Separation of sulphonic acids from the medium in which they are prepared
    1.
    发明授权
    Separation of sulphonic acids from the medium in which they are prepared 失效
    从制备它们的介质中分离出磺酸

    公开(公告)号:US4233236A

    公开(公告)日:1980-11-11

    申请号:US972726

    申请日:1978-12-26

    CPC分类号: C07C303/42

    摘要: A process for the separation of sulphonated paraffins from their sulphonation medium, which comprises neutralization of the sulphuric acid present and separation into two phases, the lower phase containing the sulphate. The neutralization is carried out in such a way that only a part of the sulphuric acid is neutralized. A hydrocarbon is added, which dissolves the sulphonated and non-sulphonated paraffins and forms with water, an azeotropic mixture which is distilled in order to remove all or a part of the water present. The process allows the separation of sulphonates which are purer than in the past and which are poor in sulphates, while the sulphate layer contains only very little sulphonic acid.

    摘要翻译: 从其磺化介质中分离磺化石蜡的方法,其包括中和存在的硫酸和分离成两相,含有硫酸盐的下层。 中和以这样的方式进行,即只有一部分硫酸被中和。 加入烃,其溶解磺化和非磺化的链烷烃并与水形成,共沸混合物被蒸馏以除去存在的全部或部分水。 该方法允许分离比过去更纯且硫酸盐不良的磺酸盐,而硫酸盐层仅含有极少量的磺酸。

    Method to prepare copolyesteramides for moulding
    3.
    发明授权
    Method to prepare copolyesteramides for moulding 失效
    制备共聚酯酰胺成型的方法

    公开(公告)号:US4115475A

    公开(公告)日:1978-09-19

    申请号:US704815

    申请日:1976-07-13

    申请人: Paul Foy Rene Kern

    发明人: Paul Foy Rene Kern

    IPC分类号: C08G69/00 C08G69/44 C08L77/00

    CPC分类号: C08G69/44

    摘要: A process for synthesizing sequence copolyesteramides with the general formulaOH [CO--A--COO--B--O].sub.n Hwhere A is a linear aliphatic polyamide sequence and B is a linear aliphatic copolyesteramide sequence, for use in producing moulded or extruded articles with good mechanical resistance at elevated temperature; the process consists of polycondensation of a linear aliphatic copolyesteramide with hydroxyl end-groups, with a molecular weight of between 1,000 and 10,000, and a polyamide with carboxyl end-groups, with a molecular weight of between 2,000 and 15,000.

    摘要翻译: 用于合成通式为OH [CO-A-COO-BO] n H的顺式共聚酯酰胺的方法,其中A为直链脂族聚酰胺序列,B为直链脂族共聚酯酰胺序列,用于生产具有良好机械性能的模制或挤出制品 高温阻力; 该方法由直链脂肪族共聚酯酰胺与羟基端基缩聚,分子量为1,000至10,000,和具有羧基端基的聚酰胺,分子量为2,000至15,000。