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    Process for the production of cardanol
    3.
    发明授权
    Process for the production of cardanol 有权
    生产腰果酚的方法

    公开(公告)号：US07825284B2

    公开(公告)日：2010-11-02

    申请号：US11911347

    申请日：2006-04-05

    申请人： Setsuo Sato ,  Wanderson Bueno de Almeida ,  Arnaldo Ferreira Filho ,  Ramiro Carielo Bueno

    发明人： Setsuo Sato ,  Wanderson Bueno de Almeida ,  Arnaldo Ferreira Filho ,  Ramiro Carielo Bueno

    IPC分类号： C07C39/10 ,  C07C39/00

    CPC分类号： C07C37/74 ,  C07C37/004 ,  C07C37/685 ,  C07C37/86 ,  C07C39/19

    摘要： A process for the production of a color-stable composition containing cardanol and cardol including (a) subjecting crude, cashew nutshell liquid to distillation to obtain a distillate: (b) reacting the distillate with boric acid to obtain a reaction mixture; and (c) subjecting the reaction mixture to distillation is provided. A method for the production of color-stable phenalkamines including (a) subjecting crude, cashew nutshell liquid to distillation to obtain a distillate; (b) reacting the distillate with boric acid to obtain a reaction mixture; (c) subjecting the reaction mixture to distillation to obtain a main fraction; and (d) reacting the main fraction with an aliphatic amine and formaldehyde to form a color-stable phenalkamine is also provided.

    摘要翻译： 一种生产含有腰果酚和卡波尔的颜色稳定组合物的方法，包括（a）使粗的腰果油液体经蒸馏得到馏出物：（b）使馏出物与硼酸反应得到反应混合物; 和（c）使反应混合物进行蒸馏。 一种生产色稳定性酚烷胺的方法，包括（a）使粗，腰果油液体蒸馏得到馏出物; （b）使馏出物与硼酸反应得到反应混合物; （c）使反应混合物蒸馏得到主要馏分; 并且（d）还提供了主要馏分与脂族胺和甲醛反应以形成色稳定的苯胺。

    Curing agents for epoxy resins
    4.
    发明申请
    Curing agents for epoxy resins 审中-公开
    环氧树脂固化剂

    公开(公告)号：US20100012888A1

    公开(公告)日：2010-01-21

    申请号：US12470130

    申请日：2009-05-21

    申请人： Setsuo Sato ,  Ramiro Carielo Bueno ,  Alexssander Shigueru Araújo ,  Arnaldo Ferreira

    发明人： Setsuo Sato ,  Ramiro Carielo Bueno ,  Alexssander Shigueru Araújo ,  Arnaldo Ferreira

    IPC分类号： C09K3/00

    CPC分类号： C08G59/56 ,  C08G59/60 ,  C08L63/00

    摘要： The present invention relates to hardener compositions for epoxy resins (epoxy resin curing agent composition) comprising a mixture of crosslinking agents comprising(a) at least one polyamide functional compound, which has at least one amide function and at least one amine function per molecule, with the proviso that the polyamide (a) is obtained by the reaction of a dimer fatty acid or an alkylester of a dimer fatty acid with at least one polyamine, and(b) at least one phenalkamine compound, which is the condensation product of an alkyl phenol, formaldehyde and one or more at least dibasic polyamine, provided that the dimer fatty acid building block used to obtain the polyamide functional compound (a) comprises monomeric fatty acid in an amount of 20-60% by weight, based on the total amount of the dimer fatty acid.

    摘要翻译： 本发明涉及包含交联剂的混合物的环氧树脂固化剂组合物（环氧树脂固化剂组合物），其包含（a）至少一种聚酰胺官能化合物，其每分子具有至少一个酰胺官能团和至少一个胺官能团， 条件是聚酰胺（a）通过二聚脂肪酸或二聚脂肪酸的烷基酯与至少一种多胺的反应获得，和（b）至少一种苯胺化合物，其为 烷基酚，甲醛和一种或多种至少二元多胺，条件是用于获得聚酰胺官能化合物（a）的二聚脂肪酸结构单元包含基于总量的20-60重量％的单体脂肪酸 二聚脂肪酸的量。

    Polyamides from dimer and trimer acid esters and methods for their preparation
    5.
    发明授权
    Polyamides from dimer and trimer acid esters and methods for their preparation 失效
    二聚体和三聚酸酯的聚酰胺及其制备方法

    公开(公告)号：US6072023A

    公开(公告)日：2000-06-06

    申请号：US119557

    申请日：1998-07-21

    申请人： Setsuo Sato ,  Ramiro Carielo Bueno ,  Wanderson Bueno De Almeida

    发明人： Setsuo Sato ,  Ramiro Carielo Bueno ,  Wanderson Bueno De Almeida

    IPC分类号： C07C231/02 ,  C07C235/10 ,  C08G69/34 ,  C08G69/02 ,  C08G69/26 ,  C08G73/00 ,  C08L79/02

    CPC分类号： C08G69/34 ,  C07C231/02 ,  C07C235/10

    摘要： Polyamides and process for their preparation comprising eitherA) epoxidizing an unsaturated or partially hydrogenated fatty acid glyceride;B) transesterifying the epoxidized glyceride with a C.sub.1-4 alkanol to obtain epoxidized fatty acid C.sub.1-4 alkyl esters;C) ring opening and dimerizing the epoxidized fatty acid C.sub.1-4 alkyl esters; andD) reacting the dimerized fatty acid C.sub.1-4 alkyl esters with a polyamine to obtain a polyamide; orA) transesterifying an unsaturated or partially hydrogenated glyceride with a C.sub.14 alkanol to obtain olefinically unsaturated fatty acid C.sub.1-4 alkyl esters;B) epoxidizing the unsaturated fatty acid C.sub.1-4 alkyl esters;C) ring opening and dimerizing the epoxidized fatty acid C.sub.1-4 alkyl esters; andD) reacting the dimerized fatty acid C.sub.1-4 alkyl esters with a polyamine to obtain a polyamide.

    摘要翻译： 聚酰胺及其制备方法，包括A）环氧化不饱和或部分氢化的脂肪酸甘油酯; B）用C 1-4链烷醇酯交换环氧化甘油酯得到环氧化脂肪酸C 1-4烷基酯; C）开环并使环氧化脂肪酸C 1-4烷基酯二聚; 和D）使二聚脂肪酸C 1-4烷基酯与多胺反应得到聚酰胺; 或A）使不饱和或部分氢化的甘油酯与C14链烷醇酯交换，得到烯属不饱和脂肪酸C 1-4烷基酯; B）环氧化不饱和脂肪酸C 1-4烷基酯; C）开环并使环氧化脂肪酸C 1-4烷基酯二聚; 和D）使二聚脂肪酸C 1-4烷基酯与多胺反应得到聚酰胺。

    Process for the preparation of polyamides
    6.
    发明授权
    Process for the preparation of polyamides 失效
    制备聚酰胺的方法

    公开(公告)号：US6011131A

    公开(公告)日：2000-01-04

    申请号：US81887

    申请日：1998-05-19

    申请人： Setsuo Sato ,  Hercules Peloggia ,  Tracy Hunt ,  Joerg Schwarzer ,  Ramiro Carielo Bueno ,  Roger A. Lovald

    发明人： Setsuo Sato ,  Hercules Peloggia ,  Tracy Hunt ,  Joerg Schwarzer ,  Ramiro Carielo Bueno ,  Roger A. Lovald

    IPC分类号： C08G69/34 ,  C08G73/10 ,  C08G69/26

    CPC分类号： C08G69/34

    摘要： Process for the preparation of polyamides comprising the steps of A) reacting a soybean oil condensate obtained from the deodorization of refined soybean oil and which contains less than 30% by weight of free and esterified oleic acid based on the total weight of free and esterified fatty acids in said condensate, with a C.sub.1-4 alkanol in the presence of a zinc oxide catalyst to convert free fatty acids and fatty acid glyceride esters to fatty acid C.sub.1-4 alkyl esters;B) removing excess C.sub.1-4 alkanol, volatile reaction by-products, water, and the zinc oxide catalyst from the resulting reaction mixture;C) heating the reaction mixture from step B) under vacuum to obtain a distillate of fatty acid C.sub.1-4 alkyl esters;D) separating the distillate from step C) into a fraction containing mostly C.sub.16-18 saturated fatty acid C.sub.1-4 alkyl esters and a second fraction containing mostly C.sub.16-18 unsaturated fatty acid C.sub.1-4 alkyl esters wherein the oleic acid C.sub.1-4 alkyl ester content is less than about 35% by weight thereof;E) dimerizing said second fraction in the presence of montmorillonite clay; andF) reacting the dimerized second fraction with a polyamine.

    摘要翻译： 制备聚酰胺的方法包括以下步骤：使得自精制大豆油的除臭得到的大豆油缩合物与游离和酯化脂肪的总重量相比含有少于30重量％的游离和酯化油酸 所述缩合物中的酸与C 1-4烷醇在氧化锌催化剂存在下将游离脂肪酸和脂肪酸甘油酯转化为脂肪酸C 1-4烷基酯; B）从所得反应混合物中除去过量的C 1-4烷醇，挥发性反应副产物，水和氧化锌催化剂; C）在真空下加热来自步骤B）的反应混合物，得到脂肪酸C 1-4烷基酯的馏出物; D）将馏出物与步骤C）分离成大部分含有C16-18饱和脂肪酸C1-4烷基酯的馏分和主要含有C16-18不饱和脂肪酸C1-4烷基酯的第二馏分，其中油酸C 1-4烷基酯含量较少 约35重量％以上; E）在蒙脱石粘土存在下将所述第二级分二聚化; 和F）使二聚第二级分与多胺反应。

    Method for producing cardanol (II)
    8.
    发明授权
    Method for producing cardanol (II) 有权
    腰果酚（II）生产方法

    公开(公告)号：US07781623B2

    公开(公告)日：2010-08-24

    申请号：US11918418

    申请日：2006-04-05

    申请人： Setsuo Sato ,  Wanderson Bueno De Almeida ,  Ramiro Carielo Bueno ,  Alexssander Shigueru Araujo

    发明人： Setsuo Sato ,  Wanderson Bueno De Almeida ,  Ramiro Carielo Bueno ,  Alexssander Shigueru Araujo

    IPC分类号： C07C29/80 ,  C07C209/84 ,  C07C209/90

    CPC分类号： C07C37/004 ,  C07C39/06

    摘要： A process for the production of a color-stable composition containing cardanol, including (a) subjecting crude, cashew nutshell liquid to distillation to obtain a distillate; (b) reacting the distillate with acetic anhydride to obtain a reaction mixture; and (c) subjecting the reaction mixture to fractional distillation is provided. A method for the production of color-stable phenalkamines, including (a) subjecting crude, cashew nutshell liquid to distillation to obtain a distillate; (b) reacting the distillate with acetic anhydride to obtain a reaction mixture; (c) subjecting the reaction mixture to fractional distillation to obtain a cardanol-containing fractional distillate; and (d) reacting the fractional distillate with an aliphatic amine and formaldehyde to form a color-stable phenalkamine is also provided.

    摘要翻译： 一种生产含有腰果酚的颜色稳定组合物的方法，包括（a）使粗的腰果壳液体经蒸馏得到馏出物; （b）使馏出物与乙酸酐反应得到反应混合物; 和（c）使反应混合物进行分馏。 一种生产颜色稳定的酚烷胺的方法，包括（a）使粗的腰果壳液体蒸馏得到馏出物; （b）使馏出物与乙酸酐反应得到反应混合物; （c）使反应混合物进行分馏以获得含有含硬脂酸的分馏馏分; 并且（d）还提供了分馏馏分与脂族胺和甲醛反应以形成颜色稳定的苯胺。

    PROCESS FOR THE PRODUCTION OF CARDANOL
    9.
    发明申请
    PROCESS FOR THE PRODUCTION OF CARDANOL 有权
    生产CARDANOL的方法

    公开(公告)号：US20090281355A1

    公开(公告)日：2009-11-12

    申请号：US11911347

    申请日：2006-04-05

    申请人： Setsuo Sato ,  Wanderson Bueno De Almeida ,  Arnaldo Ferreira Filho ,  Ramiro Carielo Bueno

    发明人： Setsuo Sato ,  Wanderson Bueno De Almeida ,  Arnaldo Ferreira Filho ,  Ramiro Carielo Bueno

    IPC分类号： C07C37/74 ,  C07C209/00

    CPC分类号： C07C37/74 ,  C07C37/004 ,  C07C37/685 ,  C07C37/86 ,  C07C39/19

    摘要： A process for the production of a color-stable composition containing cardanol and cardol including (a) subjecting crude, cashew nutshell liquid to distillation to obtain a distillate: (b) reacting the distillate with boric acid to obtain a reaction mixture; and (c) subjecting the reaction mixture to distillation is provided. A method for the production of color-stable phenalkamines including (a) subjecting crude, cashew nutshell liquid to distillation to obtain a distillate; (b) reacting the distillate with boric acid to obtain a reaction mixture; (c) subjecting the reaction mixture to distillation to obtain a main fraction; and (d) reacting the main fraction with an aliphatic amine and formaldehyde to form a color-stable phenalkamine is also provided.

    摘要翻译： 一种生产含有腰果酚和卡波尔的颜色稳定组合物的方法，包括（a）使粗的腰果油液体经蒸馏得到馏出物：（b）使馏出物与硼酸反应得到反应混合物; 和（c）使反应混合物进行蒸馏。 一种生产色稳定性酚烷胺的方法，包括（a）使粗，腰果油液体蒸馏得到馏出物; （b）使馏出物与硼酸反应得到反应混合物; （c）使反应混合物蒸馏得到主要馏分; 并且（d）还提供了主要馏分与脂族胺和甲醛反应以形成色稳定的苯胺。