R.sup.9, R.sup.9 together with R.sup.10, R.sup.10 together with R.sup.11 or R.sup.11 together with R.sup.15 may independently constitute the atoms necessary to complete a 5-atom or 6-atom carbocylic or heterocyclic ring; R.sup.12, R.sup.13 and R.sup.14 independently represent hydrogen, chlorine, bromine or fluorine; and A.sup.- is a fluorinated alkyl or aryl anion in which the degree of fluorination is greater than 70%; a production process therefor and a photothermographic recording process therefor.
摘要翻译： 一种光热记录材料，包括载体; 一种可光寻址的可热显影元件，包括基本上不光敏的有机银盐，感光卤化银与对电磁光谱的红外区域光谱敏化的基本上不光敏的有机银盐和粘合剂催化缔合; 并且在疏水层中具有根据通式（I）的防光晕染料：其中R 1和R 15独立地表示烷基或被至少一个氟，氯，溴或烷氧基 - ，芳氧基或酯 - 取代的烷基， 组; R2，R3，R16和R17独立地表示烷基; R4，R5，R6，R7，R18，R19，R20和R21独立地表示氢，氯，溴，氟或酮基，磺基，羧基，酯 - ，磺酰胺 - ，酰胺 - ，二烷基氨基 - ，硝基 - 氰基，烷基 - ，烯基 - ，芳基 - ，烷氧基 - 或芳氧基 - 或R 4与R 5，R 5，R 6，R 6一起与R 7，R 18一起与R 19，R 19一起与R 20或R 20一起与R 21一起独立地构成完成苯环所必需的原子; R 8，R 9，R 10和R 11独立地表示氢，烷基或R 1与R 8，R 8与R 9，R 9一起与R 10，R 10一起与R 11或R 11一起与R 15一起可以独立地构成完成 5-原子或6-原子碳环或杂环; R 12，R 13和R 14独立地表示氢，氯，溴或氟; A是氟化烷基或芳基阴离子，其中氟化度大于70％; 其生产方法及其光热敏记录方法。
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8.发明授权
公开(公告)号：US5876915A
公开(公告)日：1999-03-02
申请号：US889481
申请日：1997-07-08
CPC分类号： C09B23/0066 , C09B23/0016 , C09B23/0075 , C09B23/086 , G03C1/49854 , G03C1/28 , G03C1/49863 , Y10S430/145
摘要： A photothermographic recording material comprising a support and a photo-addressable thermally developable element comprising a substantially light-insensitive organic silver salt, a reducing agent therefor in thermal working relationship therewith, photosensitive silver halide spectrally sensitized with a dye and in catalytic association with the substantially light-insensitive organic silver salt and a binder, characterized in that the dye is represented by formula (I): ##STR1## with an anion if necessary for charge compensation, wherein Z.sup.1 and Z.sup.2 independently represent S, O or Se; R.sup.1 and R.sup.13 independently represent an alkylene group; X.sup.1 and X.sup.2 independently represent a --(C.dbd.O)--R.sup.18, a --(SO.sub.2)R.sup.19 or a (S.dbd.O)--R.sup.20 group where R.sup.18, R.sup.19, and R.sup.20 independently represent an alkoxy-, aryloxy-, amino- or substituted amino-group.
摘要翻译： 一种光热记录材料，其包括支持体和可光寻址的热显影元件，其包含基本上不光敏的有机银盐，与其热加工关系的还原剂，用染料光谱感光并与基本上 光敏性有机银盐和粘合剂，其特征在于染料由式（I）表示：如果需要，用阴离子进行电荷补偿，其中Z1和Z2独立地表示S，O或Se; R1和R13独立地表示亚烷基; X1和X2独立地表示 - （C = O）-R18， - （SO2）R19或（S = O）-R20基团，其中R18，R19和R20独立地表示烷氧基 - ，芳氧基 - ，氨基 - 或 取代氨基。
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公开(公告)号：US08871015B2
公开(公告)日：2014-10-28
申请号：US13501256
申请日：2010-10-15
申请人： Geert Deroover
发明人： Geert Deroover
IPC分类号： C09D11/02 , C08K5/22 , C08K5/3437 , C08K5/3447 , C09B48/00 , C09B29/33 , C09B67/22 , C09B67/20 , C09B67/46 , C09D11/101 , C09D11/326 , C09D11/36 , C09D11/40 , C09D11/30
CPC分类号： C09B29/331 , C09B67/0041 , C09B67/0051 , C09B67/0069 , C09B67/0086 , C09D11/101 , C09D11/30 , C09D11/326 , C09D11/36 , C09D11/40
摘要： Non-aqueous pigment dispersions exhibiting improved dispersion quality and/or stability were prepared for a specific selection of naphthol AS pigments, diketopyrrolo-pyrrole pigments and quinacridone pigments, by using specific yellow monoazo dispersion synergists. The non-aqueous pigment dispersions can be advantageously used in inkjet inks inkjet printing methods.
摘要翻译： 通过使用特定的黄色单偶氮分散协同剂，制备了表现出改善的分散质量和/或稳定性的非水性颜料分散体，用于特定选择萘酚AS颜料，二酮吡咯并 - 吡咯颜料和喹吖啶酮颜料。 非水性颜料分散体可以有利地用于喷墨油墨喷墨印刷方法中。
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10.发明授权Pigment dispersions with polymeric dispersants having pending chromophore groups 有权具有悬浮发色团的聚合物分散剂的颜料分散体公开(公告)号：US08759441B2
公开(公告)日：2014-06-24
申请号：US11995330
申请日：2006-06-23
CPC分类号： C09B69/106 , C09B67/0033 , C09B67/0036 , C09B67/0051 , C09B67/0063 , C09B67/009 , C09B69/10 , C09B69/109 , C09D11/101 , C09D11/326
摘要： A pigment dispersion includes a color pigment and a polymeric dispersant having at least one pending chromophore group covalently bound to the polymeric backbone of the polymeric dispersant through a linking group, wherein the at least one pending chromophore group is a derivative from a color pigment selected from the group consisting of monoazo pigments, disazo pigments, β-naphtol pigments, naphtol AS pigments, azo pigment lakes, benzimidazolone pigments, disazo condensation pigments, metal complex pigments, isoindolinone pigments, isoindolinine pigments, phthalocyanine pigments, quinacridone pigments, diketopyrrolo-pyrrole pigments, thioindigo pigments, anthraquinone pigments, anthrapyrimidine pigments, indanthrone pigments, flavanthrone pigments, pyranthrone pigments, anthanthrone pigments, isoviolanthrone pigments, aluminum pigment lakes, dioxazine pigments, triarylcarbonium pigments, and quinophthalone pigments; the at least one pending chromophore group is a chromophore group occurring as a side group on the polymeric backbone and not a group in the polymeric backbone itself or occurring solely as an end group of the polymeric backbone; the linking group consists of all the atoms between the polymeric backbone and the first atom of the aromatic group by which the pending chromophore group is linked to the polymeric backbone; the polymeric dispersant has a polymeric backbone with a polymerization degree between 5 and 1,000; and at most 30 % of the monomer units of the polymeric backbone have a pending chromophore group. The pigment dispersion can be advantageously used in inkjet inks. Also disclosed is a method for preparing the pigment dispersion including the step of preparing the polymeric dispersant by copolymerizing a monomer already containing the pending chromophore group.
摘要翻译： 颜料分散体包括着色颜料和聚合物分散剂，其具有通过连接基团与聚合物分散剂的聚合物主链共价结合的至少一个待处理的发色团，其中所述至少一个未完成的发色团是来自选自以下的颜色颜料的衍生物： 由单偶氮颜料，双偶氮颜料，萘酚颜料，萘酚AS颜料，偶氮颜料湖，苯并咪唑酮颜料，双偶氮缩合颜料，金属络合颜料，异吲哚啉酮颜料，异吲哚啉颜料，酞菁颜料，喹吖啶酮颜料，二酮吡咯并 - 吡咯 颜料，硫靛颜料，蒽醌颜料，蒽嘧啶颜料，阴丹酮颜料，黄烷酮酮颜料，吡喃酮颜料，蒽醌颜料，异卤蒽酮颜料，铝颜料湖，二恶嗪颜料，三芳基碳鎓颜料和喹酞酮颜料; 至少一个未决发色团组是作为聚合物主链上的侧基而不是聚合物主链本身中的基团发生或仅作为聚合物主链的端基发生的发色团。 连接基团由聚合物主链和芳族基团的第一个原子之间的所有原子组成，待处理的发色团通过该原子连接到聚合物主链上; 聚合物分散剂具有聚合度为5至1,000的聚合物主链; 并且至多30％的聚合物主链的单体单元具有未决的发色团组。 颜料分散体可以有利地用于喷墨油墨中。 还公开了一种制备颜料分散体的方法，其包括通过使已经含有未完成发色团的单体共聚制备聚合物分散剂的步骤。
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