摘要:
The invention concerns an apparatus and a method for continuous measuring volumetric flow rates or volume changes in a material that undergoes physical, chemical-physical and/or chemical processes. The apparatus is constructed with a reference chamber which is connected to a test chamber, and means for maintaining a selected pressure in the reference chamber, as well as means for regulating the temperature in the reference chamber.
摘要:
The present invention concerns a method for in situ measuring of evaporation from a surface and an apparatus for measuring the evaporation from a surface. The apparatus comprises an evaporation surface made of a porous, hydrophilic material, which surface is connected to a reservoir. The method describes how to use the apparatus according to the invention.
摘要:
The invention provides for a dynamic dew point analysis method as well as an apparatus for carrying out the method wherein the method comprises: arranging a moisture containing gas in the immediate vicinity of at least two thermocouples, where one thermocouple is shielded from the gas; creating an analogous temperature change in both thermocouples and registering the temperature in both thermocouples during a cycle where the condensation point of the moisture containing gas is passed, using the different temperatures from the at least two thermocouples as input for determining the dew point according to basic thermodynamic principles.
摘要:
Process for adjusting the halogen content of halogenated aliphatic ethers, by selective replacement of a halide substituent on the ether with a hydrogen. The process is particularly useful for the production of certain inhalant anesthetics.
摘要:
Processes for the preparation of certain halogenated aliphatic ethers are described, and in particular the preparation of 1,1,2-trifluoro-2-chloroethyl methyl ether, i.e., CH.sub.3 OCF.sub.2 CHFCl. This particular ether has many uses, and is a valuable material for use in the production of the inhalant anesthetic enflurane, 1,1,2-trifluoro-2-chloroethyl difluoromethyl ether, i.e., CF.sub.2 HOCF.sub.2 CHFCl, made and sold under the trademark ETHRANE by Airco, Inc., Montvale, New Jersey 07645.
摘要:
Methods for the dehalogenation of various haloethers are disclosed, comprising providing a haloether having the formula CX'.sub.3 -[CY.sub.2 ].sub.n -O-CZ.sub.2 -CX.sub.3 in which X', Y, Z and X are specifically disclosed combinations of hydrogen, fluorine chlorine and bromine such that the molecule includes at least one reducible group, but where both portions of any ethyl groups present are not reducible. Dehalogenation of these haloethers is carried out by contacting same with a hydrogen donor comprising an amine, preferably a primary or secondary amine or a primary, secondary or tertiary alkanol amine. The amine is preferably used in combination with a catalyst, such as a varivalent metal or a salt thereof, such as copper or a copper salt.