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    Process and unit for regeneration of a catalyst for the production of aromatic compounds or for reforming
    1.
    发明授权
    Process and unit for regeneration of a catalyst for the production of aromatic compounds or for reforming 失效
    用于生产芳香族化合物或重整用催化剂再生的方法和单元

    公开(公告)号：US06048814A

    公开(公告)日：2000-04-11

    申请号：US59294

    申请日：1998-04-14

    申请人： Marianne Capelle ,  Jean-Marie Deves ,  Frederic Hoffmann ,  Michel Thery ,  Fran.cedilla.ois-Xavier Brunet ,  Emmanuelle Bromet

    发明人： Marianne Capelle ,  Jean-Marie Deves ,  Frederic Hoffmann ,  Michel Thery ,  Fran.cedilla.ois-Xavier Brunet ,  Emmanuelle Bromet

    IPC分类号： B01J38/14 ,  B01J23/96 ,  B01J38/22 ,  B01J38/44 ,  C07B61/00 ,  C07C17/152 ,  C10G35/12 ,  B01J38/00

    CPC分类号： B01J8/12 ,  B01J23/96 ,  B01J38/44 ,  C10G35/12

    摘要： The invention concerns a process and unit for regenerating a catalyst for the production of aromatic compounds, in particular for reforming, the catalyst being in a moving bed, comprising combustion, oxychlorination and calcining steps, in which at least one chlorinating agent, at least one oxygen-containing gas, and water are introduced into the oxychlorination step such that the H.sub.2 O/HCl molar ratio is 1 to 50, the oxychlorination step being carried out in the presence of an oxychlorination gas containing less than 21% of oxygen and at least 50 ppm by weight of chlorine (based on HCl), and at a temperature of 350-600.degree. C., and in which the combustion step is carried out in at least two combustion zones, each zone being separated from the adjacent zones, and at least one gas charged with oxygen is introduced into each zone, the gases produced being extracted from each zone, and in which the severity of the operating conditions increases in the direction of flow of the catalyst.

    摘要翻译： 本发明涉及用于再生催化剂的方法和单元，所述催化剂用于生产芳族化合物，特别是重整催化剂在移动床中，包括燃烧，氧氯化和煅烧步骤，其中至少一种氯化剂，至少一种 将含氧气体和水引入到氧氯化步骤中，使得H 2 O / HCl摩尔比为1至50，氧氯化步骤在含有小于21％氧气和至少50％的氧氯化气体存在下进行 氯化氢（基于HCl），并且在350-600℃的温度下，并且其中燃烧步骤在至少两个燃烧区域中进行，每个区域与相邻区域分离，并且在 将至少一个带有氧气的气体引入每个区域，所产生的气体从每个区域提取，并且其中操作条件的严重性在催化剂流动方向上增加。

    Process and unit for regeneration of a catalyst for the production of aromatic compounds or for reforming
    2.
    发明授权
    Process and unit for regeneration of a catalyst for the production of aromatic compounds or for reforming 有权
    用于生产芳香族化合物或重整用催化剂再生的方法和单元

    公开(公告)号：US06277335B1

    公开(公告)日：2001-08-21

    申请号：US09503731

    申请日：2000-02-15

    申请人： Marianne Capelle ,  Jean-Marie Deves ,  Frédéric Hoffmann ,  Michel Thery ,  François-Xavier Brunet ,  Emmanuelle Bromet

    发明人： Marianne Capelle ,  Jean-Marie Deves ,  Frédéric Hoffmann ,  Michel Thery ,  François-Xavier Brunet ,  Emmanuelle Bromet

    IPC分类号： B01J3800

    CPC分类号： B01J8/12 ,  B01J23/96 ,  B01J38/44 ,  C10G35/12

    摘要： The invention concerns a process and unit for regenerating a catalyst for the production of aromatic compounds, in particular for reforming, the catalyst being in a moving bed, comprising combustion, oxychlorination and calcining steps, in which at least one chlorinating agent, at least one oxygen-containing gas, and water are introduced into the oxychlorination step such that the H2O/HCl molar ratio is 1 to 50, the oxychlorination step being carried out in the presence of an oxychlorination gas containing less than 21% of oxygen and at least 50 ppm by weight of chlorine (based on HCl), and at a temperature of 350-600° C., and in which the combustion step is carried out in at least two combustion zones, each zone being separated from the adjacent zones, and at least one gas charged with oxygen is introduced into each zone, the gases produced being extracted from each zone, and in which the severity of the operating conditions increases in the direction of flow of the catalyst.

    摘要翻译： 本发明涉及用于再生催化剂的方法和单元，所述催化剂用于生产芳族化合物，特别是重整催化剂在移动床中，包括燃烧，氧氯化和煅烧步骤，其中至少一种氯化剂，至少一种 将含氧气体和水引入到氧氯化步骤中，使得H 2 O / HCl摩尔比为1至50，氧氯化步骤在含有小于21％氧气和至少50％的氧氯化气体存在下进行 ppm（基于HCl），并且在350-600℃的温度下，并且其中燃烧步骤在至少两个燃烧区域中进行，每个区域与相邻区域分离，并且在 将至少一个带有氧气的气体引入每个区域，所产生的气体从每个区域提取，并且其中操作条件的严重性在催化剂流动方向上增加。

    Staged combustion process and apparatus for regenerating a reforming or aromatic compound production catalyst in a moving bed
    3.
    发明授权
    Staged combustion process and apparatus for regenerating a reforming or aromatic compound production catalyst in a moving bed 失效
    用于在移动床中再生重整或芳族化合物生产催化剂的分段燃烧方法和装置

    公开(公告)号：US6103652A

    公开(公告)日：2000-08-15

    申请号：US59292

    申请日：1998-04-14

    申请人： Fran.cedilla.ois-Xavier Brunet ,  Emmanuelle Bromet ,  Jean-Marie Deves

    发明人： Fran.cedilla.ois-Xavier Brunet ,  Emmanuelle Bromet ,  Jean-Marie Deves

    IPC分类号： B01J27/32 ,  B01J23/96 ,  B01J38/14 ,  B01J38/20 ,  B01J38/24 ,  B01J38/34 ,  B01J38/44 ,  C07B61/00 ,  C10G35/12 ,  B01J20/34 ,  B01J38/12 ,  B01J38/22

    CPC分类号： B01J8/12 ,  B01J23/96 ,  B01J38/20 ,  B01J38/24 ,  B01J38/44 ,  C10G35/12

    摘要： The invention concerns a process for moving bed regeneration of a reforming or aromatic hydrocarbon production catalyst. The catalyst includes a support, at least one noble metal and at least one halogen. The process includes a combustion step in which the catalyst is treated in at least two successive combustion zones. Also, the process includes each combustion zone separated from adjacent combustion zones allowing catalyst to pass and preventing passage of gas, at least one oxygen-containing gas introduced into each zone and produced gases extracted from each zone, and the severity of the operating conditions in each zone increasing in the direction of catalyst flow. Advantageously, the combustion step ends in a zone for monitoring and controlling combustion completion characterized by a low or zero oxygen consumption.

    摘要翻译： 本发明涉及一种用于移动重整或芳族烃生产催化剂的床再生的方法。 催化剂包括载体，至少一种贵金属和至少一种卤素。 该方法包括燃烧步骤，其中在至少两个连续的燃烧区域中处理催化剂。 此外，该方法还包括从相邻燃烧区分离的每个燃烧区，使得催化剂通过并防止气体的通过，至少一个引入每个区域的含氧气体和从每个区域提取的产生的气体，以及操作条件的严重性 每个区域在催化剂流动方向上增加。 有利地，燃烧步骤终止于用于监测和控制燃烧完成的区域，其特征在于低或零氧气消耗。

    Process and vessel for regeneration of a catalyst including monitoring and monitoring and control of combustion completion
    4.
    发明授权
    Process and vessel for regeneration of a catalyst including monitoring and monitoring and control of combustion completion 失效
    用于再生催化剂的过程和容器，包括监测和监测和控制燃烧完成

    公开(公告)号：US06239055B1

    公开(公告)日：2001-05-29

    申请号：US09059407

    申请日：1998-04-14

    申请人： François-Xavier Brunet ,  Emmanuelle Bromet ,  Jean-Marie Deves ,  Dominique Humeau ,  Eric Sanchez

    发明人： François-Xavier Brunet ,  Emmanuelle Bromet ,  Jean-Marie Deves ,  Dominique Humeau ,  Eric Sanchez

    IPC分类号： B01J3822

    CPC分类号： B01J8/12 ,  B01J38/12 ,  B01J38/14 ,  B01J38/20 ,  B01J38/24 ,  C10G35/12

    摘要： The invention concerns a process for regenerating a catalyst in a fixed or moving bed, for example a catalyst for reforming or for aromatic compound production, including a step for monitoring and controlling combustion completion which is carried out after the catalyst has undergone all of the combustion steps of the process. The monitoring and control step is carried out by injecting an oxygen-containing gas into the zone where monitoring and control takes place, the monitoring and control step being carried out under conditions which are more severe than those in the combustion steps. The monitoring and control step is carried out with an oxygen consumption of less than 10%. The temperature advantageously remains substantially constant. The vessel for carrying out the invention is also claimed.

    摘要翻译： 本发明涉及一种在固定或移动床中再生催化剂的方法，例如用于重整或芳族化合物生产的催化剂，包括用于监测和控制燃烧完成的步骤，其在催化剂经历了所有燃烧之后进行 过程的步骤。 监测和控制步骤通过将氧含量气体注入进行监测和控制的区域中进行，监测和控制步骤在比燃烧步骤更严格的条件下进行。 监测和控制步骤的耗氧量小于10％。 温度有利地保持基本恒定。 还要求用于实施本发明的容器。

    Process and vessel for regeneration of a catalyst including monitoring and monitoring and control of combustion completion
    5.
    发明授权
    Process and vessel for regeneration of a catalyst including monitoring and monitoring and control of combustion completion 有权
    用于再生催化剂的过程和容器，包括监测和监测和控制燃烧完成

    公开(公告)号：US06506702B2

    公开(公告)日：2003-01-14

    申请号：US09811693

    申请日：2001-03-20

    申请人： François-Xavier Brunet ,  Emmanuelle Bromet ,  Jean-Marie Deves ,  Dominique Humeau ,  Eric Sanchez

    发明人： François-Xavier Brunet ,  Emmanuelle Bromet ,  Jean-Marie Deves ,  Dominique Humeau ,  Eric Sanchez

    IPC分类号： B01J3800

    CPC分类号： B01J8/12 ,  B01J38/12 ,  B01J38/14 ,  B01J38/20 ,  B01J38/24 ,  C10G35/12

    摘要： The invention concerns a process for regenerating a catalyst in a fixed bed, for example a catalyst for reforming or for aromatic compound production, including a step for monitoring and controlling combustion completion which is carried out after the catalyst has undergone all of the combustion steps of the process. The monitoring and control step is carried out by injecting an oxygen-containing gas into the zone where monitoring and control takes place, the monitoring and control step being carried out under conditions which are more severe than those in the combustion steps. The monitoring and control step is carried out with an oxygen consumption of less than 10%. The temperature advantageously remains substantially constant.

    摘要翻译： 本发明涉及一种在固定床中再生催化剂的方法，例如用于重整或芳族化合物生产的催化剂，包括用于监测和控制燃烧完成的步骤，其在催化剂经历了所有燃烧步骤之后进行 的过程。 监测和控制步骤通过将氧含量气体注入进行监测和控制的区域中进行，监测和控制步骤在比燃烧步骤更严格的条件下进行。 监测和控制步骤的耗氧量小于10％。 温度有利地保持基本恒定。

    Vessel for regeneration of a catalyst including monitoring and monitoring and control of combustion completion
    6.
    发明授权
    Vessel for regeneration of a catalyst including monitoring and monitoring and control of combustion completion 有权
    用于再生催化剂的容器，包括监测和监测和控制燃烧完成

    公开(公告)号：US08728404B1

    公开(公告)日：2014-05-20

    申请号：US09551831

    申请日：2000-04-18

    申请人： François-Xavier Brunet ,  Emmanuelle Bromet ,  Jean-Marie Deves ,  Dominique Humeau ,  Eric Sanchez

    发明人： François-Xavier Brunet ,  Emmanuelle Bromet ,  Jean-Marie Deves ,  Dominique Humeau ,  Eric Sanchez

    IPC分类号： B01J38/14 ,  B01J38/20 ,  B01J38/22

    CPC分类号： B01J8/12 ,  B01J38/12 ,  B01J38/14 ,  B01J38/20 ,  B01J38/24 ,  C10G35/12

    摘要： A vessel for regenerating used catalyst comprising at least one combustion zone provided with at least two walls (5a, 5b) between which the catalyst circulates as a moving bed, and provided with at least one conduit (4) for introducing at least one oxygen-containing gas entering the moving bed via one of the walls and leaving via another wall, characterized in that it also comprises a zone (FC) for monitoring and controlling the end of combustion located after the end of the flame front of the last combustion zone (Z2), provided with a conduit (11) for introducing an oxygen-containing monitoring and control gas and at least one means for measuring the temperature and/or the oxygen content in the gas and/or the catalyst leaving the monitoring and control zone.A separator (29) is located between the monitoring and control zone and the last combustion zone for preventing the passage of gas while allowing for the passage of the catalyst.

    摘要翻译： 一种用于再生所用催化剂的容器，包括至少一个燃烧区，该燃烧区设置有至少两个壁（5a，5b），催化剂在其之间作为移动床循环，并且设置有至少一个导管（4），用于引入至少一个氧 - 包含气体通过一个壁进入移动床并通过另一个壁离开，其特征在于，其还包括用于监测和控制位于最后燃烧区域的火焰前端的末端之后的燃烧端的区域（FC） Z2），其具有用于引入含氧监测和控制气体的导管（11）和用于测量离开监测和控制区的气体和/或催化剂中的温度和/或氧含量的至少一种装置。 分离器（29）位于监测和控制区域与最后一个燃烧区之间，用于防止气体通过，同时允许催化剂通过。

    Staged combustion process and apparatus for regenerating a reforming or aromatic compound production catalyst in a moving bed
    7.
    发明授权
    Staged combustion process and apparatus for regenerating a reforming or aromatic compound production catalyst in a moving bed 有权
    用于在移动床中再生重整或芳族化合物生产催化剂的分段燃烧方法和装置

    公开(公告)号：US06689331B1

    公开(公告)日：2004-02-10

    申请号：US09562754

    申请日：2000-05-02

    申请人： François-Xavier Brunet ,  Emmanuelle Bromet ,  Jean-Marie Deves

    发明人： François-Xavier Brunet ,  Emmanuelle Bromet ,  Jean-Marie Deves

    IPC分类号： B01J2390

    CPC分类号： B01J8/12 ,  B01J23/96 ,  B01J38/20 ,  B01J38/24 ,  B01J38/44 ,  C10G35/12

    摘要： An apparatus for regeneration a reforming or aromatic compound production catalyst comprises a first combustion zone wherein the first combustion zone receives catalyst and an oxygen-containing gas; a successive second combustion zone; and a conduit communicating the first and second combustion zones for transferring catalysts from the first combustion zone to the second combustion zone. The first combustion zone is isolated from the second combustion zone to prevent passage of oxygen-containing gas from the first combustion zone to the second combustion zone and the severity of the operating conditions increases from the first combustion zone to the second combustion zone.

    摘要翻译： 用于再生重整或芳族化合物生产催化剂的装置包括第一燃烧区，其中第一燃烧区接收催化剂和含氧气体; 连续的第二燃烧区; 以及连通第一和第二燃烧区以将催化剂从第一燃烧区转移到第二燃烧区的导管。 第一燃烧区与第二燃烧区隔离，以防止含氧气体从第一燃烧区通过到第二燃烧区，并且操作条件的严重性从第一燃烧区增加到第二燃烧区。