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    Polyarylether containing N-substituted imide groups and process for producing the same
    1.
    发明授权
    Polyarylether containing N-substituted imide groups and process for producing the same 失效
    含有N-取代的酰亚胺基团的聚芳醚基及其制备方法

    公开(公告)号：US6018055A

    公开(公告)日：2000-01-25

    申请号：US892707

    申请日：1997-07-15

    申请人： Kil-Yeong Choi ,  Dong-Hack Suh ,  Young-Taik Hong ,  Eun-Young Chung

    发明人： Kil-Yeong Choi ,  Dong-Hack Suh ,  Young-Taik Hong ,  Eun-Young Chung

    IPC分类号： C07D487/04 ,  C08G65/40 ,  C08G73/06 ,  C07D487/02

    CPC分类号： C07D487/04 ,  C08G73/0672

    摘要： A polyarylether of the formula (VIII) ##STR1## wherein wherein Z' is 1-3 optionally substituted rings selected from the group consisting of an aromatic ring, a hetero aromatic ring or an aliphatic ring.A is --R.sub.1 --Z--Y in which R.sub.1 is H, C.sub.1 -C.sub.30 -alkyl or -aralkyl or phenyl, Z is a direct bond or CH.sub.2, S, O or NH, Y is CH.sub.3, OR.sub.3, SR.sub.3, NHR.sub.3, N(R.sub.3).sub.2, COOR.sub.3, COOM, SO.sub.3 R.sub.3 or SO.sub.3 M in which R.sub.3 is C.sub.1 -C.sub.30 alkyl and M is alkali metal,produced from 3,6-dihalogen- or -dintro-1,2,4,5-diimide having an N,N-substituent and which is suitable for use as a monomer for high temperature structural and functional polymers, and a process for producing the same are disclosed.

    摘要翻译： 式（VIII）的聚芳醚，其中Z'为1-3个选自芳香环，杂芳环或脂族环的任选取代的环。 A是-R1-ZY，其中R1是H，C1-C30 - 烷基或 - 烷基或苯基，Z是直接键或CH2，S，O或NH，Y是CH3，OR3，SR3，NHR3，N ）2，CO 3，COOM，SO 3 R 3或SO 3 M，其中R 3为C 1 -C 30烷基且M为碱金属，由具有N，N的3,6-二卤代 - 或二苯并1,2,4,5-二酰亚胺 并且其适合用作高温结构和功能性聚合物的单体，并且公开了其制备方法。

    Cyclohexane-1,2,4,5-diimide derivative and process for preparing the same
    2.
    发明授权
    Cyclohexane-1,2,4,5-diimide derivative and process for preparing the same 失效
    环己烷-1,4,5-二酰亚胺衍生物及其制备方法

    公开(公告)号：US5919942A

    公开(公告)日：1999-07-06

    申请号：US879977

    申请日：1997-06-20

    申请人： Kil-Yeong Choi ,  Dong-Hack Suh ,  Young-Taik Hong ,  Sang-Hyun Park

    发明人： Kil-Yeong Choi ,  Dong-Hack Suh ,  Young-Taik Hong ,  Sang-Hyun Park

    IPC分类号： C07D487/04 ,  C08G73/10

    CPC分类号： C07D487/04 ,  C08G73/10

    摘要： The disclosure describes a cyclohexane-1,2,4,5-diimide derivative which can be used for the production of colorless transparent polymer and novel engineering plastics having good processability and solubility with an excellent physical property, and a process for preparing the same which comprises reacting a bicyclooctene-1,2,4,5-tetracarboxylic anhydride with alkylamine and aniline derivative and then oxidizing the resulting product with ozone, potassium permanganate, ruthenium chloride hydroxide and aqeous hydrogen peroxide under non-basic condition to convert double bond to dicarboxylic acid or dialdehyde without destroying the imide group.

    摘要翻译： 本公开内容描述了可用于生产无色透明聚合物的环己烷-1,2,4,5-二酰亚胺衍生物和具有优异物理性能的具有良好加工性和溶解性的新型工程塑料及其制备方法， 包括使双环辛烯-1,2,4,5-四羧酸酐与烷基胺和苯胺衍生物反应，然后在非碱性条件下用臭氧，高锰酸钾，氯化钌和过氧化氢氧化所得产物，以将双键转化成二羧酸 酸或二醛，而不会破坏酰亚胺基团。

    Process for preparing polyamideimide resins by direct polymerization
    3.
    发明授权
    Process for preparing polyamideimide resins by direct polymerization 失效
    通过直接聚合制备聚酰胺酰亚胺树脂的方法

    公开(公告)号：US5955568A

    公开(公告)日：1999-09-21

    申请号：US956923

    申请日：1997-10-23

    申请人： Kil-Yeong Choi ,  Dong-Hack Suh ,  Mi-Hie Yi ,  Young-Taik Hong ,  Moon-Young Jin

    发明人： Kil-Yeong Choi ,  Dong-Hack Suh ,  Mi-Hie Yi ,  Young-Taik Hong ,  Moon-Young Jin

    IPC分类号： C08G73/14 ,  C08G69/28

    CPC分类号： C08G73/14

    摘要： The disclosure describes a process for preparing a polyamideimide resin having high molecular weight in a simple manner wherein major problems of the prior processes such as low heat resistance and low melt flowability are improved. The process comprises condensation of an aromatic tricarboxylic acid anhydride and an aromatic diamine in a polar solvent, subjecting the resulting diimidedicarboxylic acid to acyl halogenating agent treatment to give an intermediate having good reactivity at low temperature, and then subjecting the latter to direct polymerization by using diamine as a nucleophilic agent to give a polyamideimide resin having high molecular weight. The polyamideimide resin prepared by the present invention can be used as major heat resistant structural material in advanced industries and as paint, sheet, adhesives, sliding material, fiber and film having heat resistance.

    摘要翻译： 本公开内容描述了以简单的方式制备具有高分子量的聚酰胺酰亚胺树脂的方法，其中诸如低耐热性和低熔融流动性的现有方法的主要问题得到改善。 该方法包括在极性溶剂中将芳族三羧酸酐和芳族二胺缩合，将所得二酰亚胺二羧酸进行酰卤处理，得到在低温下具有良好反应性的中间体，然后使用后者通过使用 二胺作为亲核剂，得到具有高分子量的聚酰胺酰亚胺树脂。 本发明制备的聚酰胺酰亚胺树脂可用作先进工业中的主要耐热结构材料，可用作具有耐热性的油漆，片材，粘合剂，滑动材料，纤维和薄膜。

    Process for preparing polyamideimide resins having high molecular weight
    4.
    发明授权
    Process for preparing polyamideimide resins having high molecular weight 失效
    制备高分子量聚酰胺酰亚胺树脂的方法

    公开(公告)号：US5532334A

    公开(公告)日：1996-07-02

    申请号：US339391

    申请日：1994-11-14

    申请人： Kil-Yeong Choi ,  Dong-Hack Suh ,  Mi-Hie Yi ,  Young-Taik Hong ,  Jong-Chan Won

    发明人： Kil-Yeong Choi ,  Dong-Hack Suh ,  Mi-Hie Yi ,  Young-Taik Hong ,  Jong-Chan Won

    IPC分类号： C08G73/14 ,  H01B3/30 ,  C08G69/26

    CPC分类号： C08G73/14 ,  H01B3/303

    摘要： A process for preparing polyamideimide resins having high molecular weights as described wherein major problems of prior art processes such as low heat resistance and low melt flowability are improved. Polyamideimide resins having an intrinsic viscosity of 0.4 to 1.50 dl/g as measured on a solution of dimethylacetamide as a solvent at a concentration of 0.5 g/dl at 30.degree. C., are prepared by reacting an aromatic tricarboxylic acid anhydride with an aromatic diamine in N-methyl pyrrolidone solvent in the presence of a first catalyst selected from a group consisting of thionyl chloride, p-toluenesulphonly chloride, sulfuryl chloride, cyanuric chloride and phosphorus trichloride at a temperature of 50.degree. C. to 130.degree. C. over a period of 1 to 5 hours and further reacting the resultant reaction mixture in the presence of a second catalyst which is a compound of the formula (RO).sub.3 P wherein R is an aliphatic or aromatic substituent, or a compound which is phosphoric acid, pyrophosphoric acid, phosphorous pentaoxide or phosphorous pentachloride as a second catalyst at a temperature of 50.degree. C. to 130.degree. C. over a period of 1 to 5 hours.

    摘要翻译： 制备如上所述的具有高分子量的聚酰胺酰亚胺树脂的方法，其中提高了诸如低耐热性和低熔融流动性的现有技术方法的主要问题。 通过在30℃下以0.5g / dl的浓度作为溶剂的二甲基乙酰胺溶液测定的特性粘度为0.4至1.50dl / g的聚酰胺酰亚胺树脂通过芳族三羧酸酐与芳族二胺 在N-甲基吡咯烷酮溶剂中，在50℃至130℃的温度下，在选自亚硫酰氯，对甲苯磺酰氯，磺酰氯，氰尿酰氯和三氯化磷的第一催化剂存在下，在 时间为1至5小时，并且在第二催化剂存在下进一步反应，所述第二催化剂是式（RO）3P的化合物，其中R是脂族或芳族取代基，或者是磷酸化合物，焦磷酸 ，五氧化二磷或五氯化磷作为第二催化剂，温度为50〜130℃，时间为1〜5小时。

    Polyamide-imide having head-to-tail backbone
    5.
    发明授权
    Polyamide-imide having head-to-tail backbone 失效
    具有头对头骨架的聚酰胺酰亚胺

    公开(公告)号：US06433184B1

    公开(公告)日：2002-08-13

    申请号：US09605026

    申请日：2000-06-28

    申请人： Kil-Yeong Choi ,  Jae Heung Lee ,  Young-Taik Hong ,  Moon Young Jin ,  Kyoung-Su Choi ,  Ho-Jin Park

    发明人： Kil-Yeong Choi ,  Jae Heung Lee ,  Young-Taik Hong ,  Moon Young Jin ,  Kyoung-Su Choi ,  Ho-Jin Park

    IPC分类号： C07D20948

    CPC分类号： C08G73/14

    摘要： The present invention relates to polyamide-imides having head-to-tail backbone and more particularly, to polyamide-imimdes having head-to-tail ragularity to provide excellent heat and chemical resistance, physical and mechanical properties, processability, and gas permeability and selectivity. The polyamide-imides represented in the following formula (1) are obtained by direct polymerization, in the presence of dehydrating catalyst, of alone or as a mixture of 2 or above of monomers prepared by condensation of an amine compound having a nitro group with a carboxylic acid anhydride,

    摘要翻译： 本发明涉及具有头 - 尾主链的聚酰胺 - 酰亚胺，更具体地说，涉及具有头对尾的粗糙度以提供优异的耐热和耐化学性，物理和机械性能，可加工性和气体渗透性和选择性的聚酰胺酰亚胺 。 在下式（1）中表示的聚酰胺 - 酰亚胺通过在脱水催化剂的存在下，单独或作为2种以上的单体的混合物直接聚合而获得，所述单体通过具有硝基的胺化合物与 羧酸酐，

    Soluble polyimide resin having a dialkyl substituent for a liquid crystal alignment layer, the monomers and manufacturing methods thereof
    8.
    发明授权
    Soluble polyimide resin having a dialkyl substituent for a liquid crystal alignment layer, the monomers and manufacturing methods thereof 失效
    具有用于液晶取向层的二烷基取代基的可溶性聚酰亚胺树脂，其单体及其制造方法

    公开(公告)号：US06162893A

    公开(公告)日：2000-12-19

    申请号：US138377

    申请日：1998-08-24

    申请人： Kil-Yeong Choi ,  Mi-Hie Yi ,  Moon-Young Jin ,  Jin-Tae Jung ,  Jae-Geun Park ,  Dae-Woo Ihm

    发明人： Kil-Yeong Choi ,  Mi-Hie Yi ,  Moon-Young Jin ,  Jin-Tae Jung ,  Jae-Geun Park ,  Dae-Woo Ihm

    IPC分类号： C08G73/10 ,  G02F1/1337 ,  A61K38/17

    CPC分类号： C08G73/1078 ,  C08G73/1039 ,  C08G73/1067 ,  C08G73/1071 ,  G02F1/133723

    摘要： The invention herein relates to a soluble polyimide resin having a dialkyl substituent for a liquid alignment layer, wherein aliphatic tetracarboxylic dianhydride and aromatic diamine having a dialkyl substituent are used to yield said soluble polyimide resin which has superior heat-resistance, solubility, transparency, and liquid crystal alignment capacity. According to the present invention, the soluble polyimide polymer having a dialkyl substituent, for a liquid crystal alignment layer, comprising the following a repetitive unit of formula 1: ##STR1## Consequently, the polyimide resin under the present invention not only has superior heat-resistance but also excellent solubility and transparency, which could be applicable as a liquid crystal alignment layer for the TFT-LCD requiring a low temperature processing. Further, the invention has the effects of providing a polyimide resin with superior physical property for heat-resistance structural material, and the monomer therein, in addition to the manufacturing methods thereof.

    摘要翻译： 本发明涉及具有用于液体取向层的二烷基取代基的可溶性聚酰亚胺树脂，其中使用具有二烷基取代基的脂族四羧酸二酐和芳族二胺，得到所述可溶性聚酰亚胺树脂，其具有优异的耐热性，溶解性，透明性和 液晶对准能力。 根据本发明，用于液晶取向层的具有二烷基取代基的可溶性聚酰亚胺聚合物包含以下式1的重复单元：因此，本发明的聚酰亚胺树脂不仅具有优异的耐热性，而且 优异的溶解性和透明性，其可以用作需要低温加工的TFT-LCD的液晶取向层。 此外，除了其制造方法之外，本发明还具有提供对耐热结构材料及其单体具有优异物理性质的聚酰亚胺树脂的效果。

    Process for manufacturing phosphoric acid-type chelate resin as uranyl ion absorbents
    10.
    发明授权
    Process for manufacturing phosphoric acid-type chelate resin as uranyl ion absorbents 失效
    制备磷酸型螯合树脂作为铀酰离子吸收剂的方法

    公开(公告)号：US5489616A

    公开(公告)日：1996-02-06

    申请号：US224057

    申请日：1993-04-07

    申请人： In Hwan Park ,  Kil-Yeong Choi ,  Jin-Chul Jung ,  Jae-Oh Joo

    发明人： In Hwan Park ,  Kil-Yeong Choi ,  Jin-Chul Jung ,  Jae-Oh Joo

    IPC分类号： C08F8/12 ,  C08F8/42 ,  C08F230/02 ,  C08F8/40

    CPC分类号： C08F8/42 ,  C08F2810/20

    摘要： This invention relates to a process of manufacturing phosphoric acid-type chelate resins as uranyl ion adsorbents having enhanced chelation and re-utilizing ability by introducing plenty of phosphoric acid groups both on main- and side-chain of the copolymer skeleton. The resin is prepared by both the radical suspension copolymerization of vinyl monomers such as styrene, divinylbenzene, and bis-(2-chloroethyl) vinylphosphonate and the additional introduction of phosphono group onto the copolymer.

    摘要翻译： 本发明涉及通过在共聚物骨架的主链和侧链上引入大量的磷酸基来制备磷酸型螯合树脂作为铀离子吸附剂的方法，其具有增强的螯合和再利用能力。 树脂通过乙烯基单体如苯乙烯，二乙烯基苯和双 - （2-氯乙基）乙烯基膦酸酯的自由基悬浮共聚和在共聚物上另外引入膦酰基来制备。