Solvent exchange column and a method of use therefor
    1.
    发明授权
    Solvent exchange column and a method of use therefor 失效
    溶剂交换柱及其使用方法

    公开(公告)号:US06471865B1

    公开(公告)日:2002-10-29

    申请号:US09696041

    申请日:2000-10-25

    IPC分类号: B01D1104

    CPC分类号: B01D3/22

    摘要: The present invention provides a solvent exchange column for continuously exchanging styrene monomer with the solvent used to produce polybutadiene and a method of use therefor. The solvent exchange column includes an exchange plate support structure coupled to and supporting spaced apart exchange plates, wherein each of the exchange plates has holes located therein to allow a passage of fluid therethrough. The solvent exchange column further includes a vapor ventilation system for allowing the volatized solvent to exit the solvent exchange column.

    摘要翻译: 本发明提供了一种用于连续交换苯乙烯单体与用于生产聚丁二烯的溶剂的溶剂交换柱及其使用方法。 溶剂交换柱包括耦合到并支撑间隔开的交换板的交换板支撑结构,其中每个更换板具有位于其中的孔,以允许流体通过其中。 溶剂交换塔还包括用于使挥发的溶剂离开溶剂交换塔的蒸气通风系统。

    Method of controlling molecular weight distributions during a polymerization process
    2.
    发明授权
    Method of controlling molecular weight distributions during a polymerization process 失效
    在聚合过程中控制分子量分布的方法

    公开(公告)号:US06486271B1

    公开(公告)日:2002-11-26

    申请号:US09803598

    申请日:2001-03-09

    IPC分类号: C08F606

    CPC分类号: C08F6/001 C08F6/006 C08L25/00

    摘要: The present invention provides to overcome the deficiencies of the prior art, the present invention provides a method of producing a polymer. The method includes taking a product stream from a monovinyl aromatic polymerization system wherein the product stream comprises a polymerized monomer and a monomer. The product stream is introduced into an up-flow heat exchanger in a presence of an initiator, such as a peroxide, that affects a polymerization of the monomer in the up-flow heat exchanger. The initiator may include a low-temperature initiator and a high-temperature initiator where a ratio of the high-temperature initiator to the low-temperature initiator can range from about 0:600 to about 50:600.

    摘要翻译: 本发明提供克服现有技术的不足之处,本发明提供聚合物的制造方法。 该方法包括从单乙烯基芳族聚合体系中获取产物流,其中产物流包含聚合的单体和单体。 在引发剂如过氧化物的存在下,将产物流引入上流式热交换器,其影响单体在上流式热交换器中的聚合。 引发剂可以包括低温引发剂和高温引发剂,其中高温引发剂与低温引发剂的比率可以在约0:600至约50:600的范围内。

    Process for recovering polymers from commingled materials
    3.
    发明授权
    Process for recovering polymers from commingled materials 失效
    从混合材料中回收聚合物的方法

    公开(公告)号:US5994417A

    公开(公告)日:1999-11-30

    申请号:US869050

    申请日:1997-06-04

    IPC分类号: C08J11/08 C08J11/04

    摘要: A process for recovering polymers from commingled materials is disclosed. In general, the process includes first contacting the commingled materials with a solvent which selectively dissolves the polymer to form a solvent and polymer solution. The solvent and polymer solution is then contacted with an anti-solvent into which the solvent is soluble but into which the polymer is insoluble. When the solvent and polymer solution is contacted with the anti-solvent, the anti-solvent causes the polymer to nucleate and precipitate from the solution. In one embodiment, it has been found that the process of the present invention is particularly well adapted to recovering nylon from commingled materials such as carpet waste.

    摘要翻译: 公开了从混合材料中回收聚合物的方法。 通常,该方法包括首先使混合的材料与选择性溶解聚合物形成溶剂和聚合物溶液的溶剂接触。 然后将溶剂和聚合物溶液与其中溶剂可溶的抗溶剂接触,但聚合物不溶于其中。 当溶剂和聚合物溶液与反溶剂接触时,反溶剂使聚合物成核并从溶液中沉淀出来。 在一个实施方案中,已经发现本发明的方法特别适用于从混合材料如地毯废料中回收尼龙。

    Method for removing volatiles from a block copolymer
    4.
    发明授权
    Method for removing volatiles from a block copolymer 失效
    从嵌段共聚物中除去挥发物的方法

    公开(公告)号:US06962960B1

    公开(公告)日:2005-11-08

    申请号:US10044759

    申请日:2002-01-09

    IPC分类号: C08F2/06 C08F6/00

    CPC分类号: C08F6/003 C08L53/02

    摘要: A method and apparatus are disclosed for purifying copolymer compounds having monovinyl aromatic blocks and conjugated diene blocks by reducing the residual monomer content of the finished polymer. The method and apparatus includes a combination of heat exchangers and devolatilizers used in conjunction with a copolymerization reactor system.

    摘要翻译: 公开了通过降低成品聚合物的残留单体含量来纯化具有单乙烯基芳族嵌段和共轭二烯嵌段的共聚物化合物的方法和装置。 该方法和装置包括与共聚反应器系统结合使用的热交换器和脱挥发分剂的组合。

    Apparatus and method for removal of volatiles from a mass processable polymer
    5.
    发明授权
    Apparatus and method for removal of volatiles from a mass processable polymer 有权
    从可加脂聚合物中除去挥发物的装置和方法

    公开(公告)号:US07087139B1

    公开(公告)日:2006-08-08

    申请号:US10226413

    申请日:2002-08-23

    IPC分类号: B01D1/00 C08F6/10

    CPC分类号: B01D3/06 C08F6/005 Y10S159/10

    摘要: The present invention provides an apparatus and method of reducing volatiles in a mass processable polymer. The apparatus includes a multi-chambered devolatilizer having first and second collectors contained therein. In one embodiment, the invention provides a method that includes passing the mass processable polymer stream from a polymerization process to a first devolatilizer. The method continues by passing the polymer stream from the first devolatilizer to the multi-chambered devolatilizer. The apparatus and method allows for the production of a polymer having less than 100 ppm of volatiles.

    摘要翻译: 本发明提供一种在可加脂聚合物中还原挥发物的装置和方法。 该设备包括多室分散器,其中包含第一和第二收集器。 在一个实施方案中,本发明提供了一种方法,其包括将可加工聚合物流从聚合过程传递到第一脱挥发物。 该方法通过使聚合物流从第一脱挥发物流入多室脱挥发剂而继续。 该装置和方法允许生产具有小于100ppm挥发物的聚合物。