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1.发明授权N,N-Dialkyl-N-aminoalkyl-N-(amino or nitro)phenylalkyl- and N-methyl-N-[3-(amino or nitro)phenoxy-2-hydroxy-1-propyl]-N,N-bis(3-aminopropyl)quaternary ammonium salts 失效N，N-二烷基-N-氨基烷基-N-（氨基或硝基）苯基烷基和N-甲基-N- [3-（氨基或硝基）苯氧基-2-羟基-1-丙基] -N， （3-氨基丙基）季铵盐
公开(公告)号：US4206144A
公开(公告)日：1980-06-03
申请号：US963031
申请日：1978-11-22
CPC分类号： C09B44/02
摘要： N,N-Dialkyl-N-aminoalkyl-N-aminophenylalkyl quaternary ammonium salts and N-methyl-N-(3-aminophenoxy-2-hydroxy-1-propyl)-N,N-bis(3-aminopropyl) quaternary ammonium salts and their N-nitrophenylalkyl and N-(3-nitrophenoxy) precussor quaternary ammonium salts, respectively are intermediates to water-soluble azo-dyestuffs useful for coloring natural fibers, synthetic fiber-forming materials and cellulosic materials. These dyes dye cotton and paper various shades of yellows, reds, and oranges with less prone to bleed and with a high degree of discharge when bleached with hypochlorite or chlorine bleaches.
摘要翻译： N，N-二烷基-N-氨基烷基-N-氨基苯基烷基季铵盐和N-甲基-N-（3-氨基苯氧基-2-羟基-1-丙基）-N，N-双（3-氨基丙基）季铵盐 和它们的N-硝基苯基烷基和N-（3-硝基苯氧基）预混合季铵盐分别是可用于着色天然纤维，合成纤维形成材料和纤维素材料的水溶性偶氮染料的中间体。 这些染料染色棉花和纸张，黄色，红色和橙色的各种色调，不太容易出血，并且在用次氯酸盐或氯漂白剂漂白时会出现高度的放电。
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公开(公告)号：US4065500A
公开(公告)日：1977-12-27
申请号：US672428
申请日：1976-03-31
摘要： Water-soluble cationic dyestuffs of the formulae ##STR1## WHEREIN R.degree. is hydrogen, lower-alkyl or hydroxy-lower-alkyl;R.sup.1 is lower-alkyl, lower-alkenyl or hydroxy-lower-alkyl;R.sup.2 is lower-alkyl, lower-alkenyl, hydroxy-lower-alkyl or -(lower-alkylene)-NR.degree.Y or R.sup.1 and R.sup.2 together with the nitrogen atom, are pyrrolidino, piperidino or 4-lower-alkanoyl piperazino;Y is hydrogen or ##STR2## wherein R is hydrogen, lower-alkyl, lower-alkenyl, phenyl or phenyl-lower-alkyl;A is a member selected from the group consisting of an aromatic azo dyestuff residue attached to the quaternary ammonium nitrogen atom through a lower-alkylene bridge.k is a small integer whose value is dependent on the nature of A such that it has a range from one to two;R.sup.8 is lower-alkyl, lower-alkenyl or hydroxy-lower-alkyl;R.sup.9 is lower-alkyl, hydroxy-lower-alkyl or NH.sub.2 ;R.sup.10 is lower-alkyl or lower-alkenyl;A.sup.1 is an aromatic azo dyestuff residue attached to the quaternary ammonium nitrogen atom through a lower-alkylene bridge;g is a small integer whose value is dependent on the nature of A.sup.1 such that it has a range from one to two;R.sup.8' is lower alkyl;R.sup.9' is lower-alkyl, lower-alkenyl or hydroxy-lower-alkyl;R.sup.10' is lower-alkyl, lower-alkenyl or hydroxy-lower-alkyl or R.sup.9' and R.sup.10' together with the nitrogen atom are morpholino;A.sup.2 is an aromatic azo dyestuff residue attached to the quaternary ammonium nitrogen atom through a lower-alkylene bridge;h is a small integer whose value is dependent on the nature of A.sup.2 such that it has a range from one to two; andAn is an anionAre particularly useful for coloring natural fibers, synthetic fiber-forming materials and cellulosic materials. These dyes dye cotton and paper various shades of stable yellows, reds and oranges. The dyeing from these dyes on paper are less prone to bleed and have a high degree of color discharge when bleached with hypochlorite or chlorine bleaches.
摘要翻译： 下式的水溶性阳离子染料，其中R为氢，低级烷基或羟基 - 低级 - 烷基; R1是低级烷基，低级烯基或羟基 - 低级 - 烷基; R2是低级烷基，低级烯基，羟基 - 低级 - 烷基或 - （低级亚烷基）-NRYY或R1和R2与氮原子一起是吡咯烷子基，哌啶子基或4-低级烷酰基哌嗪子基; Y是氢或者其中R是氢，低级烷基，低级烯基，苯基或苯基 - 低级 - 烷基; A是选自通过低级亚烷基桥连接到季铵氮原子的芳族偶氮染料残基的成员。
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公开(公告)号：US3996282A
公开(公告)日：1976-12-07
申请号：US486180
申请日：1974-07-05
摘要： Water-soluble cationic dyestuffs of the formulae ##STR1## WHEREIN R.sup.0 is hydrogen, lower-alkyl or hydroxy-lower-alkyl;R.sup.1 is lower-alkyl, lower-alkenyl or hydroxy-lower-alkyl;R.sup.2 is lower-alkyl, lower-alkenyl, hydroxy-lower-alkyl or -(lower-alkylene)-NR.sup.0 Y or R.sup.1 and R.sup.2 together with the nitrogen atom, are pyrrolidino, piperidino or 4-lower-alkanoyl piperazino;Y is hydrogen or ##STR2## wherein R is hydrogen, lower-alkyl, lower-alkenyl, phenyl or phenyl-lower-alkyl;A is a member selected from the group consisting of an aromatic azo dyestuff residue attached to the quaternary ammonium nitrogen atom through a lower-alkylene bridge.K is a small integer whose value is dependent on the nature of A such that it has a range from one to two;R.sup.8 is lower-alkyl, lower-alkenyl or hydroxy-lower-alkyl;R.sup.9 is lower-alkyl, hydroxy-lower-alkyl or NH.sub.2 ;R.sup.10 is lower-alkyl or lower-alkenyl;A.sup.1 is an aromatic azo dyestuff residue attached to the quaternary ammonium nitrogen atom through a lower-alkylene bridge;g is a small integer whose value is dependent on the nature of A.sup.1 such that it has a range from one to two;R.sup.8.sup.' is lower-alkyl;R.sup.9.sup.' is lower-alkyl, lower-alkenyl or hydroxy-lower-alkyl;Rk.sup.10.sup.' is lower-alkyl, lower-alkenyl or hydroxy-lower-alkyl or R.sup.9.sup.' and R.sup.10.sup.' together with the nitrogen atom are morpholino;A.sup.2 is an aromatic azo dyestuff residue attached to the quaternary ammonium nitrogen atom through a lower-alkylene bridge;h is a small integer whose value is dependent on the nature of A.sup.2 such that it has a range from one to two; andAn is an anionAre particularly useful for coloring natural fibers, synthetic fiber-forming materials and cellulosic materials.
摘要翻译： 下式的水溶性阳离子染料：其中R 0为氢，低级烷基或羟基 - 低级 - 烷基; R1是低级烷基，低级烯基或羟基 - 低级 - 烷基; R2是低级烷基，低级烯基，羟基 - 低级 - 烷基或 - （低级亚烷基）-NR0Y或R1和R2与氮原子一起是吡咯烷子基，哌啶子基或4-低级烷酰基哌嗪子基; Y是氢或者其中R是氢，低级烷基，低级烯基，苯基或苯基 - 低级 - 烷基; A是选自通过低级亚烷基桥连接到季铵氮原子的芳族偶氮染料残基的成员。
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公开(公告)号：US3935182A
公开(公告)日：1976-01-27
申请号：US332511
申请日：1973-02-14
摘要： Water-soluble cationic dyestuffs of the formulae ##SPC1##WhereinR.sup.0 is hydrogen, lower-alkyl or hydroxy-lower-alkyl;R.sup.1 is lower-alkyl, lower-alkenyl or hydroxy-lower-alkyl;R.sup.2 is lower-alkyl, lower-alkenyl, hydroxy-lower-alkyl or -(lower-alkylene)-NRO Y or R.sup.1 and R.sup.2 together with the nitrogen atom, are pyrrolidino, piperidino or 4-lower-alkanoyl piperazino;Y is hydrogen or ##EQU1## wherein R is hydrogen, lower-alkyl, lower-alkenyl, phenyl or phenyl-lower-alkyl;A is a member selected from the group consisting of an aromatic azo dyestuff residue attached to the quaternary ammonium nitrogen atom through a lower-alkylene bridge.k is a small integer whose value is dependent on the nature or A such that it has a range from one to two;R.sup.8 is lower-alkyl, lower-alkenyl or hydroxy-lower-alkyl;R.sup.9 is lower-alkyl, hydroxy-lower-alkyl or NH.sub.2 ;R.sup.10 is lower-alkyl or lower-alkenyl;A.sup.1 is an aromatic azo dyestuff residue attached to the quaternary ammonium nitrogen atom through a lower-alkylene bridge;g is a small integer whose value is dependent on the nature of A.sup.1 such that it has a range from one to two;R.sup.8.sup.' is lower-alkyl;R.sup.9.sup.' is lower-alkyl, lower alkenyl or hydroxy-lower-alkyl;R.sup.10.sup.' is lower-alkyl, lower -alkenyl or hydroxy-lower-alkyl or R.sup.9.sup.' and R.sup.10.sup.' together with the nitrogen atom are morpholino;A.sup.2 is an aromatic azo dyestuff residue attached to the quaternary ammonium nitrogen atom through a lower-alkylene bridge;h is a small integer whose value is dependent on the nature of A.sup.2 such that it has a range from one to two; andAn is an anionAre particularly useful for coloring natural fibers, synthetic fiber-forming materials and cellulosic materials.
摘要翻译： 式WHEREIN R0为氢，低级烷基或羟基 - 低级 - 烷基的水溶性阳离子染料; R1是低级烷基，低级烯基或羟基 - 低级 - 烷基; R2是低级烷基，低级烯基，羟基 - 低级 - 烷基或 - （低级亚烷基）-NROY或R1和R2与氮原子一起是吡咯烷子基，哌啶子基或4-低级烷酰基哌嗪子基; Y是氢或O并原-C-R，其中R是氢，低级烷基，低级烯基，苯基或苯基 - 低级 - 烷基; A是选自通过低级亚烷基桥连接到季铵氮原子的芳族偶氮染料残基的成员。
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5.发明授权Azo dyestuff intermediate nitro- or aminobenzenes ring-substituted by a quaternized amine alkyl or amino-alkoxy group 失效偶氮染料中间体被季铵化的烷基或氨基 - 烷氧基环取代的硝基或氨基苯
公开(公告)号：US4146558A
公开(公告)日：1979-03-27
申请号：US839975
申请日：1977-10-06
IPC分类号： C09B44/02 , C09B47/32 , C07C85/02 , C07C87/30 , C07C103/54
摘要： Water-soluble cationic dyestuffs of the formulae ##STR1## WHEREIN R.sup.0 is hydrogen, lower-alkyl or hydroxy-lower-alkyl;R.sup.1 is lower-alkyl, lower-alkenyl or hydroxy-lower-alkyl;R.sup.2 is lower-alkyl, lower-alkenyl, hydroxy-lower-alkyl or -(lower-alkylene)-NR.sup.0 Y or R.sup.1 and R.sup.2 together with the nitrogen atom, are pyrrolidino, piperidino or 4-lower-alkanoyl piperazino;Y is hydrogen or ##STR2## wherein R is hydrogen, lower-alkyl, lower-alkenyl, phenyl or phenyl-lower-alkyl;A is a member selected from the group consisting of an aromatic azo dyestuff residue attached to the quaternary ammonium nitrogen atom through a lower-alkylene bridge.K is a small integer whose value is dependent on the nature of A such that it has a range from one to two;R.sup.8 is lower-alkyl, lower-alkenyl or hydroxy-lower-alkyl;R.sup.9 is lower-alkyl, hydroxy-lower-alkyl or NH.sub.2 ;R.sup.10 is lower-alkyl or lower-alkenyl;A.sup.1 is an aromatic azo dyestuff residue attached to the quaternary ammonium nitrogen atom through a lower-alkylene bridge;G is a small integer whose value is dependent on the nature of A.sup.1 such that it has a range from one to two;R.sup.8 ' is lower-alkyl;R.sup.9 ' is lower-alkyl, lower-alkenyl or hydroxy-lower-alkyl;R.sup.10 ' is lower-alkyl, lower-alkenyl or hydroxy-lower-alkyl or R.sup.9 ' and R.sup.10 ' together with the nitrogen atom are morpholino;A.sup.2 is an aromatic azo dyestuff residue attached to the quaternary ammonium nitrogen atom through a lower-alkylene bridge;h is a small integer whose value is dependent on the nature of A.sup.2 such that it has a range from one to two; andAn is an anionare particularly useful for coloring natural fibers, synthetic fiber-forming materials and cellulosic materials. These dyes dye cotton and paper various shades of stable yellows, reds and oranges. The dyeing from these dyes on paper are less prone to bleed and have a high degree of color discharge when bleached with hypochlorite or chlorine bleaches.
摘要翻译： 下式的水溶性阳离子染料：其中R 0为氢，低级烷基或羟基 - 低级 - 烷基; R1是低级烷基，低级烯基或羟基 - 低级 - 烷基; R2是低级烷基，低级烯基，羟基 - 低级 - 烷基或 - （低级亚烷基）-NR0Y或R1和R2与氮原子一起是吡咯烷子基，哌啶子基或4-低级烷酰基哌嗪子基; Y是氢或
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公开(公告)号：US4103092A
公开(公告)日：1978-07-25
申请号：US595864
申请日：1975-07-14
CPC分类号： C09B44/02
摘要： Water-soluble cationic dyestuffs of the formulae ##STR1## WHEREIN R.sup.0 is hydrogen, lower-alkyl or hydroxy-lower-alkyl;R.sup.1 is lower-alkyl, lower-alkenyl or hydroxy-lower-alkyl;R.sup.2 is lower-alkyl, lower-alkenyl, hydroxy-lower-alkyl or -(lower-alkylene)-NR.sup.0 Y or R.sup.1 and R.sup.2 together with the nitrogen atom, are pyrrolidino, piperidino or 4-lower-alkanoyl piperazino;Y is hydrogen or ##STR2## wherein R is hydrogen, lower-alkyl, lower-alkenyl, phenyl or phenyl-lower-alkyl;A is a member selected from the group consisting of an aromatic azo dyestuff residue attached to the quaternary ammonium nitrogen atom through a lower-alkylene bridge.k is a small integer whose value is dependent on the nature or A such that it has a range from one to two;R.sup.8 is lower-alkyl, lower-alkenyl or hydroxy-lower-alkyl;R.sup.9 is lower-alkyl, hydroxy-lower-alkyl or NH.sub.2 ;R.sup.10 is lower-alkyl or lower-alkenyl;A.sup.1 is an aromatic azo dyestuff residue attached to the quaternary ammonium nitrogen atom through a lower-alkylene bridge;g is a small integer whose value is dependent on the nature of A.sup.1 such that it has a range from one to two;R.sup.8' is lower-alkyl;R.sup.9' is lower-alkyl, lower-alkenyl or hydroxy-lower-alkyl;R.sup.10' is lower-alkyl, lower-alkenyl or hydroxy-lower-alkyl or R.sup.9' and R.sup.10' together with the nitrogen atom are morpholino;A.sup.2 is an aromatic azo dyestuff residue attached to the quaternary ammonium nitrogen atom through a lower-alkylene bridge;h is a small integer whose value is dependent on the nature of A.sup.2 such that it has a range from one to two; andAn is an anionAre particularly useful for coloring natural fibers, synthetic fiber-forming materials and cellulosic materials. These dyes dye cotton and paper various shades of stable yellows, reds and oranges. The dyeing from these dyes on paper are less prone to bleed and have a high degree of color discharge when bleached with hypochlorite or chlorine bleaches.
摘要翻译： 下式的水溶性阳离子染料：其中R 0为氢，低级烷基或羟基 - 低级 - 烷基; R1是低级烷基，低级烯基或羟基 - 低级 - 烷基; R2是低级烷基，低级烯基，羟基 - 低级 - 烷基或 -
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公开(公告)号：US4451657A
公开(公告)日：1984-05-29
申请号：US94794
申请日：1979-11-16
申请人： Nathan N. Crounse , Paul J. Schmidt
发明人： Nathan N. Crounse , Paul J. Schmidt
IPC分类号： B41M5/136 , B41M5/145 , B41M5/323 , C07D209/12 , C07D209/14 , C07D209/18 , C07D307/58 , C07D307/94 , C07D405/14
CPC分类号： C07D405/14 , B41M5/136 , B41M5/145 , B41M5/323 , C07D209/12 , C07D209/14 , C07D209/18 , C07D307/58 , C07D307/94
摘要： Mono-, bis- and tris-indolyl-substituted furanones useful as color formers, particularly in carbonless duplicating and thermal marking systems, which are prepared respectively by: the interaction of an indole with mucochloric acid; the interaction of an indole with a 4-mono(indolyl-substituted 4-oxo-2-butenoic acid; and by the interaction of an indole with a 2,4-bis(indolyl)-substituted 4-oxobutanoic acid or with a 3,5-bis(indolyl)-substituted furanone.
摘要翻译： 单 - ，双 - 和三 - 吲哚基取代的呋喃酮可用作成色剂，特别是在无碳复制和热标记体系中，其分别通过以下制备：吲哚与粘多氯酸的相互作用; 吲哚与4-单（吲哚基取代的4-氧代-2-丁烯酸）的相互作用;以及吲哚与2,4-双（吲哚基）取代的4-氧代丁酸或3 ，5-双（吲哚基）取代的呋喃酮。
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公开(公告)号：US4448722A
公开(公告)日：1984-05-15
申请号：US423932
申请日：1982-09-27
申请人： Nathan N. Crounse
发明人： Nathan N. Crounse
CPC分类号： C09B69/06 , C09B47/26 , C09B67/0032 , D21H21/28
摘要： Storage-stable aqueous compositions containing dissolved water-soluble novel acid addition salts of poly(N-substituted sulfonamido) phthalocyanines which are prepared by the interaction of a single acid or a mixture of acids and poly(N-substituted sulfonamido) phthalocyanines, are useful for direct dyeing, particularly the dyeing of cellulose.
摘要翻译： 通过单一酸或酸与聚（N-取代亚磺酰氨基）酞菁的混合物的相互作用制备的含有溶解的水溶性聚（N-取代亚磺酰氨基）酞菁新型酸加成盐的储存稳定含水组合物是有用的 用于直接染色，特别是染色纤维素。
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公开(公告)号：US4412950A
公开(公告)日：1983-11-01
申请号：US361187
申请日：1982-03-24
申请人： Nathan N. Crounse
发明人： Nathan N. Crounse
IPC分类号： C09B29/01 , C09B29/15 , C09B31/06 , C09B33/147 , C09B33/153 , C09B35/227 , C09B46/00
CPC分类号： C09B33/147 , C09B29/0003 , C09B29/103 , C09B31/061 , C09B33/153 , C09B35/227
摘要： This invention relates to novel (N-substituted sulfonamido) monoazo and disazo compounds, to acid-addition salts of said azo compounds which are useful as direct dyes particularly in the dyeing of cellulose, to novel (N-substituted sulfonamido) substituted nitrobenzene, aniline and acetanilide intermediates to said azo compounds and to methods of preparation of said azo compounds and said intermediates to said azo compounds.
摘要翻译： 本发明涉及新的（N-取代的磺酰氨基）单偶氮和双偶氮化合物，所述偶氮化合物的酸加成盐可用作特别是染色纤维素的直接染料，用于新的（N-取代的磺酰氨基）取代的硝基苯，苯胺 以及所述偶氮化合物的乙酰苯胺中间体以及所述偶氮化合物和所述中间体对所述偶氮化合物的制备方法。
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公开(公告)号：US4379088A
公开(公告)日：1983-04-05
申请号：US293393
申请日：1981-08-17
申请人： Nathan N. Crounse
发明人： Nathan N. Crounse
CPC分类号： C09B29/103 , C09B35/18 , C09B35/28
摘要： This invention relates to novel mixtures consisting essentially of monoazo compounds and disazo compounds which are substituted with x (N-substituted sulfonamido) groups, to acid-addition salts of said azo compounds, useful as direct dyes particularly in the dyeing of cellulose, and to methods of preparation of said mixtures of (N-substituted sulfonamido) substituted monoazo and disazo compounds.
摘要翻译： 本发明涉及基本上由单偶氮化合物和被x（N-取代的亚磺酰氨基）取代的二重氮化合物，所述偶氮化合物的酸加成盐，特别是在纤维素染色中用作直接染料的新型混合物，以及 所述（N-取代亚磺酰氨基）取代的单偶氮和双偶氮化合物的混合物的制备方法。
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