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公开(公告)号：US5391474A
公开(公告)日：1995-02-21
申请号：US181267
申请日：1994-01-13
摘要： The invention provides a process for incorporating iridium into silver chloride or silver chlorobromide emulsions containing 90% or more chloride which comprises addition of an iridium salt along with or followed by the addition of bromide to the emulsion, after completion of the precipitation stage of emulsion manufacture. The invention also encompasses the formed emulsions and photographic elements comprising the emulsions.
摘要翻译： 本发明提供了一种将铱纳入含有90％或更多氯化物的氯化银或氯溴酸银乳液的方法，其中包括在乳液制备沉淀阶段完成之后，将铱盐加入或随后加入到乳液中 。 本发明还包括形成的乳液和包含乳液的照相元件。
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2.发明授权Color photographic materials and methods with stabilized silver chloride emulsions 失效彩色照相材料和方法用稳定的氯化银乳剂
公开(公告)号：US5356770A
公开(公告)日：1994-10-18
申请号：US127531
申请日：1993-09-28
申请人： Roger Lok , Jess B. Hendricks, III
发明人： Roger Lok , Jess B. Hendricks, III
CPC分类号： G03C7/3022 , G03C1/346 , G03C7/39236 , Y10S430/164
摘要： Color photographic materials and methods employ a substrate bearing a silver chloride emulsion. The silver chloride emulsion includes a diamino disulfide and a sulfinate. The diamino disulfide and the sulfinate are included in a weight ratio of from about 1:1 to about 1:20, and provide improved storage stability and reduced high temperature sensitivity during exposure.
摘要翻译： 彩色照相材料和方法采用带有氯化银乳液的基材。 氯化银乳剂包括二氨基二硫醚和亚磺酸盐。 二氨基二硫化物和亚磺酸盐以重量比约1：1至约1:20包含，并提供改善的储存稳定性和降低曝光期间的高温敏感性。
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公开(公告)号：US08637228B1
公开(公告)日：2014-01-28
申请号：US13671939
申请日：2012-11-08
CPC分类号： G03C7/3029 , G03C2001/03517 , G03C2001/7635 , G03C2007/3036
摘要： A color photographic element has a reflective support and a blue light sensitive color record, a green light sensitive color record, and a red light sensitive color record and can be used to provide color photographic prints. The element also has a non-light sensitive layer over the red light sensitive color record. This non-light sensitive layer has (1) a hydrophilic colloid in an amount of at least 200 mg/m2 to and including 2,000 mg/m2, (2) matte particles, and (3) an acrylate latex polymer having latex particles having an average size of less than 1 μm and a glass transition temperature of at least 70° C. The dry weight ratio of the acrylate latex polymer to the hydrophilic colloid is at least 0.8:1 and the dry weight ratio of the acrylate latex polymer to the total matte particles is at least 15:1.
摘要翻译： 彩色摄影元件具有反射支撑和蓝色感光彩色记录，绿色感光彩色记录和红色光敏彩色记录，可用于提供彩色照相。 该元素在红光敏感色记录上也具有非光敏层。 该非感光层具有（1）至少200mg / m 2至包括2000mg / m 2的亲水胶体，（2）无光泽颗粒，和（3）具有胶乳颗粒的丙烯酸酯胶乳聚合物，其具有 平均粒径小于1um，玻璃化转变温度至少为70℃。丙烯酸酯胶乳聚合物与亲水胶体的干重比至少为0.8:1，丙烯酸酯胶乳聚合物与干燥重量比 总磨砂颗粒至少为15：1。
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4.发明授权公开(公告)号：US06733961B1
公开(公告)日：2004-05-11
申请号：US10328493
申请日：2002-12-23
IPC分类号： G03C109
CPC分类号： G03C1/035 , G03C1/09 , G03C5/04 , G03C2001/03517 , G03C2001/03535 , G03C2001/03541 , G03C2001/093 , G03C2200/39
摘要： A method for forming a radiation-sensitive high chloride silver halide emulsion is described comprising growing cubical silver halide grains having a central portion accounting for up to 98 percent of total silver of the grains which central portion contains an iridium coordination complex dopant, and chemically sensitizing the surface of the emulsion grains at a pH of at least 5.75. Localized addition of the known in the art reciprocity-controlling iridium dopants to an internal portion of the emulsion grains and chemical finishing of such an emulsion at elevated pH conditions improves reciprocity and latent image stability of the formed high chloride emulsions.
摘要翻译： 描述了形成辐射敏感性高氯化卤化银乳剂的方法，其包括生长立方卤化银颗粒，其中心部分占中心部分含有铱配位络合物掺杂剂的颗粒的总银的98％，并且化学增感 乳液颗粒的表面在至少5.75的pH下。 将本领域已知的互易控制铱掺杂剂局部添加到乳液颗粒的内部，并且在升高的pH条件下对这种乳液进行化学处理改善了形成的高氯化物乳液的互易性和潜像稳定性。
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公开(公告)号：US07223530B2
公开(公告)日：2007-05-29
申请号：US11230343
申请日：2005-09-20
CPC分类号： G03C7/39216 , G03C7/3022 , G03C7/3041 , G03C7/346 , G03C7/383 , G03C7/3835 , G03C7/407 , G03C2001/03517 , G03C2007/3025 , G03C2200/52
摘要： The invention relates to a photographic element comprising a support and at least three color records comprising at least three light sensitive layers and at least two interlayers, wherein the light sensitive layers include cyan, magenta, or yellow dye-forming coupler, the light sensitive layers include silver halide grains comprising greater than 90% silver chloride, scavengers are included in the interlayers, the ratio of the total level of scavenger to the total level of coupler is from 0.15 to 0.50, the ratio of the total level of scavenger to the total level of silver is from 0.05 to 0.15, and the reciprocity characteristics of the silver halide grains are such that for a separation exposure of 1 microsecond and 0.4 seconds, upon development, the difference in maximum density is 10% or less and a method for processing the element comprising color developing the element for less than 30 seconds.
摘要翻译： 本发明涉及一种照相元件，其包括支撑体和至少三个彩色记录，其包含至少三个光敏层和至少两个中间层，其中光敏层包括青色，品红色或黄色染料形成成色剂，光敏层 包括大于90％氯化银的卤化银颗粒，中间层中包含清除剂，清除剂的总含量与总成色剂的比例为0.15至0.50，清除剂总量与总量之比 银的含量为0.05〜0.15，卤化银颗粒的互易特性使得对于1微秒和0.4秒的分离曝光，显影时的最大密度差为10％以下，加工方法 该元件包括彩色显影元件少于30秒。
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公开(公告)号：US06422736B1
公开(公告)日：2002-07-23
申请号：US09598573
申请日：2000-06-21
申请人： Michael G. Antoniades , Harold G. Judd , Katrin I. Parsiegla , Benjamin T. Chen , Douglas E. Singer , Donald R. Irwin , Sucheta Tandon , Jess B. Hendricks, III , Heinz E. Stapelfeldt
发明人： Michael G. Antoniades , Harold G. Judd , Katrin I. Parsiegla , Benjamin T. Chen , Douglas E. Singer , Donald R. Irwin , Sucheta Tandon , Jess B. Hendricks, III , Heinz E. Stapelfeldt
IPC分类号： B01F722
摘要： A mixer for preparing silver halide grains for photographic use has upper and lower impellers housed in a draft tube. The bottom impeller has flat blades for micromixing silver and halide reactants introduced into the bottom of the draft tube. The upper impeller has pitched blades for macromixing the bulk fluid. The impellers are spaced apart at least the distance of their diameters so that the upper and lower impellers operate independently of one another so that micromixing is independent of macromixing. A flow disrupter structurally associated with the draft tube and positioned above the top impeller prevents vortexing of the fluid during mixing. Baffles may be provided in the draft tube to discourage vortexing.
摘要翻译： 用于制备用于照相用途的卤化银颗粒的混合器具有容纳在引流管中的上部和下部叶轮。 底部叶轮具有用于将引入到引流管底部的银和卤化物反应物微混合的扁平叶片。 上部叶轮具有用于使体积流体大块混合的叶片。 叶轮至少间隔其直径的距离，使得上部和下部叶轮彼此独立地操作，使得微混合独立于大分子混合。 与引流管结构相关并位于顶部叶轮上方的流动扰流器防止混合过程中的流体涡流。 可以在引流管中设置挡板以阻止涡旋。
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公开(公告)号：US08546070B1
公开(公告)日：2013-10-01
申请号：US13651613
申请日：2012-10-15
CPC分类号： G03C7/3029 , G03C2001/03517 , G03C2007/3036 , G03C2200/35
摘要： A color photographic element has a reflective support and a blue light sensitive color record, a green light sensitive color record, and a red light sensitive color record can be used to provide color photographic prints. The element also has a non-light sensitive interlayer between the green light and red light sensitive color records. This interlayer comprises a hydrophilic colloid and an acrylic latex polymer having a glass transition temperature (Tg) of less than 0° C. The presence of this acrylic latex polymer in the interlayer reduces the formation of a cyan line defect when the color photographic print is folded or creased, such as in photobooks.
摘要翻译： 彩色照相元件具有反射支撑和蓝色感光彩色记录，绿色感光色记录和红色光敏彩色记录可用于提供彩色照相。 该元件还具有绿光和红光敏感色记录之间的非光敏中间层。 该中间层包含亲水胶体和玻璃化转变温度（Tg）小于0℃的丙烯酸胶乳聚合物。当该彩色照相印刷品为 折叠或折叠，如照相簿。
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8.发明授权公开(公告)号：US06265145B1
公开(公告)日：2001-07-24
申请号：US09475405
申请日：1999-12-30
申请人： Rajesh V. Mehta , Jerzy A. Budz , Jess B. Hendricks, III , Heinz E. Stapelfeldt , Seshadri Jagannathan , Ramesh Jagannathan
发明人： Rajesh V. Mehta , Jerzy A. Budz , Jess B. Hendricks, III , Heinz E. Stapelfeldt , Seshadri Jagannathan , Ramesh Jagannathan
IPC分类号： G03C1005
CPC分类号： G03C1/015 , G03C1/035 , G03C1/07 , G03C2001/03517 , G03C2200/01
摘要： A process for the preparation of a radiation-sensitive silver halide emulsion comprised of high chloride cubical silver halide grains containing from 0.05 to 3 mole percent iodide, based on total silver, where the iodide is incorporated in the grains in a controlled, non-uniform distribution forming a core containing at least 50 percent of total silver, an iodide free surface shell having a thickness of greater than 50 Å, and a sub-surface shell that contains a maximum iodide concentration is disclosed, the process comprising: (a) providing in a stirred reaction vessel a dispersing medium and host high chloride silver halide cubical grains comprising a speed enhancing amount of iodide, and (b) precipitating silver halide onto the host grains by introducing at least a silver salt solution into the dispersing medium at a rate such that the normalized molar addition rate, Rn, is above 3.0×10−2 min−1, Rn satisfying the formula: Rn=[Qf×Cf]/M where Qf is the volumetric rate of addition, in L/min, of silver salt solution into the reaction vessel; Cf is the concentration, in moles/L, of the silver salt solution; and M is total moles of silver halide in the host grains in the reaction vessel at the precise moment of addition of the silver salt solution. In a further aspect, this invention is directed towards a photographic recording element comprising a support and at least one light sensitive silver halide emulsion layer comprising silver halide grains prepared as described above. The advantages of the invention are generally accomplished in accordance with the discovery that when the exterior portion of profiled silver iodochloride grains are grown under specific conditions of high molar addition rates, iodochloride emulsions of enhanced sensitivity and photographic curve shape are produced, as speed can be increased while keeping fog to a low level.
摘要翻译： 一种用于制备辐射敏感的卤化银乳剂的方法，其包含基于总银含有0.05至3摩尔％碘化物的高氯化物立方体卤化银颗粒，其中碘化物以受控的，不均匀的方式掺入颗粒中 分布形成包含总银的至少50％，厚度大于Å的无碘化物表面壳和含有最大碘化物浓度的亚表面壳的芯，该方法包括：（a）提供 在搅拌的反应容器中，分散介质和包含加速量的碘化物的高氯化物卤化银立方晶粒和（b）通过将至少一种银盐溶液以一定速率引入到分散介质中而将卤化银沉淀到主体颗粒上 使得归一化的摩尔加成速率Rn高于3.0×10 -2分钟-1，Rn满足下式：其中Qf是硅的体积加入速率（L / min） 将盐溶液加入到反应容器中; Cf是银盐溶液的浓度，以摩尔/ L表示; 并且M是在银盐溶液的添加的精确时刻反应容器中的主体颗粒中卤化银的总摩尔数。 在另一方面，本发明涉及一种照相记录元件，其包括载体和包含如上所述制备的卤化银颗粒的至少一种感光卤化银乳剂层。 本发明的优点通常根据以下发现来实现：当异氰酸银碘化银颗粒的外部部分在高摩尔添加速率的特定条件下生长时，产生增强灵敏度的碘氯化物乳剂和照相曲线形状，因为速度可以 在将雾保持在低水平的同时增加。
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