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    BLUE LIGHT EMITTING GLASS AND PREPARATION METHOD THEREOF
    1.
    发明申请
    BLUE LIGHT EMITTING GLASS AND PREPARATION METHOD THEREOF 有权
    蓝光发光玻璃及其制备方法

    公开(公告)号：US20120091394A1

    公开(公告)日：2012-04-19

    申请号：US13377569

    申请日：2009-06-25

    申请人： Mingjie Zhou ,  Wenbo Ma ,  Zhaopu Shi

    发明人： Mingjie Zhou ,  Wenbo Ma ,  Zhaopu Shi

    IPC分类号： C09K11/79 ,  C03B32/00

    CPC分类号： C03C3/095 ,  C03B32/00 ,  C03C3/062 ,  C03C4/12 ,  C09K11/7721

    摘要： Blue light emitting glass and the preparation method thereof are provided. The blue light emitting glass has the following composition: aCaO.bAl2O3.cSiO2.xCeO2, wherein a, b, c and x are, by mol part, 15-55, 15-35, 20-60 and 0.01-5 respectively. The preparation method comprises: weighing the raw materials according to the composition of the blue light emitting glass; mixing the raw materials uniformly and melting the raw materials to obtain glass melt; moulding the glass melt to obtain transparent glass; thermally treating the transparent glass under reducing atmosphere, and thereafter obtaining the finished product. The blue light emitting glass obtained has intense broadband excitation spectrum in ultraviolet region and emits intense blue light under the excitation of ultraviolet light. It is suitable for using as luminescent medium material.

    摘要翻译： 提供蓝色发光玻璃及其制备方法。 蓝色发光玻璃具有以下组成：aCaO.bAl2O3.cSiO2.xCeO2，其中a，b，c和x分别为15-55,15-35,20-60和0.01-5。 制备方法包括：根据蓝色发光玻璃的成分称量原料; 均匀混合原料，熔化原料，得到玻璃熔体; 将玻璃熔体成型得到透明玻璃; 在还原气氛下对透明玻璃进行热处理，然后得到成品。 获得的蓝色发光玻璃在紫外线区域具有强烈的宽带激发光谱，并在紫外光的激发下发出强烈的蓝光。 适合用作发光介质材料。

    Rare Earth Ion Doped Silicate Luminescence Glass and Preparation Method Thereof
    2.
    发明申请
    Rare Earth Ion Doped Silicate Luminescence Glass and Preparation Method Thereof 有权
    稀土离子掺杂硅酸盐发光玻璃及其制备方法

    公开(公告)号：US20120061615A1

    公开(公告)日：2012-03-15

    申请号：US13320753

    申请日：2009-05-19

    申请人： Mingjie Zhou ,  Wenbo Ma ,  Zhaopu Shi ,  Yanbo Qiao ,  Qingtao Li

    发明人： Mingjie Zhou ,  Wenbo Ma ,  Zhaopu Shi ,  Yanbo Qiao ,  Qingtao Li

    IPC分类号： C09K11/79

    CPC分类号： C03C4/12 ,  C03C3/062 ,  C03C3/095

    摘要： A rare earth ion doped silicate luminescence glass and preparation method thereof are provided. The luminescence glass is the material with the following formula: aM2O.bM′2O3.cSiO2.dRE2O3, wherein M is at least one of Na, K and Li, M′ is at least one of Y, Gd, La, Sc and Lu, RE is at least one of Ce, Tm, Tb, Ho, Dy, Er, Nd, Sm, Eu and Pr. The preparation method is: grinding the raw material until mixed uniformly, calcining the raw material at 1200-1500° C. for 1-5 h, cooling to room temperature, annealing at 600-1100° C. for 0.5-24 h, cooling to room temperature again, molding then getting the product. The performance of the product is stable. The product is homogenous, and the luminescence performance is good. The light transmittance is high. The process of the preparation method is simple and with low cost.

    摘要翻译： 提供了一种稀土离子掺杂硅酸盐发光玻璃及其制备方法。 发光玻璃是具有下式的材料：aM2O.bM'2O3.cSiO2.dRE2O3，其中M是Na，K和Li中的至少一种，M'是Y，Gd，La，Sc和Lu中的至少一种 ，RE为Ce，Tm，Tb，Ho，Dy，Er，Nd，Sm，Eu和Pr中的至少一种。 制备方法为：研磨原料直至混合均匀，在1200-1500℃下煅烧原料1-5小时，冷却至室温，在600-1100℃退火0.5-24小时，冷却 再到室温，成型然后得到产品。 产品性能稳定。 产品均匀，发光性能好。 透光率高。 制备方法简单，成本低。

    BISMUTH ION SENSITIZED RARE EARTH GERMANATE LUMINESCENCE MATERIALS AND PREPARATION METHODS THEREOF
    3.
    发明申请
    BISMUTH ION SENSITIZED RARE EARTH GERMANATE LUMINESCENCE MATERIALS AND PREPARATION METHODS THEREOF 有权
    BISMUTH离子敏感稀土地球化学发光材料及其制备方法

    公开(公告)号：US20120199791A1

    公开(公告)日：2012-08-09

    申请号：US13501596

    申请日：2009-10-12

    申请人： Mingjie Zhou ,  Wenbo Ma ,  Zhaopu Shi

    发明人： Mingjie Zhou ,  Wenbo Ma ,  Zhaopu Shi

    IPC分类号： C09K11/78

    CPC分类号： C09K11/7775 ,  C09K11/7793

    摘要： Bismuth ion sensitized rare earth germanate luminescence materials and preparation methods are disclosed. The luminescence materials are the compounds of the following general formula (Y1-x-y-zAxBiyLnz)2GeO5. The preparation methods comprise: using oxides, carbonates, oxalates, acetates, nitrates or halides of Y, A, Bi, Ln and Ge as raw materials, wherein A is one of Gd, Lu, Sc and La, and Ln is at least one of Tm, Ho, Sm, Tb, Eu and Dy, homogeneously grinding the raw materials, sintering at 1300-1500° C. for 6-24 h, and then cooling them to room temperature to obtain the bismuth ion sensitized rare earth germanate luminescence materials.

    摘要翻译： 公开了铋离子敏化稀土锗酸盐发光材料及制备方法。 发光材料是以下通式（Y1-x-y-zAxBiyLnz）2GeO5的化合物。 制备方法包括：以Y，A，Bi，Ln和Ge为原料的氧化物，碳酸盐，草酸盐，乙酸盐，硝酸盐或卤化物为原料，其中A为Gd，Lu，Sc和La之一，Ln为至少一种 的Tm，Ho，Sm，Tb，Eu和Dy，对原材料进行均匀研磨，在1300-1500℃下烧结6〜24h，然后冷却至室温，得到铋离子增感稀土锗酸盐发光 材料

    ZnO green luminescent material and its preparation
    6.
    发明授权
    ZnO green luminescent material and its preparation 有权
    ZnO绿色发光材料及其制备

    公开(公告)号：US08709284B2

    公开(公告)日：2014-04-29

    申请号：US13254862

    申请日：2009-03-06

    申请人： Mingjie Zhou ,  Wenbo Ma ,  Zhaopu Shi

    发明人： Mingjie Zhou ,  Wenbo Ma ,  Zhaopu Shi

    IPC分类号： C09K11/78

    CPC分类号： C09K11/773

    摘要： The present invention relates to ZnO green luminescent material and its preparation. The ZnO green luminescent material is prepared by doping a trivalent rare earth ion compound and a Li compound into zinc oxide material. The method comprises the following steps: (1) weighing raw material in the stoichiometric ratio of formula ZnO: xA, yLi, (2) grinding the raw material, sintering it at 800-1200° C. for 2-8 h, cooling to the room temperature, and then obtaining the ZnO green luminescent material. The present ZnO green luminescent material doped with trivalent rare earth ion compound and Li compound has high stability and luminous intensity, and has higher low-voltage cathode ray luminescence efficiency. The method can easily be operated and can be used widely.

    摘要翻译： 本发明涉及ZnO绿色发光材料及其制备方法。 通过将三价稀土离子化合物和Li化合物掺杂到氧化锌材料中来制备ZnO绿色发光材料。 该方法包括以下步骤：（1）以式ZnO的化学计量比称量原料：xA，yLi，（2）研磨原料，在800-1200℃下烧结2-8小时，冷却至 室温，然后得到ZnO绿色发光材料。 掺有三价稀土离子化合物和Li化合物的本发明的ZnO绿色发光材料具有高稳定性和发光强度，并且具有更高的低电压阴极射线发光效率。 该方法易于操作，可广泛应用。

    ZnO GREEN LUMINESCENT MATERIAL AND ITS PREPARATION
    7.
    发明申请
    ZnO GREEN LUMINESCENT MATERIAL AND ITS PREPARATION 有权
    ZnO绿色发光材料及其制备

    公开(公告)号：US20120175560A1

    公开(公告)日：2012-07-12

    申请号：US13254862

    申请日：2009-03-06

    申请人： Mingjie Zhou ,  Wenbo Ma ,  Zhaopu Shi

    发明人： Mingjie Zhou ,  Wenbo Ma ,  Zhaopu Shi

    IPC分类号： C09K11/78 ,  B02C19/00 ,  C09K11/85

    CPC分类号： C09K11/773

    摘要： The present invention relates to ZnO green luminescent material and its preparation. The ZnO green luminescent material is prepared by doping a trivalent rare earth ion compound and a Li compound into zinc oxide material. The method comprises the following steps: (1) weighing raw material in the stoichiometric ratio of formula ZnO: xA, yLi, (2) grinding the raw material, sintering it at 800-1200° C. for 2-8 h, cooling to the room temperature, and then obtaining the ZnO green luminescent material. The present ZnO green luminescent material doped with trivalent rare earth ion compound and Li compound has high stability and luminous intensity, and has higher low-voltage cathode ray luminescence efficiency. The method can easily be operated and can be used widely.

    摘要翻译： 本发明涉及ZnO绿色发光材料及其制备方法。 通过将三价稀土离子化合物和Li化合物掺杂到氧化锌材料中来制备ZnO绿色发光材料。 该方法包括以下步骤：（1）以式ZnO的化学计量比称量原料：xA，yLi，（2）研磨原料，在800-1200℃下烧结2-8小时，冷却至 室温，然后得到ZnO绿色发光材料。 掺有三价稀土离子化合物和Li化合物的本发明的ZnO绿色发光材料具有高稳定性和发光强度，并且具有更高的低电压阴极射线发光效率。 该方法易于操作，可广泛应用。

    GREEN LUMINESCENT GLASS FOR ULTRAVIOLET LED AND PREPARATION METHOD THEREOF
    8.
    发明申请
    GREEN LUMINESCENT GLASS FOR ULTRAVIOLET LED AND PREPARATION METHOD THEREOF 审中-公开
    绿光LED用绿色荧光灯及其制备方法

    公开(公告)号：US20120138854A1

    公开(公告)日：2012-06-07

    申请号：US13390093

    申请日：2009-08-10

    申请人： Mingjie Zhou ,  Wenbo Ma ,  Zhaopu Shi

    发明人： Mingjie Zhou ,  Wenbo Ma ,  Zhaopu Shi

    IPC分类号： C03C4/12 ,  C03B5/235 ,  C03B25/00 ,  C03B3/00

    CPC分类号： C03C4/12 ,  C03C3/062 ,  C03C3/095

    摘要： A green luminescent glass for ultraviolet LED and a preparation method for glass are disclosed. The preparation method includes: weighing raw materials of CaCO3, Al2O3, SiO2, CeO2 and Tb4O7 respectively and mixing the raw materials evenly; melting the raw materials at 1500˜1700 for 0.5˜3 hours and then molding to form a glass; annealing the formed glass in reducing atmosphere with temperature of 650˜1050 for 3˜20 hours; and cooling the glass to room temperature to obtain the green luminescent glass for ultraviolet LED. The green luminescent glass for ultraviolet LED prepared according to the preparation method of the disclosure has advantages of high luminous intensity, uniformity and stability.

    摘要翻译： 公开了一种用于紫外线LED的绿色发光玻璃和玻璃的制备方法。 制备方法包括：分别称量CaCO3，Al2O3，SiO2，CeO2和Tb4O7的原料，均匀混合原料; 将原料在1500〜1700℃下熔炼0.5〜3小时，然后成型形成玻璃; 在650〜1050℃的还原气氛中退火成型玻璃3〜20小时; 并将玻璃冷却至室温，得到用于紫外线LED的绿色发光玻璃。 根据本发明的制备方法制备的用于紫外线LED的绿色发光玻璃具有高发光强度，均匀性和稳定性的优点。

    Blue light emitting glass and preparation method thereof
    9.
    发明授权
    Blue light emitting glass and preparation method thereof 有权
    蓝色发光玻璃及其制备方法

    公开(公告)号：US08741178B2

    公开(公告)日：2014-06-03

    申请号：US13377569

    申请日：2009-06-25

    申请人： Mingjie Zhou ,  Wenbo Ma ,  Zhaopu Shi

    发明人： Mingjie Zhou ,  Wenbo Ma ,  Zhaopu Shi

    IPC分类号： C03C3/068 ,  C03C3/095 ,  C03C4/12

    CPC分类号： C03C3/095 ,  C03B32/00 ,  C03C3/062 ,  C03C4/12 ,  C09K11/7721

    摘要： Blue light emitting glass and the preparation method thereof are provided. The blue light emitting glass has the following composition: aCaO.bAl2O3.cSiO2.xCeO2, wherein a, b, c and x are, by mol part, 15-55, 15-35, 20-60 and 0.01-5 respectively. The preparation method comprises: weighing the raw materials according to the composition of the blue light emitting glass; mixing the raw materials uniformly and melting the raw materials to obtain glass melt; molding the glass melt to obtain transparent glass; thermally treating the transparent glass under reducing atmosphere, and thereafter obtaining the finished product. The blue light emitting glass obtained has intense broadband excitation spectrum in ultraviolet region and emits intense blue light under the excitation of ultraviolet light. It is suitable for using as luminescent medium material.

    摘要翻译： 提供蓝色发光玻璃及其制备方法。 蓝色发光玻璃具有以下组成：aCaO.bAl2O3.cSiO2.xCeO2，其中a，b，c和x分别为15-55,15-35,20-60和0.01-5。 制备方法包括：根据蓝色发光玻璃的成分称量原料; 均匀混合原料，熔化原料，得到玻璃熔体; 将玻璃熔体成型得到透明玻璃; 在还原气氛下对透明玻璃进行热处理，然后得到成品。 获得的蓝色发光玻璃在紫外线区域具有强烈的宽带激发光谱，并在紫外光的激发下发出强烈的蓝光。 适合用作发光介质材料。

    Bismuth ion sensitized rare earth germanate luminescence materials and preparation methods thereof
    10.
    发明授权
    Bismuth ion sensitized rare earth germanate luminescence materials and preparation methods thereof 有权
    铋离子敏化稀土锗酸盐发光材料及其制备方法

    公开(公告)号：US08703020B2

    公开(公告)日：2014-04-22

    申请号：US13501596

    申请日：2009-10-12

    申请人： Mingjie Zhou ,  Wenbo Ma ,  Zhaopu Shi

    发明人： Mingjie Zhou ,  Wenbo Ma ,  Zhaopu Shi

    IPC分类号： C09K11/78 ,  C09K11/77

    CPC分类号： C09K11/7775 ,  C09K11/7793

    摘要： Bismuth ion sensitized rare earth germanate luminescence materials and preparation methods are disclosed. The luminescence materials are the compounds of the following general formula (Y1-x-y-zAxBiyLnz)2GeO5. The preparation methods comprise: using oxides, carbonates, oxalates, acetates, nitrates or halides of Y, A, Bi, Ln and Ge as raw materials, wherein A is one of Gd, Lu, Sc and La, and Ln is at least one of Tm, Ho, Sm, Tb, Eu and Dy, homogeneously grinding the raw materials, sintering at 1300-1500° C. for 6-24 h, and then cooling them to room temperature to obtain the bismuth ion sensitized rare earth germanate luminescence materials.

    摘要翻译： 公开了铋离子敏化稀土锗酸盐发光材料及制备方法。 发光材料是以下通式（Y1-x-y-zAxBiyLnz）2GeO5的化合物。 制备方法包括：以Y，A，Bi，Ln和Ge为原料的氧化物，碳酸盐，草酸盐，乙酸盐，硝酸盐或卤化物为原料，其中A为Gd，Lu，Sc和La之一，Ln为至少一种 的Tm，Ho，Sm，Tb，Eu和Dy，对原材料进行均匀研磨，在1300-1500℃下烧结6〜24h，然后冷却至室温，得到铋离子增感稀土锗酸盐发光 材料