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    Water miscible solvent based process for purifying a bisphosphate
    4.
    发明授权
    Water miscible solvent based process for purifying a bisphosphate 有权
    用于纯化二磷酸的水混溶溶剂基方法

    公开(公告)号：US08299149B2

    公开(公告)日：2012-10-30

    申请号：US13133346

    申请日：2009-12-21

    申请人： Joseph Zilberman ,  Dorit Canfi ,  Andrew Gregor ,  Andrew Piotrowski

    发明人： Joseph Zilberman ,  Dorit Canfi ,  Andrew Gregor ,  Andrew Piotrowski

    IPC分类号： C08K5/523

    CPC分类号： C07F9/12 ,  C08K5/523 ,  C09K21/12

    摘要： There is provided herein a process for purifying bisphosphate comprising solvating a molten bisphosphate in a mixture of water and water miscible solvent; cooling the solution over a period and to a temperature that provides for crystallization of solid product; increasing the pH of the solution prior to, and/or during, and/or after the initiation of crystallization, and/or after crystallization, by the addition of a base; and after crystallization is complete, separating solid product from the solution; washing the separated solid product in the same and/or different mixture of water and water miscible solvent; and, washing the solid product which has been washed in the mixture with water.

    摘要翻译： 本文提供了一种纯化二磷酸盐的方法，其包括在水和水混溶性溶剂的混合物中溶解熔融的二磷酸盐; 在一段时间内将溶液冷却至提供固体产物结晶的温度; 在结晶开始之前和/或期间和/或之后，和/或在结晶后，通过加入碱来增加溶液的pH值; 结晶完成后，将固体产物与溶液分离; 在与水和水混溶的溶剂的相同和/或不同混合物中洗涤分离的固体产物; 并且用水洗涤已经在混合物中洗涤的固体产物。

    WATER MISCIBLE SOLVENT BASED PROCESS FOR PURIFYING A BISPHOSPHATE
    5.
    发明申请
    WATER MISCIBLE SOLVENT BASED PROCESS FOR PURIFYING A BISPHOSPHATE 有权
    用于净化双磷酸盐的基于水的混合溶剂的方法

    公开(公告)号：US20120022193A1

    公开(公告)日：2012-01-26

    申请号：US13133346

    申请日：2009-12-21

    申请人： Joseph Zilberman ,  Dorit Canfi ,  Andrew Gregor ,  Andrew Piotrowski

    发明人： Joseph Zilberman ,  Dorit Canfi ,  Andrew Gregor ,  Andrew Piotrowski

    IPC分类号： C08K5/521 ,  C07F9/09

    CPC分类号： C07F9/12 ,  C08K5/523 ,  C09K21/12

    摘要： There is provided herein a process for purifying bisphosphate comprising solvating a molten bisphosphate in a mixture of water and water miscible solvent; cooling the solution over a period and to a temperature that provides for crystallization of solid product; increasing the pH of the solution prior to, and/or during, and/or after the initiation of crystallization, and/or after crystallization, by the addition of a base; and after crystallization is complete, separating solid product from the solution; washing the separated solid product in the same and/or different mixture of water and water miscible solvent; and, washing the solid product which has been washed in the mixture with water.

    摘要翻译： 本文提供了一种纯化二磷酸盐的方法，其包括在水和水混溶性溶剂的混合物中溶解熔融的二磷酸盐; 在一段时间内将溶液冷却至提供固体产物结晶的温度; 在结晶开始之前和/或期间和/或之后，和/或在结晶后，通过加入碱来增加溶液的pH值; 结晶完成后，将固体产物与溶液分离; 在与水和水混溶的溶剂的相同和/或不同混合物中洗涤分离的固体产物; 并且用水洗涤已经在混合物中洗涤的固体产物。