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1.发明授权Preparation of maleic anhydride from butane using fluidized vanadium-phosphorous-oxide containing catalysts 失效使用流化的含钒 - 氧化磷氧化物催化剂从丁烷制备马来酸酐
公开(公告)号：US4351773A
公开(公告)日：1982-09-28
申请号：US221670
申请日：1980-12-31
IPC分类号： C07D307/60 , B01J27/18 , B01J27/198 , C01B25/37 , C01B25/45 , C07B61/00 , C07C51/215
CPC分类号： B01J23/002 , B01J27/198 , C07C51/215 , B01J2523/00
摘要： A process is provided for the preparation of fluid bed oxidation catalysts containing the mixed oxides of vanadium and phosphorus, comprising the steps of preparing the catalyst precursor, comminuting the precursor, introducing the precursor into water to form an aqueous slurry and spray drying the slurry. The resulting microspheroidal particles are excellent fluid bed catalysts for the preparation of maleic anhydride from 4-carbon atom hydrocarbons.
摘要翻译： 提供了一种制备含有钒和磷的混合氧化物的流化床氧化催化剂的方法，包括制备催化剂前体，粉碎前体，将前体引入水中以形成含水浆料并喷雾干燥浆料的步骤。 所得微球颗粒是用于从4-碳原子烃制备马来酸酐的优异流化床催化剂。
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公开(公告)号：US4400522A
公开(公告)日：1983-08-23
申请号：US374219
申请日：1982-05-03
IPC分类号： B01J23/22 , B01J27/198 , C07C51/215 , C07C51/25 , C07D307/60
CPC分类号： B01J23/002 , B01J23/22 , B01J27/198 , C07C51/215 , C07C51/25 , C07C51/252 , B01J2523/00
摘要： The present invention provides a method for the preparation of oxidation catalysts containing mixed oxides of vanadium and phosphorus, which catalysts are particularly effective in the oxidation of n-butane, n-butenes, 1,3-butadiene or a mixture thereof with molecular oxygen or an oxygen-containing gas in the vapor phase to produce high yields of maleic anhydride with good selectivity. Vanadium phosphorus mixed oxide catalyst precursors prepared in solution in organic media are extracted from the organic media with water, with subsequent drying down to recover a precursor solid, or impregnation of a support with the aqueous solution.
摘要翻译： 本发明提供一种制备含有钒和磷的混合氧化物的氧化催化剂的方法，该催化剂在正丁烷，正丁烯，1,3-丁二烯或其与分子氧或其混合物的氧化中是特别有效的 气相中的含氧气体，以产生高产率的马来酸酐，具有良好的选择性。 在有机介质溶液中制备的钒磷混合氧化物催化剂前体用水从有机介质中萃取，随后干燥以回收前体固体，或用水溶液浸渍载体。
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公开(公告)号：US4360453A
公开(公告)日：1982-11-23
申请号：US210885
申请日：1980-11-28
IPC分类号： B01J23/22 , B01J27/198 , C07C51/215 , C07C51/25 , B01J27/14
CPC分类号： C07C51/252 , B01J23/002 , B01J23/22 , B01J27/198 , C07C51/215 , C07C51/25 , B01J2523/00
摘要： The present invention provides a method for the preparation of oxidation catalysts containing mixed oxides of vanadium and phosphorus, which catalysts are particularly effective in the oxidation of n-butane, n-butenes, 1,3-butadiene or a mixture thereof with molecular oxygen or an oxygen-containing gas in the vapor phase to produce high yields of maleic anhydride with good selectivity. Vanadium phosphorus mixed oxide catalyst precursors prepared in solution in organic media are extracted from the organic media with water, with subsequent drying down to recover a precursor solid, or impregnation of a support with the aqueous solution.
摘要翻译： 本发明提供一种制备含有钒和磷的混合氧化物的氧化催化剂的方法，该催化剂在正丁烷，正丁烯，1,3-丁二烯或其与分子氧或其混合物的氧化中是特别有效的 气相中的含氧气体，以产生高产率的马来酸酐，具有良好的选择性。 在有机介质溶液中制备的钒磷混合氧化物催化剂前体用水从有机介质中萃取，随后干燥以回收前体固体，或用水溶液浸渍载体。
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