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公开(公告)号:US06336741B1
公开(公告)日:2002-01-08
申请号:US09597687
申请日:2000-06-19
申请人: Roger L. Blaine
发明人: Roger L. Blaine
IPC分类号: G01N2500
CPC分类号: G01G1/22 , G01N5/04 , G01N25/4833
摘要: A method for controlling a thermogravimetry experiment and for quantitatively determining kinetic constants for decomposition or volatilization reactions using periodic forcing (modulated) temperature functions. A temperature program having a linear part and a periodically varying part superimposed thereon is applied to a sample in a thermogravimetric analyzer. The resulting mass signal is deonvoluted, or separated, into one or more deconvoluted signals.
摘要翻译: 一种控制热重分析实验的方法,并使用周期性强制(调制)温度函数定量测定分解或挥发反应的动力学常数。 将具有直线部分和周期性变化部分重叠的温度程序应用于热重分析仪中的样品。 所得到的质量信号被解卷积或分离成一个或多个解卷积的信号。
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公开(公告)号:US6113261A
公开(公告)日:2000-09-05
申请号:US105238
申请日:1998-06-26
申请人: Roger L. Blaine
发明人: Roger L. Blaine
CPC分类号: G01G1/22 , G01N25/4833 , G01N5/04
摘要: A method for controlling a thermogravimetry experiment and for quantitatively determining kinetic constants for decomposition or volatilization reactions using periodic forcing (modulated) temperature functions. A temperature program having a linear part and a periodically varying part superimposed thereon is applied to a sample in a thermogravimetric analyzer. The resulting mass signal is deconvoluted, or separated, into one or more deconvoluted signals.
摘要翻译: 一种控制热重分析实验的方法,并使用周期性强制(调制)温度函数定量测定分解或挥发反应的动力学常数。 将具有直线部分和周期性变化部分重叠的温度程序应用于热重分析仪中的样品。 所得到的质量信号被解卷积或分离成一个或多个解卷积的信号。
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