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公开(公告)号：US4771032A
公开(公告)日：1988-09-13
申请号：US760781
申请日：1985-07-31
申请人： Jun Yamaguchi , Toshiharu Tanaka , Toshimasa Usami , Sadao Ishige
发明人： Jun Yamaguchi , Toshiharu Tanaka , Toshimasa Usami , Sadao Ishige
CPC分类号： G03C1/52
摘要： A heat-sensitive recording material and a recording method are disclosed, wherein the heat-sensitive recording material comprises a support having formed thereon plural heat-coloring elements each comprising a diazo compound and a coupling component capable of causing heat-coloring, the heat-coloring elements coloring in two or more different hues, and the coloring property in each heat-coloring element being capable of being stopped by the action of different radiations, and the recording method comprises first heat-coloring a heat-coloring element of the heat-sensitive recording material, stopping the heat-coloring property of the uncolored portions of the first heat-coloring element by radiation, and then heat-coloring another heat-coloring element; wherein the recording method comprises applying two or more heat-coloring procedures and one or more irradiations of radiation to form recorded images composed of two or more colors on the same sheet.
摘要翻译： 公开了一种热敏记录材料和记录方法，其中热敏记录材料包括其上形成有多个加热着色元件的支撑体，每个加热着色元件均包含重氮化合物和能够引起热着色的偶联成分， 着色元件以两种或更多种不同的色调着色，并且每个加热着色元件中的着色性能能够通过不同辐射的作用而停止，并且记录方法包括首先对散热元件的热着色元件进行加热着色， 通过辐射来停止第一加热着色元件的未着色部分的着色性，然后对另一个热着色元件进行加热着色; 其中所述记录方法包括施加两个或多个加热着色步骤和一次或多次辐射照射，以在同一张纸上形成由两种或更多种颜色组成的记录图像。
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2.发明授权Black color heat-sensitive diazo microcapsule recording material with benzoylacetic amide coupler 失效黑色热敏重氮微胶囊记录材料与苯甲酰乙酰胺偶合剂
公开(公告)号：US4842979A
公开(公告)日：1989-06-27
申请号：US129350
申请日：1987-11-30
IPC分类号： B41M5/323 , B41M5/28 , B41M5/30 , B41M5/337 , C07C235/80 , G03C1/00 , G03C1/58 , G03C1/60 , G03C1/61 , G03C5/18 , G03C7/36
CPC分类号： B41M5/3375 , C07C235/80 , G03C1/002 , G03C1/58 , G03C5/18 , G03C7/362
摘要： A heat-sensitive recording material comprising a support having provided thereon a heat-sensitive layer containing microcapsules containing at least one diazonium salt capable of azo-coupling with 2-hydroxy-3-naphthoic acid anilide to develop a blue color, a 2-hydroxy-3-naphthoic acid amide derivative, a benzoylacetic amide derivative represented by the following formula and a basic substance: ##STR1## wherein X represents a hydrogen atom, a halogen atom, a lower alkyl group or an alkoxy, aralkyloxy, phenoxy or acylamino group having up to 18 carbon atoms; Y represents an alkyl or aralkyl group having from 7 to 18 carbon atoms, an alkoxy, aralkyloxy, phenoxy, naphthyloxy, alkylthio, aralkylthio or phenylthio group having from 6 to 18 carbon atoms, a naphthylthio group, a sulfonyloxy group, a sulfamoyl gorup, a ureido group, a thioureido group or an acylamino group; X' and Y' each represents a hydrogen atom, a halogen atom, a lower alkyl group or a lower alkoxy group; and Y and Y' may combine to form a substituted or unsubstituted benzene ring. The material has excellent preservability before heat recording, provides a high color density upon heat recording, and develops a black color fixable with light.
摘要翻译： 一种热敏记录材料，其包括在其上设置有包含含有至少一种能够与2-羟基-3-萘甲酸苯胺偶氮偶联的重氮盐以形成蓝色的微胶囊的热敏层的载体，2-羟基 -3-萘甲酸酰胺衍生物，下式表示的苯甲酰基乙酰胺衍生物和碱性物质：其中X表示氢原子，卤素原子，低级烷基或烷氧基，芳烷氧基，苯氧基或酰氨基 具有多达18个碳原子; Y表示碳原子数为7〜18的烷基或芳烷基，碳原子数6〜18的烷氧基，芳烷氧基，苯氧基，萘氧基，烷硫基，芳烷硫基或苯硫基，萘硫基，磺酰氧基，氨磺酰基， 脲基，硫脲基或酰氨基; X'和Y'各自表示氢原子，卤素原子，低级烷基或低级烷氧基; 并且Y和Y'可以结合形成取代或未取代的苯环。 该材料在热记录之前具有优异的保存性，在加热记录时提供高的色彩密度，并且可以发展出可用光固定的黑色。
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3.发明授权
公开(公告)号：US4865939A
公开(公告)日：1989-09-12
申请号：US220336
申请日：1988-07-13
CPC分类号： B41M5/30
摘要： A process for the production of a heat-sensitive recording material in which a color former causing a color formation reaction and a developer forming color on reaction with the color former are incorporated in a heat-sensitive recording layer, and at least one of the color former and the developer is contained in microcapsules having walls which are impermeable to both the color former and the developer at ordinary temperature but which becomes permeable to at least one of the color former and the developer on heating, where the heat-sensitive recording layer is coated on a support which is then subjected to surface treatment by passing it through a pressure applying apparatus comprising a metallic roll and an elastic roll in such a manner that the heat-sensitive recording layer is in contact with the metallic roll.
摘要翻译： 一种用于生产热敏记录材料的方法，其中将导致成色反应的成色剂和与成色剂反应的显色剂形成在热敏记录层中，并且至少一种颜色 前者和显影剂包含在具有在常温下对成色剂和显色剂不渗透的壁的微胶囊中，但是对于加热时的至少一种着色剂和显色剂而言，其中热敏记录层是 涂覆在支撑体上，然后通过使其通过包括金属辊和弹性辊的压力施加装置进行表面处理，使得热敏记录层与金属辊接触。
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公开(公告)号：US4783439A
公开(公告)日：1988-11-08
申请号：US786567
申请日：1985-10-11
CPC分类号： B41M5/3375 , B41M2205/04 , B41M5/1655 , B41M5/287 , B41M5/323 , B41M5/3275 , B41M5/3335 , Y10S428/913 , Y10T428/273 , Y10T428/277
摘要： A heat-sensitive recording material is disclosed. The material comprises a support having provided on the same surface thereof microcapsules containing a basic colorless dye and an organic solvent, and a developer capable of reacting with the basic colorless dye to develop a color, the capsule walls of said microcapsules being impermeable to either of the basic colorless dye and the developer at room temperature but becoming permeable to the colorless dye and/or the developer upon application of heat. The organic solvent is a compound containing at least two benzene rings in the molecule thereof with a total number of at least one hetero atom selected from nitrogen, sulfur, oxygen and phosphorus atoms, if any, being less than 1/10 a total number of carbon atoms of the organic solvent. The material is excellent in preservability before and after recording and is excellent in heat-developability.
摘要翻译： 公开了一种热敏记录材料。 该材料包括在其相同表面上提供含有碱性无色染料和有机溶剂的微胶囊的支持体和能够与碱性无色染料反应以显色的显影剂，所述微胶囊的胶囊壁不可渗透到 碱性无色染料和显色剂，但在加热时变得透明无色染料和/或显色剂。 有机溶剂是在其分子中含有至少两个苯环的化合物，其总数为至少一个选自氮，硫，氧和磷原子的杂原子（如果有的话）小于总数的1/10 有机溶剂的碳原子。 该材料在记录之前和之后的保存性优异，并且热显影性优异。
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公开(公告)号：US4742043A
公开(公告)日：1988-05-03
申请号：US824346
申请日：1986-01-23
申请人： Toshiharu Tanaka , Toshimasa Usami
发明人： Toshiharu Tanaka , Toshimasa Usami
CPC分类号： B41M5/287 , B41M5/30 , Y10T428/2985 , Y10T428/2987
摘要： A heat-sensitive recording material is disclosed, comprising a support and heat-sensitive recording layer on the support, said layer containing (1) microcapsules containing a basic dye precursor and an organic solvent as the core thereof and (2) a developer capable of forming color on reacting with the basic dye precursor, wherein said microcapsules are produced by the use of a wall-forming substance comprising xylylene diisocyanate or an adduct thereof such that the microcapsule walls are impermeable to both the basic dye precursor and developer at room temperature, but at a temperature of a thermal head during a recording process, become permeable to at least one of the basic dye precursor and developer, thereby permitting formation of a colored image as a result of the reaction between the basic dye precursor and the developer. This material can retain its excellent recording ability for a long period of time; that is, it possesses excellent storage stability, and moreover can produce a recorded image of high storage stability.
摘要翻译： 公开了一种热敏记录材料，其包含载体上的载体和热敏记录层，所述层含有（1）含有碱性染料前体和有机溶剂作为其核心的微胶囊，和（2）能够 在与所述碱性染料前体反应时形成颜色，其中所述微胶囊通过使用包含亚二甲苯基二异氰酸酯或其加合物的壁形成物质来制备，使得所述微胶囊壁在室温下对于所述碱性染料前体和显色剂都是不可渗透的， 但是在记录过程中在热敏头的温度下，对于至少一种碱性染料前体和显影剂变得可渗透，从而由于碱性染料前体和显影剂之间的反应而形成着色图像。 该材料可长期保持良好的记录能力; 即具有良好的储存稳定性，并且能够产生高储存稳定性的记录图像。
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公开(公告)号：US4722921A
公开(公告)日：1988-02-02
申请号：US855058
申请日：1986-04-23
CPC分类号： B41M5/287 , Y10T428/25 , Y10T428/254 , Y10T428/256 , Y10T428/257 , Y10T428/258 , Y10T428/259
摘要： A heat-sensitive recording material is disclosed, comprising a support having provided thereon a heat-sensitive recording layer containing microcapsules containing a color former and an organic solvent as core materials and a color developer exterior thereto, the wall of said microcapsules being impermeable to both of the color former and the color developer at room temperature but becoming permeable to at least one of the color former and color developer upon the application of heat, wherein the heat-sensitive recording layer further contains a pigment having an average particle size greater than that of the microcapsules. The material exhibits improved handling and running properties.
摘要翻译： 本发明公开了一种热敏记录材料，其包括：载体，其上设有包含含有成色剂和有机溶剂作为核心材料的微胶囊的热敏记录层和外部的彩色显影剂，所述微胶囊的壁不可渗透 的着色剂和彩色显影剂，但是在施加热量时对成色剂和彩色显影剂中的至少一种变得透气，其中热敏记录层还含有平均粒径大于其的平均粒径的颜料。 的微胶囊。 该材料表现出改善的处理和运行性能。
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公开(公告)号：US4644376A
公开(公告)日：1987-02-17
申请号：US729722
申请日：1985-05-02
申请人： Toshimasa Usami , Toshiharu Tanaka
发明人： Toshimasa Usami , Toshiharu Tanaka
CPC分类号： B41M5/287 , Y10S430/165
摘要： A heat-sensitive recording material is described, comprising a support having thereon a layer containing microcapsules containing at least a first coloring component capable of undergoing a coloring reaction and an organic solvent in a core, and at least a second component causing said coloring reaction with said first coloring component in the microcapsules, wherein two or more kinds of microcapsules comprising respective microcapsule walls having different glass transition points constitute said microcapsules.
摘要翻译： 描述了一种热敏记录材料，其包括其上具有包含至少含有能够进行着色反应的第一着色组分和核心中的有机溶剂的微胶囊的层，以及至少第二组分，其引起所述着色反应与 所述微胶囊中的所述第一着色组分，其中包含具有不同玻璃化转变点的各自微胶囊壁的两种或更多种微胶囊构成所述微胶囊。
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公开(公告)号：US4686547A
公开(公告)日：1987-08-11
申请号：US871350
申请日：1986-06-06
CPC分类号： G03C1/52
摘要： A heat-sensitive recording material comprising a support having provided thereon a heat-sensitive recording layer, the heat-sensitive recording layer containing a diazo compound encapsulated in microcapsules and a component capable of undergoing a color forming reaction with said diazo compound, wherein a protective coating layer containing as a binder a modified polyvinyl alcohol containing silicon atoms, and at least one of colloidal silica and amorphous silica is applied on the surface of the heat-sensitive recording layer.
摘要翻译： 一种热敏记录材料，包括在其上设置有热敏记录层的支撑体，所述热敏记录层含有包封在微胶囊中的重氮化合物和能够与所述重氮化合物进行着色反应的成分， 包含作为粘合剂的包含硅原子的改性聚乙烯醇的涂层，并且将胶体二氧化硅和无定形二氧化硅中的至少一种涂布在热敏记录层的表面上。
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公开(公告)号：US4650740A
公开(公告)日：1987-03-17
申请号：US650143
申请日：1984-09-13
CPC分类号： G03C1/002 , G03C1/52 , Y10S430/165
摘要： A heat-sensitive recording material is described, comprising a support having provided thereon a recording layer comprising a binder containing a diazonium compound and a coupling component, said diazonium compound being a diazonium salt represented by formula (I)ArN.sub.2.sup.+ X.sup.- (I)wherein Ar represents a substituted or unsubstituted aromatic moiety; and X.sup.- represents an acid anion containing an alkyl group having three or more fluorine atoms.
摘要翻译： 描述了一种热敏记录材料，其包括其上设置有包含含有重氮化合物和偶联组分的粘合剂的记录层的载体，所述重氮化合物是由式（I）表示的重氮盐ArN2 + X-（I） 其中Ar表示取代或未取代的芳族部分; X表示含有具有3个以上氟原子的烷基的酸性阴离子。
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公开(公告)号：US4529681A
公开(公告)日：1985-07-16
申请号：US552892
申请日：1983-11-17
IPC分类号： B41M5/28 , B41M5/30 , B41M5/323 , B41M5/333 , B41M5/337 , G03F7/00 , G03F7/004 , G03F7/26 , H01L21/027 , G03C1/48
CPC分类号： G03F7/002 , B41M5/287 , H01L21/0276 , B41M5/30 , B41M5/323 , B41M5/333 , B41M5/3372 , B41M5/3375
摘要： A light- and heat-sensitive recording material is disclosed. The material include microcapsule in which are encapsulated a particular combination comprised of a vinyl compound, a photopolymerization initiator, and a color forming component being capable of undergoing a color reaction with another color forming component to cause color formation. These coloring components are provided on the same side of a support.
摘要翻译： 公开了一种光和热敏记录材料。 该材料包括微胶囊，其中包含由乙烯基化合物，光聚合引发剂和可与其它成色组分进行着色反应的成色组分组成的特定组合，以形成颜色。 这些着色部件设置在支撑体的同一侧。
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