METHOD FOR MANUFACTURING METHYLTETRAHYDROPHTHALIC ANHYDRIDE

    公开(公告)号:US20240140900A1

    公开(公告)日:2024-05-02

    申请号:US18069943

    申请日:2022-12-21

    CPC classification number: C07C51/56 C07D307/89

    Abstract: A method for manufacturing methyltetrahydrophthalic anhydride is provided, which includes steps as follows. Maleic anhydride is added into a reactor. Piperylene is added into the reactor, so that the piperylene and the maleic anhydride undergo a first addition reaction. When a conversion rate of the maleic anhydride is more than 25%, the first addition reaction is completed. Isoprene is added into the reactor, so that the isoprene and the maleic anhydride undergo a second addition reaction to obtain a methyltetrahydrophthalic anhydride product. The methyltetrahydrophthalic anhydride product contains 3-methyltetrahydrophthalic anhydride and 4-methyltetrahydrophthalic anhydride.

    METHOD FOR ISOMERIZING METHYLTETRAHYDROPHTHALIC ANHYDRIDE

    公开(公告)号:US20250034103A1

    公开(公告)日:2025-01-30

    申请号:US18474204

    申请日:2023-09-25

    Abstract: A method for isomerizing methyltetrahydrophthalic anhydride includes the following processes. A liquid reactant is provided. Under a condition of injecting nitrogen gas, an alkaline catalyst is added into the liquid reactant for an isomerization reaction, so as to obtain an isomerization product. The liquid reactant includes 3-methyltetrahydrophthalic anhydride and 4-methyltetrahydrophthalic anhydride. Based on a total weight of the isomerization product being 100 wt %, an amount of a methyltetrahydrophthalic anhydride dimer is lower than 1.6 wt %.

    PLASTICIZER AND METHOD FOR MANUFACTURING THE SAME

    公开(公告)号:US20230374202A1

    公开(公告)日:2023-11-23

    申请号:US18072619

    申请日:2022-11-30

    CPC classification number: C08G63/16

    Abstract: A plasticizer and a method for manufacturing the plasticizer are provided. The method includes the following steps. A dicarboxylic acid, a diol, and a catalyst are mixed to form a reactant mixture. The reactant mixture is reacted at a temperature ranging from 130° C. to 220° C. to form a semi-product. An endcapping alcohol is added into the semi-product at a temperature ranging from 205° C. to 220° C. to form a coarse plasticizer. The coarse plasticizer is purified under a pressure ranging from 760 Torr to 5 Torr to obtain the plasticizer. The dicarboxylic acid includes succinic acid or adipic acid. The diol includes diethylene glycol and 2-methyl-1,3-propanediol. The endcapping alcohol is an ether alcohol or a fatty alcohol having a carbon number of less than or equal to 4. The dicarboxylic acid, the diol, and the endcapping alcohol have a molar ratio ranging from 1:0.6 to 0.9:0.3 to 0.6.

    PLASTICIZER AND METHOD FOR MANUFACTURING THE SAME

    公开(公告)号:US20230374201A1

    公开(公告)日:2023-11-23

    申请号:US17985597

    申请日:2022-11-11

    CPC classification number: C08G63/16 C08G63/85

    Abstract: A plasticizer and a method for manufacturing the plasticizer are provided. The method includes steps as follow. A dicarboxylic acid, a diol, and a catalyst are mixed to form a reactant mixture. The reactant mixture is reacted at a temperature ranging from 130° C. to 220° C. to form a semi-product. An endcapping alcohol into the semi-product at a temperature ranging from 205° C. to 220° C. to form a coarse plasticizer. The coarse plasticizer is purified under a pressure ranging from 760 Torr to 5 Torr to obtain the plasticizer. The dicarboxylic acid includes a first dicarboxylic acid and a second dicarboxylic acid, and the second dicarboxylic acid is adipic acid. The diol includes diethylene glycol and 2-methyl-1, 3-propanediol. The endcapping alcohol includes isooctyl alcohol, isodecyl alcohol, or 2-propylheptanol. A molar ratio of dicarboxylic acid:diol:the endcapping alcohol ranges from 1:0.6 to 0.9:0.3 to 0.6.

    PLASTICIZER AND METHOD FOR MANUFACTURING THE SAME

    公开(公告)号:US20230374200A1

    公开(公告)日:2023-11-23

    申请号:US17979070

    申请日:2022-11-02

    CPC classification number: C08G63/16

    Abstract: A plasticizer and a method for manufacturing the plasticizer are provided. The method for manufacturing the plasticizer includes steps as follows: mixing a dicarboxylic acid, a diol, and a catalyst to form a reactant mixture; reacting the reactant mixture at a temperature ranging from 130° C. to 220° C. so as to form a semi-product; adding an endcapping alcohol into the semi-product at a temperature ranging from 205° C. to 220° C. so as to form a coarse plasticizer; purifying the coarse plasticizer under a pressure ranging from 760 Torr to 5 Torr so as to obtain the plasticizer. The dicarboxylic acid includes adipic acid. The diol includes a polyglycol and a saturated fatty alcohol. The endcapping alcohol includes isooctyl alcohol, isodecyl alcohol, or 2-propylheptanol. The dicarboxylic acid, the diol, and the endcapping alcohol have a molar ratio ranging from 1:0.6 to 0.9:0.3 to 0.6.

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