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    SEMICONDUCTOR LIGHT EMITTING PACKAGE AND METHOD OF MANUFACTURING THE SAME
    1.
    发明申请
    SEMICONDUCTOR LIGHT EMITTING PACKAGE AND METHOD OF MANUFACTURING THE SAME 审中-公开
    半导体发光封装及其制造方法

    公开(公告)号：US20120175661A1

    公开(公告)日：2012-07-12

    申请号：US13497921

    申请日：2009-09-25

    申请人： Mingjie Zhou ,  Wenbo Ma ,  Guitang Chen ,  Chaopu Shi ,  Yanbo Qiao ,  Xi Luo

    发明人： Mingjie Zhou ,  Wenbo Ma ,  Guitang Chen ,  Chaopu Shi ,  Yanbo Qiao ,  Xi Luo

    IPC分类号： H01L33/44 ,  H01L33/52

    CPC分类号： H01L33/507 ,  H01L33/501 ,  H01L33/54 ,  H01L2224/48091 ,  H01L2924/00014

    摘要： A semiconductor light emitting package includes a substrate, an encapsulating material, a semiconductor light emitting chip disposed on the substrate, wires; and an integrated glass-fluorescent powder compound light-emitting structure. The encapsulating material and the integrated glass-fluorescent powder compound light-emitting structure are packaged on the semiconductor light emitting chip, the integrated glass-fluorescent powder compound light-emitting structure is coated on the encapsulating material. The semiconductor light-emitting package has a large light-emitting area, high uniformity which can effectively avoid “halo” phenomenon, and long working life. The present invention also relates to a method for manufacturing semiconductor light emitting package, which can be implemented at low temperature and improve the reliability and the stability of the light-emitting property of the compound light-emitting structure.

    摘要翻译： 半导体发光封装包括基板，封装材料，设置在基板上的半导体发光芯片，导线; 和集成的玻璃 - 荧光粉末化合物发光结构。 封装材料和集成的玻璃 - 荧光粉末化合物发光结构被封装在半导体发光芯片上，将集成的玻璃 - 荧光粉末化合物发光结构涂覆在封装材料上。 半导体发光封装具有发光面积大，均匀性高，可以有效地避免“晕”现象，使用寿命长。 本发明还涉及可以在低温下实现的半导体发光封装的制造方法，提高复合发光结构的发光特性的可靠性和稳定性。

    Rare Earth Ion Doped Silicate Luminescence Glass and Preparation Method Thereof
    2.
    发明申请
    Rare Earth Ion Doped Silicate Luminescence Glass and Preparation Method Thereof 有权
    稀土离子掺杂硅酸盐发光玻璃及其制备方法

    公开(公告)号：US20120061615A1

    公开(公告)日：2012-03-15

    申请号：US13320753

    申请日：2009-05-19

    申请人： Mingjie Zhou ,  Wenbo Ma ,  Zhaopu Shi ,  Yanbo Qiao ,  Qingtao Li

    发明人： Mingjie Zhou ,  Wenbo Ma ,  Zhaopu Shi ,  Yanbo Qiao ,  Qingtao Li

    IPC分类号： C09K11/79

    CPC分类号： C03C4/12 ,  C03C3/062 ,  C03C3/095

    摘要： A rare earth ion doped silicate luminescence glass and preparation method thereof are provided. The luminescence glass is the material with the following formula: aM2O.bM′2O3.cSiO2.dRE2O3, wherein M is at least one of Na, K and Li, M′ is at least one of Y, Gd, La, Sc and Lu, RE is at least one of Ce, Tm, Tb, Ho, Dy, Er, Nd, Sm, Eu and Pr. The preparation method is: grinding the raw material until mixed uniformly, calcining the raw material at 1200-1500° C. for 1-5 h, cooling to room temperature, annealing at 600-1100° C. for 0.5-24 h, cooling to room temperature again, molding then getting the product. The performance of the product is stable. The product is homogenous, and the luminescence performance is good. The light transmittance is high. The process of the preparation method is simple and with low cost.

    摘要翻译： 提供了一种稀土离子掺杂硅酸盐发光玻璃及其制备方法。 发光玻璃是具有下式的材料：aM2O.bM'2O3.cSiO2.dRE2O3，其中M是Na，K和Li中的至少一种，M'是Y，Gd，La，Sc和Lu中的至少一种 ，RE为Ce，Tm，Tb，Ho，Dy，Er，Nd，Sm，Eu和Pr中的至少一种。 制备方法为：研磨原料直至混合均匀，在1200-1500℃下煅烧原料1-5小时，冷却至室温，在600-1100℃退火0.5-24小时，冷却 再到室温，成型然后得到产品。 产品性能稳定。 产品均匀，发光性能好。 透光率高。 制备方法简单，成本低。

    METAL NANO PARTICLES DOPED WITH SILICATE LUMINESCENT MATERIALS AND PREPARATION METHODS THEREOF
    3.
    发明申请
    METAL NANO PARTICLES DOPED WITH SILICATE LUMINESCENT MATERIALS AND PREPARATION METHODS THEREOF 有权
    金属纳米颗粒与硅酸盐发光材料及其制备方法

    公开(公告)号：US20130126785A1

    公开(公告)日：2013-05-23

    申请号：US13812908

    申请日：2010-07-30

    申请人： Mingjie Zhou ,  Rong Wang ,  Chaopu Shi ,  Wenbo Ma

    发明人： Mingjie Zhou ,  Rong Wang ,  Chaopu Shi ,  Wenbo Ma

    IPC分类号： C09K11/87 ,  C09K11/77

    CPC分类号： C09K11/87 ,  C09K11/7734

    摘要： Metal nano particles doped with silicate luminescent materials and preparation methods thereof are provided. The luminescent materials are represented by the general formula: (Sr1-x-yAxEuy)3SiO5:Dz@Mn, wherein A is one or two selected from alkaline-earth metal elements, D is F or Cl, @ is for coating, M is one or two selected from Ag, Au, Pt, Pd or Cu metal nano particles, 0≦x≦0.5, 0.001

    摘要翻译： 提供掺杂有硅酸盐发光材料的金属纳米颗粒及其制备方法。 发光材料由以下通式表示：（Sr1-x-yAxEuy）3SiO5：Dz @ Mn，其中A为选自碱土金属元素中的一种或两种，D为F或Cl，@为涂层，M为 一种或两种选自Ag，Au，Pt，Pd或Cu金属纳米颗粒，0 @ x @ 0.5，0.001

    ZINC MANGANESE SILICATE CONTAINING METAL PARTICLES LUMINESCENT MATERIALS AND PREPARATION METHODS THEREOF
    4.
    发明申请
    ZINC MANGANESE SILICATE CONTAINING METAL PARTICLES LUMINESCENT MATERIALS AND PREPARATION METHODS THEREOF 有权
    包含金属颗粒的金属硅酸盐材料及其制备方法

    公开(公告)号：US20130126784A1

    公开(公告)日：2013-05-23

    申请号：US13703342

    申请日：2010-06-30

    申请人： Mingjie Zhou ,  Wenbo Ma ,  Chaopu Shi

    发明人： Mingjie Zhou ,  Wenbo Ma ,  Chaopu Shi

    IPC分类号： C09K11/59 ,  C09K11/87

    CPC分类号： C09K11/59 ,  C01B33/20 ,  C09K11/595 ,  C09K11/87 ,  C09K11/876

    摘要： Zinc manganese silicate containing metal particles luminescent materials and preparation methods thereof are provided. The said luminescent materials are represented by the general formula: Zn2-xSiO4: Mnx, My, wherein M is metal, 0.001≦x≦0.1, 0.00001≦y≦0.01. The said methods include the following steps: step 1, preparing silica aerogel containing metal particles; step 2, weighing source compound of zinc, source compound of manganese and the silica aerogel in step 1 at stoichiometric ratio and mixing them to form mixture; step 3, sintering the mixture in step 2, then cooling and grinding to form the said luminescent materials with higher luminescent intensity. The said methods have simple steps, easy operation, low sintering temperature and low cost.

    摘要翻译： 提供了含有金属锰酸锰的发光材料及其制备方法。 所述发光材料由以下通式表示：Zn2-xSiO4：Mnx，My，其中M是金属，0.001 @ x @ 0.1,0.00001 @ y @ 0.01。 所述方法包括以下步骤：步骤1，制备含有金属颗粒的二氧化硅气凝胶; 步骤2，在化学计量比下，在步骤1中称量锌源，锰源和二氧化硅气凝胶，混合形成混合物; 步骤3，在步骤2中烧结混合物，然后冷却和研磨以形成具有较高发光强度的所述发光材料。 所述方法操作简单，操作简便，烧结温度低，成本低。

    Metal nano particles doped with silicate luminescent materials and preparation methods thereof
    6.
    发明授权
    Metal nano particles doped with silicate luminescent materials and preparation methods thereof 有权
    掺有硅酸盐发光材料的金属纳米颗粒及其制备方法

    公开(公告)号：US09206353B2

    公开(公告)日：2015-12-08

    申请号：US13812908

    申请日：2010-07-30

    申请人： Mingjie Zhou ,  Rong Wang ,  Chaopu Shi ,  Wenbo Ma

    发明人： Mingjie Zhou ,  Rong Wang ,  Chaopu Shi ,  Wenbo Ma

    IPC分类号： C09K11/00 ,  C09K11/87 ,  C09K11/77

    CPC分类号： C09K11/87 ,  C09K11/7734

    摘要： Metal nano particles doped with silicate luminescent materials and preparation methods thereof are provided. The luminescent materials are represented by the general formula: (Sr1-x-yAxEuy)3SiO5:Dz@Mn, wherein A is one or two selected from alkaline-earth metal elements, D is F or Cl, @ is for coating, M is one or two selected from Ag, Au, Pt, Pd or Cu metal nano particles, 0≦x≦0.5, 0.001

    摘要翻译： 提供掺杂有硅酸盐发光材料的金属纳米颗粒及其制备方法。 发光材料由以下通式表示：（Sr1-x-yAxEuy）3SiO5：Dz @ Mn，其中A为选自碱土金属元素中的一种或两种，D为F或Cl，@为涂层，M为 一种或两种选自Ag，Au，Pt，Pd或Cu金属纳米颗粒，0＆lt; lE; x＆lt; lE; 0.5,0.001＆lt; y＆nlE; 0.15和0＆amp; nlE; z＆nlE; 0.5。 n是金属纳米颗粒与硅元素的摩尔比，其中0

    Zinc manganese silicate containing metal particles luminescent materials and preparation methods thereof
    7.
    发明授权
    Zinc manganese silicate containing metal particles luminescent materials and preparation methods thereof 有权
    含锌锰酸锰的金属颗粒发光材料及其制备方法

    公开(公告)号：US09115309B2

    公开(公告)日：2015-08-25

    申请号：US13703342

    申请日：2010-06-30

    申请人： Mingjie Zhou ,  Wenbo Ma ,  Chaopu Shi

    发明人： Mingjie Zhou ,  Wenbo Ma ,  Chaopu Shi

    IPC分类号： C09K11/59 ,  C09K11/87 ,  C01B33/20

    CPC分类号： C09K11/59 ,  C01B33/20 ,  C09K11/595 ,  C09K11/87 ,  C09K11/876

    摘要： Zinc manganese silicate containing metal particles luminescent materials and preparation methods thereof are provided. The said luminescent materials are a blend of metal M nanoparticles and Zn2-xSiO4:Mnx, wherein M is one of Ag, Au and Pt, 0.001≦x≦0.1, 0.00001≦y≦0.01, y is the molar ratio of M to Zn2-xSiO4:Mnx. The said methods include the following steps: step 1, preparing silica aerogel containing metal particles; step 2, weighing source compound of zinc, source compound of manganese and the silica aerogel in step 1 at stoichiometric ratio and mixing them to form mixture; step 3, sintering the mixture in step 2, then cooling and grinding to form the said luminescent materials with higher luminescent intensity. The said methods have simple steps, easy operation, low sintering temperature and low cost.

    摘要翻译： 提供了含有金属锰酸锰的发光材料及其制备方法。 所述发光材料是金属M纳米颗粒和Zn2-xSiO4：Mnx的共混物，其中M是Ag，Au和Pt之一，0.001和n1E; x和nlE; 0.1,0.00001＆amp; nlE; y＆nlE; 0.01，y是M 到Zn2-xSiO4：Mnx。 所述方法包括以下步骤：步骤1，制备含有金属颗粒的二氧化硅气凝胶; 步骤2，在化学计量比下，在步骤1中称量锌源，锰源和二氧化硅气凝胶，混合形成混合物; 步骤3，在步骤2中烧结混合物，然后冷却和研磨以形成具有较高发光强度的所述发光材料。 所述方法操作简单，操作简便，烧结温度低，成本低。

    Green light-emitting glass and method of preparing the same
    9.
    发明授权
    Green light-emitting glass and method of preparing the same 有权
    绿色发光玻璃及其制备方法

    公开(公告)号：US08592333B2

    公开(公告)日：2013-11-26

    申请号：US13257314

    申请日：2009-03-25

    申请人： Mingjie Zhou ,  Wenbo Ma ,  Zhaopu Shi ,  Yanbo Qiao ,  Qingtao Li

    发明人： Mingjie Zhou ,  Wenbo Ma ,  Zhaopu Shi ,  Yanbo Qiao ,  Qingtao Li

    IPC分类号： C03C3/095 ,  C03C4/12 ,  C03B25/00 ,  C09K11/78 ,  C09K11/79

    CPC分类号： C09K11/7774 ,  C03C3/095 ,  C03C4/12

    摘要： A green light-emitting glass and the method of preparing the same are provided. The components with parts by mole of the green light-emitting glass are alkali oxide 25-40, Y2O3 0.01-15, SiO2 40-70, Tb2O3 0.01-15. The method of preparing the glass includes mixing alkali salt with Y2O3, SiO2 and Tb4O7, firing the mixture at 1200° C.-1500° C. for 1-5 hours, cooling the precursor to the room temperature and annealing the precursor in a reducing atmosphere at 600° C.-1200° C. for 1-20 hours. A green light-emitting glass with good transparence, high uniformity, easily being made into big bulk and high stability is provided. The process of capsulation of parts by using the glass is simple. And a method of preparing the glass with simple process and low cost is provided.

    摘要翻译： 提供绿色发光玻璃及其制备方法。 具有摩尔比的绿色发光玻璃的组分是碱金属氧化物25-40，Y2O3 0.01-15，SiO2 40-70，Tb2O3 0.01-15。 制备玻璃的方法包括将碱金属盐与Y 2 O 3，SiO 2和Tb 4 O 7混合，将混合物在1200℃-1500℃下烧制1-5小时，将前体冷却至室温，并在还原 气氛在600℃-1200℃下保持1-20小时。 提供透明性好，均匀性好，容易制成大体积，高稳定性的绿色发光玻璃。 通过使用玻璃来封装部件的过程很简单。 并提供了一种以简单的工艺和低成本制备玻璃的方法。

    SILICATE FLUORESCENT MATERIAL AND PREPARATION METHOD THEREOF
    10.
    发明申请
    SILICATE FLUORESCENT MATERIAL AND PREPARATION METHOD THEREOF 审中-公开
    硅酸盐荧光材料及其制备方法

    公开(公告)号：US20130119313A1

    公开(公告)日：2013-05-16

    申请号：US13811859

    申请日：2010-07-28

    申请人： Mingjie Zhou ,  Wenbo Ma ,  Yanbo Qiao

    发明人： Mingjie Zhou ,  Wenbo Ma ,  Yanbo Qiao

    IPC分类号： C09K11/77

    CPC分类号： C09K11/7774 ,  C09K11/873

    摘要： A silicate fluorescent material is provided. The general chemical formula of the luminescent material is Ln2SiO5:Tb, M, wherein Ln represents at least one of the elements selected from Y, Gd, La or Lu, M represents at least one of the nanoparticles selected from Ag, Au, Os, Ir, Pt, Ru, Rh or Pd, the mole ratio of Tb to Ln is greater than 0 but not greater than 0.25. The porous glass containing metal nanoparticles is prepared by introducing metal nano ions into the porous glass and extracting the uniformly dispersed metal nanoparticles from the porous glass via a chemical reduction method. A silicate fluorescent material with enhanced luminescence is obtained by substituting SiO2 which is the raw material in the process for preparing the silicate fluorescent material via the conventional high temperature solid phase sintering with the porous glass containing metal nanoparticles. The performance of the silicate fluorescent material is better and the light emitting efficiency of the silicate fluorescent material is higher compared with the conventional silicate fluorescent material.

    摘要翻译： 提供硅酸盐荧光材料。 发光材料的一般化学式为Ln2SiO5：Tb，M，其中Ln表示选自Y，Gd，La或Lu中的至少一种元素，M表示选自Ag，Au，Os， Ir，Pt，Ru，Rh或Pd，Tb与Ln的摩尔比大于0但不大于0.25。 通过将金属纳米离子引入多孔玻璃中并通过化学还原法从多孔玻璃中提取均匀分散的金属纳米粒子来制备含金属纳米颗粒的多孔玻璃。 通过用含有金属纳米颗粒的多孔玻璃的常规高温固相烧结来代替通过常规高温固相烧结制备硅酸盐荧光材料的方法中的原料SiO 2来获得具有增强发光的硅酸盐荧光材料。 与传统的硅酸盐荧光材料相比，硅酸盐荧光材料的性能更好，硅酸盐荧光材料的发光效率更高。