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公开(公告)号:US20080262196A1
公开(公告)日:2008-10-23
申请号:US12059217
申请日:2008-03-31
CPC分类号: C08F6/12 , B29C48/03 , B29C48/268 , B29C48/395 , B29C48/402 , B29C48/45 , B29C48/687 , B29C48/767 , C08F6/003 , C08F6/10
摘要: The present invention relates to various embodiments of a system and method for separating polymer from a solvent. In one embodiment a system for separating polymer from a solvent comprises an extrusion apparatus includes a hollow member having a first end portion, a second end portion, and a feed port between the first end portion and the second end portion. The extrusion apparatus includes a back flash vent port disposed upstream of the feed port and a forward flash vent port disposed downstream of the feed port. The extrusion apparatus further includes a vent insert located at the forward flash vent port, a screw disposed inside the hollow member, and an internal superheating section disposed between the feed port and the downstream vent opening of the hollow member such that the length of the internal superheating section is greater than about four times the diameter, 4D, of the hollow member.
摘要翻译: 本发明涉及从溶剂中分离聚合物的系统和方法的各种实施方案。 在一个实施方案中,用于从溶剂中分离聚合物的系统包括挤出装置,其包括具有第一端部,第二端部和在第一端部和第二端部之间的进料口的中空构件。 挤出装置包括设置在进料口上游的后部闪蒸排放口和设置在进料口下游的前部快闪通气口。 挤出装置还包括位于前部快闪通气口处的通气插入件,设置在中空构件内部的螺钉和设置在中空构件的进料口和下游排气口之间的内部过热部分,使得内部 过热部分大于中空部件直径的四倍。
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公开(公告)号:US20070225479A1
公开(公告)日:2007-09-27
申请号:US11755415
申请日:2007-05-30
IPC分类号: C08J3/00
CPC分类号: C08F6/003 , B29C48/07 , B29C48/767 , C08F6/12 , C08G64/403 , C08G65/46 , C08G73/1032 , C08G73/1046 , C08L23/02
摘要: The present invention provides a method of separating a polymer from a solvent comprising introducing a superheated polymer-solvent mixture into an extruder, and isolating a polymer product, said extruder being equipped with at least one vent operated at subatmospheric pressure and at least one vent operated at about atmospheric pressure, said extruder having a screw diameter D, said extruder being operated at a feed rate FR and at a screw speed RPM such that a devolatilization performance ratio (DPR) given by Equation (I) DPR=FR/RPM Equation (I)is selected from a predetermined set of devolatilization performance ratios which correlate with a target characteristic of the polymer product.
摘要翻译: 本发明提供了一种从溶剂中分离聚合物的方法,包括将过热的聚合物 - 溶剂混合物引入挤出机中,并分离聚合物产物,所述挤出机配备有至少一个在低于大气压的压力下操作的通风口和至少一个排气操作 在约大气压下,所述挤出机具有螺杆直径D,所述挤出机以进给速率FR和螺杆转速RPM操作,使得式(I)给出的脱挥发性能比(DPR)<β在线式 描述=“在线公式”end =“lead”?> DPR = FR / RPM等式(I)<?in-line-formula description =“In-line Formulas”end =“tail”?> 与聚合物产品的目标特性相关的预定的脱挥发性能比。
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