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    Method for producing propylene oxide
    1.
    发明授权
    Method for producing propylene oxide 有权
    生产环氧丙烷的方法

    公开(公告)号：US06881853B2

    公开(公告)日：2005-04-19

    申请号：US10484204

    申请日：2002-07-18

    申请人： Joaquim Henrique Teles ,  Alwin Rehfinger ,  Anne Berg ,  Peter Rudolf ,  Norbert Rieber ,  Peter Bassler

    发明人： Joaquim Henrique Teles ,  Alwin Rehfinger ,  Anne Berg ,  Peter Rudolf ,  Norbert Rieber ,  Peter Bassler

    IPC分类号： C07D301/12

    CPC分类号： C07D301/12 ,  Y02P20/582

    摘要： A process for preparing propylene oxide comprises at least the following steps: (a) propene is reacted with a hydroperoxide in a solvent in the presence of a zeolite catalyst to give a mixture (M0), where the mixture (M0) comprises propylene oxide, solvent, unreacted propene, unreacted hydroperoxide and oxygen, (b) the propylene oxide is separated from the mixture (M0) so as to give a mixture (M1) which comprises unreacted propene and oxygen, (c) the mixture (M1) is brought into contact with a liquid medium comprising at least a solvent to give the mixtures (M2) and (M3), where the mixture (M3) comprises part of the unreacted propene and oxygen and the mixture (M2) comprises solvent and residual propene, and  the mixture (M3) which has been separated off and comprises unreacted propene and oxygen has a ratio of oxygen to propene such that the mixture (M3) is not ignitable, and  the mixture (M2) is fed to at least one reaction of propene with hydroperoxide.

    摘要翻译： 制备环氧丙烷的方法至少包括以下步骤：（a）在沸石催化剂存在下，使丙烯与溶剂中的氢过氧化物反应得到混合物（M 0），其中混合物（M 0）包含丙烯 氧化物，溶剂，未反应的丙烯，未反应的氢过氧化物和氧气，（b）将环氧丙烷与混合物（M 0）分离，得到包含未反应的丙烯和氧的混合物（M 1），（c）混合物 M 1）与包含至少一种溶剂的液体介质接触以得到混合物（M 2）和（M 3），其中混合物（M 3）包含部分未反应的丙烯和氧气以及混合物（M 2）包括溶剂和残余丙烯，并且已经分离并包含未反应的丙烯和氧的混合物（M 3）具有氧与丙烯的比例，使得混合物（M 3）不可燃，并且混合物（M 2）进料至丙烯与氢过氧化物的至少一个反应。

    Method for producing an epoxide
    2.
    发明授权
    Method for producing an epoxide 有权
    环氧化物的制造方法

    公开(公告)号：US07026493B2

    公开(公告)日：2006-04-11

    申请号：US10470275

    申请日：2002-02-06

    申请人： Joaquim Henrique Teles ,  Alwin Rehfinger ,  Anne Berg ,  Peter Rudolf ,  Norbert Rieber ,  Peter Bassler

    发明人： Joaquim Henrique Teles ,  Alwin Rehfinger ,  Anne Berg ,  Peter Rudolf ,  Norbert Rieber ,  Peter Bassler

    IPC分类号： C07D301/12

    CPC分类号： C07D301/19 ,  C07D301/12 ,  C07D301/32

    摘要： An organic compound having at least one C—C double bond is epoxidized by means of hydrogen peroxide in the presence of at least one catalytically active compound and at least one solvent, wherein a product mixture comprising α-hydroperoxyalcohols is reduced using at least one reducing agent. The process advantageously comprises at least the following steps: (i) reacting an organic compound having at least one C—C double bond with hydrogen peroxide in the presence of at least one catalytically active compound and at least one solvent to give a product mixture P1 comprising α-hydroperoxyalcohols; (ii) separating an epoxide formed in the reaction in step (i) and the unreacted organic compound having at least one C—C double bond from P1 or P1′ to give a product mixture P2 or P2′, where P2 comprises the α-hydroperoxyalcohols formed as by-product in the reaction in step (i) and P2′ is largely free of α-hydroperoxyalcohols; (iii) treating P1 and/or P2 with at least one reducing agent so that the α-hydroperoxyalcohols are converted into corresponding glycols to give a product mixture P1′ or P3.

    摘要翻译： 具有至少一个C-C双键的有机化合物在至少一种催化活性化合物和至少一种溶剂的存在下用过氧化氢进行环氧化，其中使用至少一种还原剂还原包含α-氢过氧化醇的产物混合物。 该方法有利地包括至少以下步骤：（i）在至少一种催化活性化合物和至少一种溶剂的存在下使具有至少一个CC双键的有机化合物与过氧化氢反应，得到包含α 氢过氧醇 （ⅱ）分离步骤（ⅰ）中反应生成的环氧化物和从P1或P1'至少具有一个CC双键的未反应有机化合物得到产物混合物P2或P2'，其中P2包含形成的α-氢过氧醇 作为步骤（i）和P2'中的反应中的副产物大部分不含α-氢过氧醇; （iii）用至少一种还原剂处理P1和/或P2，使得α-氢过氧化醇转化为相应的二醇，得到产物混合物P1'或P3。

    Sensor system and method
    3.
    发明申请
    Sensor system and method 审中-公开
    传感器系统和方法

    公开(公告)号：US20050118064A1

    公开(公告)日：2005-06-02

    申请号：US10501742

    申请日：2002-12-23

    申请人： Anne Berg

    发明人： Anne Berg

    IPC分类号： G01N21/55 ,  G01N21/77 ,  G01N21/80 ,  G01N33/00 ,  G01N21/64

    CPC分类号： G01N21/7703 ,  G01N21/80 ,  G01N33/004 ,  G01N33/0044 ,  G01N2021/7716 ,  G01N2021/7783

    摘要： A sensor system for the detection or measurement relating to a chemical environment, comprising an optical fibre, an optical source for launching light into the optical fibre, the sensor system being adapted to let a gas, e.g. hydrogen derived from said chemical environment, diffuse into the optical fibre. The gas thereby alters the optical properties of the optical fibre. The system comprises optical signal detection and signal analysing means adapted for determining changes in the optical properties of the optical fibre due to the in-diffusion of the said gas. The signal analysis means is adapted to derive from the determined changes at least one characteristic value representing the chemical environment.

    摘要翻译： 一种用于与化学环境相关的检测或测量的传感器系统，包括光纤，用于将光发射到光纤中的光源，所述传感器系统适于使气体例如气体发生。 衍生自所述化学环境的氢扩散到光纤中。 因此气体改变了光纤的光学特性。 该系统包括光信号检测和信号分析装置，其适于由于所述气体的扩散而确定光纤的光学特性的变化。 信号分析装置适于从确定的变化中导出表示化学环境的至少一个特征值。