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1.发明授权Dye mixture comprising water-soluble fiber-reactive azo dyes, preparation thereof and use thereof 失效包含水溶性纤维反应性偶氮染料的染料混合物，其制备及其用途
公开(公告)号：US6136045A
公开(公告)日：2000-10-24
申请号：US372123
申请日：1999-08-11
IPC分类号： C09B62/51 , C09B62/44 , C09B67/22 , D06P1/38 , D06P3/04 , D06P3/10 , D06P3/58 , D06P3/66 , C09B67/24 , D06P1/382 , D06P1/384
CPC分类号： C09B62/4413 , C09B67/0052 , D06P1/38 , Y10S8/918
摘要： The present invention relates to dye mixtures comprising one or more azo dyes of the general formula (1) and one or more azo dyes of the general formula (2) ##STR1## where p is 1 or 2,R.sub.1, R.sup.1' and R.sup.2 are independently hydrogen or a group of the general formula SO.sub.3 M or OCH.sub.3,R.sup.5 and R.sup.6 are independently hydrogen or C.sub.1 -C.sub.4 alkyl,X.sup.1 and X.sup.2 are independently fluorine or chlorine or a grouping of the general formula NR.sup.3 R.sup.4 or OR.sup.3,R.sup.3 is hydrogen, C.sub.1 -C.sub.4 alkyl or optionally substituted aryl,R.sup.4 has one of the meanings of R.sup.3 or is aryl or alkyl (which may be substituted by SO.sub.2 Y, SO.sub.3 M or OCH.sub.3), optionally substituted morpholino or pyrimidino or NHCN,Y, Y.sup.1 and Y.sup.2 are independently vinyl or a grouping of the general formula CH.sub.2 CH.sub.2 Z,Z is a grouping which can be eliminated by the action of alkali, andM is a hydrogen atom, an ammonium ion or the equivalent of an alkali or alkaline earth metal,their preparation and their use for dyeing or printing hydroxyl- and/or carboxamido-containing material.
摘要翻译： 本发明涉及包含一种或多种通式（1）的偶氮染料和一种或多种通式（2）的偶氮染料的染料混合物，其中p为1或2，R 1，R 1'和R 2独立地为氢或 通式为SO 3 M或OCH 3，R 5和R 6的基团独立地为氢或C 1 -C 4烷基，X 1和X 2独立地为氟或氯或通式为NR 3 R 4或OR 3的基团，R 3为氢，C 1 -C 4烷基或 任选取代的芳基，R 4具有R 3的含义之一，或者是芳基或烷基（其可以被SO 2 Y，SO 3 M或OCH 3取代），任选取代的吗啉代或嘧啶基或NHCN，Y，Y 1和Y 2分别是乙烯基或 通式为CH 2 CH 2 Z，Z为可通过碱作用而除去的基团，M为氢原子，铵离子或碱金属或碱土金属当量，它们的制备及其用于染色或印刷羟基的用途 - 和/或含甲酰氨基的材料。
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2.发明授权Orange dye mixtures of fiber-reactive azo dyes and use thereof for dyeing material containing hydroxy-and/or carboxamido groups 有权纤维反应性偶氮染料的橙色染料混合物及其用于含有羟基和/或羧酰氨基的染色材料的用途
公开(公告)号：US5931976A
公开(公告)日：1999-08-03
申请号：US132318
申请日：1998-08-11
申请人： Ronald P. Pedemonte , Werner Russ
发明人： Ronald P. Pedemonte , Werner Russ
摘要： The present invention concerns orange dye mixtures of fiber-reactive azo dyes, suitable for dyeing hydroxy- and/or carboxamido-containing material, such as cellulose fibers, like cotton, or wool and nylon, which comprise one or more monoazo dyestuffs corresponding to the general formula (1) and one or more monoazo dyestuffs corresponding to the formula (2) ##STR1## in which D.sub.1 and D.sub.2 are each, independently from one another, a radical of a benzene or naphthalene nucleus, R.sub.1, R.sub.2, R.sub.3 and R.sub.4 are each, independently from one another, hydrogen, methyl, ethyl, methoxy, ethoxy, sulfo or carboxy, M is hydrogen or an alkali metal and the groups Y.sub.1 --SO.sub.2 -- and Y.sub.2 --SO.sub.2 -- are each fiber reactive groups of the vinylsulfone series.
摘要翻译： 本发明涉及适用于染色含羟基和/或羧酰氨基的材料的纤维反应性偶氮染料的橙色染料混合物，例如纤维素纤维，如棉，或羊毛和尼龙，其包含一种或多种对应于 通式（1）和对应于式（2）的一种或多种单偶氮染料，其中D1和D2各自独立地为苯或萘核的基团，R1，R2，R3和R4各自为 氢，甲基，乙基，甲氧基，乙氧基，磺基或羧基，M为氢或碱金属，Y1-SO2-和Y2-SO2-基团均为乙烯基砜系列的纤维反应性基团。
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公开(公告)号：US5811529A
公开(公告)日：1998-09-22
申请号：US816758
申请日：1997-03-07
IPC分类号： C09B62/01 , C09B62/25 , C09B62/44 , C09B62/513 , C07C245/06
CPC分类号： C09B62/25 , C09B62/01 , C09B62/4415 , C09B62/513
摘要： A fiber reactive dye having the formula ##STR1## wherein R.sub.1 and R.sub.3 are independently selected from the group consisting of; hydrogen; an alkyl group having from one to four carbon atoms; the foregoing alkyl group further substituted with one or more groups selected from hydroxy; amino; sulfo; halogen; an aryl radical; a heterocyclic radical or combination thereof; where for R.sub.3 said amino group maybe further substituted by a nitrogen heterocyclic fiber reactive group of the series: 1, 3, 5 mono or dichloro triazinyl; 1, 3, 5 mono or difluoro triazinyl; trichloropyrimidinyl; difluoropyrimidinyl; or monochlorodifluoro pyrimidinyl; where the nitrogen heterocycle may be further substituted by an: alkyl; or aryl amino group; wherein B is selected from the group consisting of a C.sub.2 to C.sub.4 alkyl chain; a substituted aryl or a heterocyclic radical; wherein X is selected from the group consisting of SO.sub.3 H; SO.sub.3 Na or a hydroxy group; and wherein Q.sub.1 and Q.sub.2 are independently selected from diazo components.
摘要翻译： 一种具有式“IMAGE”的纤维活性染料，其中R 1和R 3独立地选自： 氢; 具有1-4个碳原子的烷基; 前述烷基还被一个或多个选自羟基的基团取代; 氨基; 磺基 卤素; 芳基; 杂环基或其组合; 对于R3，所述氨基可以进一步被该系列的氮杂环纤维反应性基团取代：1,3,5-单或二氯三嗪基; 1,3,5-单或二氟三嗪基; 三氯嘧啶基; 二氟嘧啶基 或一氯二氟嘧啶基; 其中氮杂环可以进一步被烷基取代; 或芳基氨基; 其中B选自C2-C4烷基链; 取代的芳基或杂环基; 其中X选自SO 3 H; SO 3 Na或羟基; 并且其中Q1和Q2独立地选自重氮组分。
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4.发明授权Reactive azo dyes having a permanent quaternary ammonium group and a fiber-reactive group 失效具有永久性季铵基团和纤维反应性基团的活性偶氮染料
公开(公告)号：US5932708A
公开(公告)日：1999-08-03
申请号：US71391
申请日：1998-05-01
IPC分类号： C09B62/006 , C09B62/01 , C09B62/08 , C09B62/24 , C09B62/44 , C09B62/507 , C09B69/00 , C09B62/09
CPC分类号： C09B62/24 , C09B62/006 , C09B62/01 , C09B62/08 , C09B62/4411 , C09B62/507 , C09B69/001
摘要： Fiber-reactive monoazo and disazo dyes, suitable for dyeing cellulose material, such as cotton, and also synthetic or natural polyamide material, such as wool, in high color depth and with good fastness properties, are described which contain a quaternary ammonium group, such as a trialkylammonium group, and contain, as a fiber-reactive group, a group of the vinyl-sulfone series, or a grouping containing a group of the vinyl-sulfone series, or a heterocyclic fiber-reactive group selected from a halogeno-substituted pyrimidine or triazine.
摘要翻译： 描述了适用于染色纤维素材料如棉花的纤维反应性单偶氮和双偶氮染料，以及高颜色深度和良好牢度性质的合成或天然聚酰胺材料如羊毛，其含有季铵基团 作为三烷基铵基团，并且作为纤维反应性基团含有一组乙烯基砜系列或包含一组乙烯基砜系列的组或选自卤代取代的杂环纤维反应性基团 嘧啶或三嗪。
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公开(公告)号：US06319291B1
公开(公告)日：2001-11-20
申请号：US09492099
申请日：2000-01-27
申请人： Ronald P. Pedemonte
发明人： Ronald P. Pedemonte
IPC分类号： D06P1382
CPC分类号： D06P1/38 , C09B67/0057 , Y10S8/918
摘要： The present invention relates to dye mixtures comprising one or more disazo dyes conforming to the formula (1) and one or more monoazo dyes corforming to the formula (2) wherein the variables are described in the specification.
摘要翻译： 本发明涉及包含符合式（1）的一种或多种二重氮染料和一种或多种与式（2）一致的单偶氮染料的染料混合物，其中变量在说明书中描述。
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公开(公告)号：US5973178A
公开(公告)日：1999-10-26
申请号：US77217
申请日：1998-05-20
IPC分类号： C07C317/36 , C07F9/09 , C07C305/12
CPC分类号： C07C317/36 , C07F9/091
摘要： A compound of the formula: ##STR1## wherein: A is hydrogen, a substituted or unsubstituted C.sub.1 to C.sub.4 alkyl, a substituted or unsubstituted C.sub.1 to C.sub.4 alkoxy or a substituted or unsubstituted phenyl;W is a substituted or unsubstituted phenylene or a substituted or unsubstituted naphthylene;Y is--CH.sub.2 --CH.sub.2 --Z wherein Z is selected from --OSO.sub.3 H, --SSO.sub.3 H, --OPO.sub.3 H, --OCOCH.sub.2 --Cll.sub.3, Cl, Br or F; andm is 1 or 2, e is 0 or 1,with the sum of e+m=2.
摘要翻译： PCT No.PCT / US96 / 15973 Sec。 371日期：1998年5月20日 102（e）日期1998年5月20日PCT提交1996年10月4日PCT公布。 第WO97 / 19047号公报 日期：1997年5月29日一种下式化合物：其中：A为氢，取代或未取代的C1至C4烷基，取代或未取代的C1至C4烷氧基或取代或未取代的苯基; W是取代或未取代的亚苯基或取代或未取代的亚萘基; Y是-CH 2 -CH 2 -Z，其中Z选自-OSO 3 H，-SSO 3 H，-OPO 3 H，-OCOCH 2 -C 13，Cl，Br或F; m为1或2，e为0或1，e + m = 2的和。
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公开(公告)号：US5409916A
公开(公告)日：1995-04-25
申请号：US77226
申请日：1993-06-14
IPC分类号： C09B62/44 , C07D251/52 , C07D251/70
CPC分类号： C09B62/4409
摘要： Fiber reactive dyes of the anthraquinone type which provide brilliant violet colors without metal complexing. These dyes may be represented by the formula: ##STR1## wherein W is selected from NR.sub.2 and oxygen;R is independently selected from hydrogen, C.sub.1 -C.sub.6 alkyl;C.sub.1 -C.sub.6 alkoxy, sulfo and carboxy;R.sub.1 is selected from hydrogen, C.sub.1 -C.sub.6 alkyl and phenyl;R.sub.2 is selected from hydrogen and C.sub.1 -C.sub.6 alkyl;R.sub.3 is selected from hydrogen, and C.sub.1 -C.sub.4 alkyl;n is an integer of 1 or 2; andY is CH.dbd.CH.sub.2, or CH.sub.2 CH.sub.2 Z wherein Z is a group capable of being split off by the action of an alkali reagent.
摘要翻译： 蒽醌类的纤维活性染料，无需金属络合即可提供辉煌的紫色。 这些染料可以由下式表示：其中W选自NR 2和氧; R独立地选自氢，C 1 -C 6烷基; C 1 -C 6烷氧基，磺基和羧基; R1选自氢，C1-C6烷基和苯基; R2选自氢和C1-C6烷基; R 3选自氢和C 1 -C 4烷基; n为1或2的整数; 并且Y是CH = CH 2或CH 2 CH 2 Z，其中Z是能够通过碱试剂的作用分裂的基团。
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8.发明授权Red-dyeing dye mixtures of water-soluble fiber-reactive azo dyes and their use 有权红染染料混合水溶性纤维反应偶氮染料及其用途
公开(公告)号：US6090163A
公开(公告)日：2000-07-18
申请号：US217355
申请日：1998-12-21
CPC分类号： C09B67/0047 , Y10S8/918 , Y10S8/924
摘要： Described are dye mixtures of dyes of the general formulae (1) and (2) ##STR1## where M is hydrogen, an alkali metal or the equivalent of an alkaline earth metal, R.sup.1, R.sup.2 and R.sup.3 are independently hydrogen or sulfo, X.sup.1 and X.sup.2, are independently chlorine, fluorine, hydroxy, alkoxy of 1 to 4 carbon atoms, optionally substituted phenyl, optionally substituted morpholino, optionally substituted pyrimidino, cyanoamino or an amino group of the formula --NR.sup.4 R.sup.5, where R.sup.4 is hydrogen, alkyl of 1 to 4 carbon atoms, unsubstituted or sulfo-substituted phenyl or unsubstituted or sulfo-substituted naphthyl, R.sup.5 is hydrogen, optionally substituted alkyl, which may be interrupted by oxy or amino, or optionally substituted phenyl or unsubstituted or sulfo-substituted naphthyl, or the group --NR.sup.4 R.sup.5 is the radical of an aliphatic heterocycle, the groups Y.sup.1 --SO.sub.2 --, Y.sup.2 --SO.sub.2 -- and Y.sup.3 --SO.sub.2 -- are each a fiber-reactive radical of the vinyl sulfone series and are attached to the benzene nucleus meta or para to the azo group.
摘要翻译： 描述了通式（1）和（2）的染料的染料混合物，其中M是氢，碱金属或碱土金属当量，R 1，R 2和R 3独立地是氢或磺基，X 1和X 2是 独立地是氯，氟，羟基，具有1至4个碳原子的烷氧基，任选取代的苯基，任选取代的吗啉代，任选取代的嘧啶基，氰基氨基或式-NR4R5的氨基，其中R4是氢，1至4个碳原子的烷基 ，未取代或磺基取代的苯基或未取代或磺基取代的萘基，R 5是氢，任选取代的烷基，其可以被氧基或氨基或任选取代的苯基或未取代或磺基取代的萘基中断，或者-NR4R5基团 脂族杂环基团，Y1-SO2-，Y2-SO2-和Y3-SO2-基团各自是乙烯基砜系列的纤维反应性基团，并连接到偶氮基团的间位或对位的苯核上。
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9.发明授权Deep black dye mixtures of fiber-reactive azo dyes and use thereof for dyeing hydroxy- and/or carboxamido-containing fiber material 失效纤维反应性偶氮染料的深黑色染料混合物及其用于染色含羟基和/或含羧酰氨基的纤维材料的用途
公开(公告)号：US5931974A
公开(公告)日：1999-08-03
申请号：US123603
申请日：1998-07-28
申请人： Ronald P. Pedemonte
发明人： Ronald P. Pedemonte
摘要： A dye mixture comprising one or more disazo dyes composed of 1-amino-3,6-disulfo-8-naphthol as the coupling component and of two diazo components of the aniline series containing each a fiber-reactive group of the vinylsulfone series, one or more monoazo dyes composed of a carboxy-substituted benzoylamino-sulfo-naphthol coupling component and a diazo component of the aniline series, containing a fiber-reactive group of the vinylsulfone series and optionally one or two monoazo dyes with 1-amino-3,6-disulfo-8-naphthol as a coupling component to which is coupled in the ortho-position to the amino group a diazo component of the aniline series substituted by a fiber-reactive group of the vinylsulfone series. The dye mixtures yield on hydroxy- and/or carboxamido-containing fiber materials, such as cellulose fibers, in particular cotton, or on, for example, wool and synthetic polyamide fibers, deep black dyeings.
摘要翻译： 一种染料混合物，其包含由1-氨基-3,6-二磺基-8-萘酚作为偶联组分的一种或多种二偶氮染料和包含乙烯基砜系列的纤维反应性基团的苯胺系列的两个重氮组分，一个 或更多的由羧基取代的苯甲酰基氨基 - 磺基 - 萘酚偶联组分和苯胺系列的重氮组分组成的单偶氮染料，其含有乙烯砜系列的纤维反应性基团和任选的一种或两种具有1-氨基-3的单偶氮染料， 6-二磺基-8-萘酚作为偶联组分，其邻位与氨基连接，由乙烯基砜系列的纤维反应性基团取代的苯胺系列的重氮组分。 染料混合物在含羟基和/或羧酰氨基的纤维材料上产生，例如纤维素纤维，特别是棉，或在例如羊毛和合成聚酰胺纤维，深黑色染色上。
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公开(公告)号：US5925745A
公开(公告)日：1999-07-20
申请号：US75569
申请日：1998-05-11
IPC分类号： C09B62/04 , C09B62/44 , C09B62/503 , C09B62/51 , C09B62/002
CPC分类号： C09B62/503 , C09B62/4403
摘要： A fiber-reactive dye corresponding to formula (1) ##STR1## in which: Fb is the radical of an azo dye, of a heavy metal complex azo dye, of a formazan dye, of a triphenodioxazine dye or of a phthalocyanine dye;U.sup.(+) is a permanent quaternary ammonium group;A.sup.(-) is a colorless anion, andR.sup.x, R.sub.4, G, Q and n are as defined in the specification, with the proviso that the dye contains at least one group of the vinylsulfone series, such as a group of the formula --SO.sub.2 Y, wherein Y is as defined in the specification, these dyes being capable of dyeing hydroxy- and/or carboxamido-containing fibres, such as cellulosic fibre and wool.
摘要翻译： 对应于式（1）的纤维活性染料，其中：Fb是偶氮染料，重金属络合偶氮染料，甲an染料，三苯并二嗪染料或酞菁染料的基团; U（+）是永久性季铵基团; A（ - ）是无色阴离子，Rx，R4，G，Q和n如说明书中所定义，条件是染料含有至少一组乙烯基砜系列，例如式 - SO 2 Y，其中Y如说明书中所定义，这些染料能够染色含有羟基和/或羧酰氨基的纤维，例如纤维素纤维和羊毛。
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