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1.发明申请1,2-BIS-(4,7-DIMETHYL-1,4,7-TRIAZACYCLONON-1-YL)-ETHANE AND INTERMEDIATE FOR THE SYNTHESIS OF SAME 有权1,2-BIS-（4,7-二甲基-1,4,7-三唑烷-1-YL） - 乙烯和其合成中间体公开(公告)号：US20130261297A1
公开(公告)日：2013-10-03
申请号：US13808565
申请日：2011-07-05
申请人： Ronald Hage , Jean Hypolites Koek , Stephen William Russell , Lodewijk Van der Wolf , Jianrong Zhang , Wei Zhao , Xiaohong Wang
发明人： Ronald Hage , Jean Hypolites Koek , Stephen William Russell , Lodewijk Van der Wolf , Jianrong Zhang , Wei Zhao , Xiaohong Wang
IPC分类号： C07D255/02 , C07D403/06
CPC分类号： C07D255/02 , C07D403/06
摘要： The present invention provides improved processes for the synthesis of 1,4-ditosyl-1,4,7-triazacyclonone and protected analogues thereof, and to synthesise bis(triazacyclononane) ligands.
摘要翻译： 本发明提供了用于合成1,4-二硫代-1,4,7-三氮杂环壬酮及其保护的类似物的改进方法，以及合成双（三氮杂环壬烷）配体。
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2.发明授权1,2-bis-(4,7-dimethyl-1,4,7-triazacyclonon-1-yl)-ethane and intermediate for the synthesis of same 有权1,2-二 - （4,7-二甲基-1,4,7-三氮杂环壬烷-1-基） - 乙烷及其合成中间体公开(公告)号：US08907082B2
公开(公告)日：2014-12-09
申请号：US13808565
申请日：2011-07-05
申请人： Ronald Hage , Jean Hypolites Koek , Stephen William Russell , Lodewijk Van der Wolf , Jianrong Zhang , Wei Zhao , Xiaohong Wang
发明人： Ronald Hage , Jean Hypolites Koek , Stephen William Russell , Lodewijk Van der Wolf , Jianrong Zhang , Wei Zhao , Xiaohong Wang
IPC分类号： C07D255/02 , C07D403/06
CPC分类号： C07D255/02 , C07D403/06
摘要： The present invention provides improved processes for the synthesis of 1,4-ditosyl-1,4,7-triazacyclonone, comprising deprotecting a compound of formula (C): wherein P is tosylate or arylsulfonate, with an acidic medium to form 1,2-bis(1,4,7-triazacyclonon-1-yl)-ethane; and subsequently adding formaldehyde and formic acid to the acidic medium to form 1,2-bis-(4,7-dimethyl-1,4,7-triazacyclonon-1-yl)-ethane (Me4-DTNE). The syntheses of intermediates are also disclosed.
摘要翻译： 本发明提供了合成1,4-二硫代-1,4,7-三氮杂环辛酮的改进方法，包括使式（C）化合物（其中P为甲苯磺酸酯或芳基磺酸酯）与酸性介质脱保护形成1,2 （1,4,7-三氮杂环壬烷-1-基） - 乙烷; 随后向酸性介质中加入甲醛和甲酸，形成1,2-双 - （4,7-二甲基-1,4,7-三氮杂环壬烷-1-基） - 乙烷（Me4-DTNE）。 还公开了中间体的合成。
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公开(公告)号：US06140294A
公开(公告)日：2000-10-31
申请号：US433157
申请日：1999-11-03
申请人： Michel Gilbert Delroisse , Bernard Lucas Feringa , Ronald Hage , Roelant Mathijs Hermant , Robertus Everardus Kalmeijer , Jean Hypolites Koek , Christiaan Lamers , Minze Theunis Rispens , Stephen William Russell , Ronaldus Theodorus Vliet , Jane Whittaker
发明人： Michel Gilbert Delroisse , Bernard Lucas Feringa , Ronald Hage , Roelant Mathijs Hermant , Robertus Everardus Kalmeijer , Jean Hypolites Koek , Christiaan Lamers , Minze Theunis Rispens , Stephen William Russell , Ronaldus Theodorus Vliet , Jane Whittaker
IPC分类号： B01J31/18 , C07F1/00 , C07F1/08 , C07F13/00 , C07F15/02 , C11D3/39 , C11D3/395 , D06L3/02 , C11D7/18 , C11D7/54
CPC分类号： D06L3/021 , B01J31/1815 , C07F1/005 , C07F13/005 , C07F15/025 , C11D3/3932 , B01J2531/16 , B01J2531/72 , B01J2531/842
摘要： A bleach and oxidation catalyst is provided comprising a catalytically ace iron, manganese or copper complex including a specified pentadentate nitrogen-containing ligand. The metal complex can activate hydrogen peroxide or peroxyacids and provides favourable stain removal properties. In addition, a considerably improved stability of these metal complex compounds in alkaline aqueous environment has been obtained, in particular at the peroxy compound concentrations generally present in the fabric washing liquor.
摘要翻译： 提供了一种漂白和氧化催化剂，其包含催化活性的铁，锰或铜络合物，包括指定的五齿配体含氮配体。 金属络合物可以活化过氧化氢或过氧酸，并提供有利的去污性能。 此外，已经获得了这些金属络合物在碱性水性环境中的显着提高的稳定性，特别是在织物洗涤液中通常存在的过氧化合物浓度。
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4.发明授权
公开(公告)号：US6165963A
公开(公告)日：2000-12-26
申请号：US433156
申请日：1999-11-03
申请人： Michel Gilbert Delroisse , Bernard Lucas Feringa , Ronald Hage , Roelant Mathijs Hermant , Robertus Everardus Kalmeijer , Jean Hypolites Koek , Christiaan Lamers , Minze Theunis Rispens , Stephen William Russell , Ronaldus Theodorus Vliet , Jane Whittaker
发明人： Michel Gilbert Delroisse , Bernard Lucas Feringa , Ronald Hage , Roelant Mathijs Hermant , Robertus Everardus Kalmeijer , Jean Hypolites Koek , Christiaan Lamers , Minze Theunis Rispens , Stephen William Russell , Ronaldus Theodorus Vliet , Jane Whittaker
CPC分类号： C11D3/3932
摘要： A detergent bleaching composition is provided comprising a compound inclug a specified pentadentate nitrogen-containing ligand. The compound can activate hydrogen peroxide or peroxyacids and provides favourable stain removal properties, particularly in the presence or iron, manganese or copper ions. In addition, an improved stability in alkaline aqueous environment has been obtained, in particular at the peroxy compound concentrations generally present in the fabric washing liquor.
摘要翻译： 提供了一种洗涤剂漂白组合物，其包含包含特定的五价含氮配体的化合物。 该化合物可以活化过氧化氢或过氧酸，并提供有利的去污性能，特别是在存在或铁，锰或铜离子的情况下。 此外，已经获得了在碱性水性环境中改善的稳定性，特别是在织物洗涤液中通常存在的过氧化合物浓度。
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公开(公告)号：US06605580B2
公开(公告)日：2003-08-12
申请号：US09741393
申请日：2000-12-20
申请人： Dirk Johannes Bijl , Ronald Hage , Jan Kevelam , Jean Hypolites Koek , Dennis Stephen Murphy , Irene Erica Smit , Johannes Jacob Verhagen , Pieter van der Vlist
发明人： Dirk Johannes Bijl , Ronald Hage , Jan Kevelam , Jean Hypolites Koek , Dennis Stephen Murphy , Irene Erica Smit , Johannes Jacob Verhagen , Pieter van der Vlist
IPC分类号： C11D100
CPC分类号： C11D3/43 , C11D3/02 , C11D3/3953 , C11D3/3956 , D06L4/13 , D06L4/17 , D06L4/23 , D06L4/24
摘要： A bleaching composition is provided comprising a) a bleach-effective amount of an inorganic bleaching agent; b) a bleach-compatible solvent c) 0 to 10 wt % of a surfactant; d) less than 10 wt % of a modifier; and e) an effective dry cleaning amount of densified carbon dioxide, said composition being essentially free of organic peracid or precursor thereof.
摘要翻译： 提供漂白组合物，其包含a）漂白有效量的无机漂白剂; b）漂白剂相容的溶剂c）0-10重量％的表面活性剂; d）小于10重量％的改性剂; 和），有效干洗量的致密二氧化碳，所述组合物基本上不含有机过酸或其前体。
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公开(公告)号：US08455423B2
公开(公告)日：2013-06-04
申请号：US13177458
申请日：2011-07-06
CPC分类号： B01J31/22 , B01J31/182 , B01J2231/70 , B01J2531/72 , C11D3/3932 , D06L4/12 , D21C9/1036 , D21C9/163
摘要： An aqueous solution of a water soluble salt of a preformed transition metal catalyst together with hydrogen peroxide is disclosed. The composition is useful in bleaching a variety of substrates.
摘要翻译： 公开了预先形成的过渡金属催化剂的水溶性盐与过氧化氢的水溶液。 该组合物可用于漂白各种底物。
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7.发明授权Bleaching composition for dry cleaning containing transition metal bleach catalyst 失效含有过渡金属漂白催化剂的漂白漂白组合物公开(公告)号：US06495502B2
公开(公告)日：2002-12-17
申请号：US09741394
申请日：2000-12-20
申请人： Dirk Johannes Bijl , Ronald Hage , Jan Kevelam , Jean Hypolites Koek , Dennis Stephen Murphy , Irene Erica Smit , Johannes J. Verhagen , Pieter van der Vlist
发明人： Dirk Johannes Bijl , Ronald Hage , Jan Kevelam , Jean Hypolites Koek , Dennis Stephen Murphy , Irene Erica Smit , Johannes J. Verhagen , Pieter van der Vlist
IPC分类号： C11D326
CPC分类号： C11D3/3947 , C11D1/82 , C11D3/168 , C11D3/3932 , D06L4/15 , D06L4/17
摘要： A bleaching composition is provided for effective bleaching with a bleach catalyst at low temperatures. The bleaching composition comprises of a) from 0.05 microM to 50 mM of an organic substance which forms a complex with a transition metal; b) a source of active oxygen corresponding to 0.05 to 100 mM of active oxygen; and c) an effective amount of liquid carbon dioxide, preferably held at 25° C. or less.
摘要翻译： 提供漂白组合物用于在低温下用漂白催化剂进行有效漂白。 漂白组合物包含a）0.05微米至50毫摩尔的与过渡金属形成络合物的有机物质; b）相当于0.05至100mM活性氧的活性氧源; 和c）有效量的液体二氧化碳，优选保持在25℃或更低。
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8.发明授权Bleaching composition for dry cleaning containing transition metal bleach catalyst 失效含有过渡金属漂白催化剂的漂白漂白组合物公开(公告)号：US06479447B2
公开(公告)日：2002-11-12
申请号：US09741392
申请日：2000-12-20
申请人： Dirk Johannes Bijl , Ronald Hage , Jan Kevelam , Jean Hypolites Koek , Dennis Stephen Murphy , Irene Erica Smit , Johannes J. Verhagen , Pieter van der Vlist
发明人： Dirk Johannes Bijl , Ronald Hage , Jan Kevelam , Jean Hypolites Koek , Dennis Stephen Murphy , Irene Erica Smit , Johannes J. Verhagen , Pieter van der Vlist
IPC分类号： C11D326
CPC分类号： C11D3/3947 , C11D1/82 , C11D3/168 , C11D3/3932 , D06L4/15 , D06L4/17
摘要： A bleaching composition is provided for effective bleaching with a bleach catalyst at low temperatures. The bleaching composition comprises of a) from 0.05 microM to 50 mM of an organic substance which forms a complex with a transition metal; b) a source of active oxygen corresponding to 0.05 to 100 mM of active oxygen; and c) an effective amount of liquid carbon dioxide.
摘要翻译： 提供漂白组合物用于在低温下用漂白催化剂进行有效漂白。 漂白组合物包含a）0.05微米至50毫摩尔的与过渡金属形成络合物的有机物质; b）相当于0.05至100mM活性氧的活性氧源; 和c）有效量的液体二氧化碳。
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公开(公告)号：US20110275510A1
公开(公告)日：2011-11-10
申请号：US13177458
申请日：2011-07-06
IPC分类号： B01J31/22
CPC分类号： B01J31/22 , B01J31/182 , B01J2231/70 , B01J2531/72 , C11D3/3932 , D06L4/12 , D21C9/1036 , D21C9/163
摘要： An aqueous solution of a water soluble salt of a preformed transition metal catalyst together with hydrogen peroxide is disclosed. The composition is useful in bleaching a variety of substrates.
摘要翻译： 公开了预先形成的过渡金属催化剂的水溶性盐与过氧化氢的水溶液。 该组合物可用于漂白各种底物。
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公开(公告)号：US20090205143A1
公开(公告)日：2009-08-20
申请号：US11920787
申请日：2006-04-26
CPC分类号： B01J31/22 , B01J31/182 , B01J2231/70 , B01J2531/72 , C11D3/3932 , D06L4/12 , D21C9/1036 , D21C9/163
摘要： The present invention concerns bleaching of substrates with an aqueous solution of a water soluble salt of a preformed transition metal catalyst together with hydrogen peroxide.
摘要翻译： 本发明涉及用预先形成的过渡金属催化剂的水溶性盐与过氧化氢的水溶液漂洗底物。
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