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公开(公告)号：US20120000475A1
公开(公告)日：2012-01-05
申请号：US13185160
申请日：2011-07-18
CPC分类号： A24D3/06 , A24B15/28 , A24B15/282 , A24B15/286 , A24B15/287 , A24B15/288 , A24D1/02 , A24D1/18 , A24D3/16 , B01D53/62 , B01D53/94 , B82Y30/00
摘要： A method of making composite nanoscale particles comprising subjecting a starting material to laser energy so as to form a vapor and condensing the vapor so as to form the composite nanoscale particles, wherein said composite nanoscale particles comprise a first metal and/or a first metal oxide incorporated in nanoscale particles of an oxide of a second metal, the first metal being different than the second metal. The starting material can comprise first and second metals or compounds of the first and second metals. The composite nanoscale particles can be formed in a reaction chamber wherein a temperature gradient is provided. The atmosphere in the chamber can be an inert atmosphere comprising argon or a reactive atmosphere comprising oxygen. The composite nanoscale particles are useful for low-temperature and near-ambient temperature catalysis. The composite nanoscale particles can be incorporated in the tobacco cut filler, cigarette paper and/or cigarette filter material of a cigarette to catalyze the oxidation of carbon monoxide to carbon dioxide.
摘要翻译： 一种制备复合纳米尺寸颗粒的方法，包括使起始材料经受激光能量以形成蒸气并使蒸气冷凝以形成复合纳米级颗粒，其中所述复合纳米级颗粒包含第一金属和/或第一金属氧化物 掺入第二金属的氧化物的纳米级颗粒中，第一金属不同于第二金属。 起始材料可以包括第一和第二金属或第一和第二金属的化合物。 复合纳米级颗粒可以在其中提供温度梯度的反应室中形成。 室中的气氛可以是包含氩气或包含氧的反应性气氛的惰性气氛。 复合纳米级颗粒可用于低温和近环境温度的催化。 复合纳米尺寸颗粒可以并入香烟的烟丝切割填料，香烟纸和/或卷烟过滤材料中，以催化一氧化碳氧化成二氧化碳。
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公开(公告)号：US08496012B2
公开(公告)日：2013-07-30
申请号：US13185160
申请日：2011-07-18
IPC分类号： A24B15/18
CPC分类号： A24D3/06 , A24B15/28 , A24B15/282 , A24B15/286 , A24B15/287 , A24B15/288 , A24D1/02 , A24D1/18 , A24D3/16 , B01D53/62 , B01D53/94 , B82Y30/00
摘要： A method of making composite nanoscale particles comprising subjecting a starting material to laser energy so as to form a vapor and condensing the vapor so as to form the composite nanoscale particles, wherein said composite nanoscale particles comprise a first metal and/or a first metal oxide incorporated in nanoscale particles of an oxide of a second metal, the first metal being different than the second metal. The starting material can comprise first and second metals or compounds of the first and second metals. The composite nanoscale particles can be formed in a reaction chamber wherein a temperature gradient is provided. The atmosphere in the chamber can be an inert atmosphere comprising argon or a reactive atmosphere comprising oxygen. The composite nanoscale particles are useful for low-temperature and near-ambient temperature catalysis. The composite nanoscale particles can be incorporated in the tobacco cut filler, cigarette paper and/or cigarette filter material of a cigarette to catalyze the oxidation of carbon monoxide to carbon dixoxide.
摘要翻译： 一种制备复合纳米尺寸颗粒的方法，包括使起始材料经受激光能量以形成蒸气并使蒸气冷凝以形成复合纳米级颗粒，其中所述复合纳米级颗粒包含第一金属和/或第一金属氧化物 掺入第二金属的氧化物的纳米级颗粒中，第一金属不同于第二金属。 起始材料可以包括第一和第二金属或第一和第二金属的化合物。 复合纳米级颗粒可以在其中提供温度梯度的反应室中形成。 室中的气氛可以是包含氩气或包含氧的反应性气氛的惰性气氛。 复合纳米级颗粒可用于低温和近环境温度的催化。 复合纳米尺寸颗粒可以并入香烟的烟丝切割填料，卷烟纸和/或卷烟过滤材料中以催化一氧化碳氧化成二氧化碳。
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公开(公告)号：US08006703B2
公开(公告)日：2011-08-30
申请号：US10972204
申请日：2004-10-25
IPC分类号： A24B15/18
CPC分类号： A24D3/06 , A24B15/28 , A24B15/282 , A24B15/286 , A24B15/287 , A24B15/288 , A24D1/02 , A24D1/18 , A24D3/16 , B01D53/62 , B01D53/94 , B82Y30/00
摘要： A method of making composite nanoscale particles comprising subjecting a starting material to laser energy so as to form a vapor and condensing the vapor so as to form the composite nanoscale particles, wherein said composite nanoscale particles comprise a first metal and/or a first metal oxide incorporated in nanoscale particles of an oxide of a second metal, the first metal being different than the second metal. The starting material can comprise first and second metals or compounds of the first and second metals. The composite nanoscale particles can be formed in a reaction chamber wherein a temperature gradient is provided. The atmosphere in the chamber can be an inert atmosphere comprising argon or a reactive atmosphere comprising oxygen. The composite nanoscale particles are useful for low-temperature and near-ambient temperature catalysis. The composite nanoscale particles can be incorporated in the tobacco cut filler, cigarette paper and/or cigarette filter material of a cigarette to catalyze the oxidation of carbon monoxide to carbon dioxide.
摘要翻译： 一种制备复合纳米尺寸颗粒的方法，包括使起始材料经受激光能量以形成蒸气并使蒸气冷凝以形成复合纳米级颗粒，其中所述复合纳米级颗粒包含第一金属和/或第一金属氧化物 掺入第二金属的氧化物的纳米级颗粒中，第一金属不同于第二金属。 起始材料可以包括第一和第二金属或第一和第二金属的化合物。 复合纳米级颗粒可以在其中提供温度梯度的反应室中形成。 室中的气氛可以是包含氩气或包含氧的反应性气氛的惰性气氛。 复合纳米级颗粒可用于低温和近环境温度的催化。 复合纳米尺寸颗粒可以并入香烟的烟丝切割填料，香烟纸和/或卷烟过滤材料中，以催化一氧化碳氧化成二氧化碳。
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公开(公告)号：US20090275466A1
公开(公告)日：2009-11-05
申请号：US12488169
申请日：2009-06-19
IPC分类号： B01J23/745 , B01J31/06 , B01J31/02 , B01J21/18 , B01J21/08
CPC分类号： A24B15/288 , A24B15/28 , A24B15/287 , B01J23/80 , B22F9/24 , B22F9/30 , B22F2998/00 , C22C1/0491 , B22F1/0018
摘要： A metallo-organic decomposition process for the preparation of intermetallic powders and films. A liquid mixture containing a first metal precursor and a second metal is heated to a temperature in a first temperature range so as to convert the first metal precursor to a first metal followed by heating to a temperature in a second temperature range so as to form an intermetallic compound by a solid state reaction between the first and second metals. The intermetallic compound can be used as a catalyst in cut filler and/or the filter of a cigarette.
摘要翻译： 用于制备金属间化合物粉末和膜的金属有机分解方法。 将含有第一金属前体和第二金属的液体混合物加热至第一温度范围内的温度，以将第一金属前体转化为第一金属，然后加热至第二温度范围内的温度，从而形成 金属间化合物通过第一和第二金属之间的固态反应。 金属间化合物可以用作螯合剂中的催化剂和/或香烟的过滤器。
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公开(公告)号：US09034431B2
公开(公告)日：2015-05-19
申请号：US12488169
申请日：2009-06-19
CPC分类号： A24B15/288 , A24B15/28 , A24B15/287 , B01J23/80 , B22F9/24 , B22F9/30 , B22F2998/00 , C22C1/0491 , B22F1/0018
摘要： A metallo-organic decomposition process for the preparation of intermetallic powders and films. A liquid mixture containing a first metal precursor and a second metal is heated to a temperature in a first temperature range so as to convert the first metal precursor to a first metal followed by heating to a temperature in a second temperature range so as to form an intermetallic compound by a solid state reaction between the first and second metals. The intermetallic compound can be used as a catalyst in cut filler and/or the filter of a cigarette.
摘要翻译： 用于制备金属间化合物粉末和膜的金属有机分解方法。 将含有第一金属前体和第二金属的液体混合物加热至第一温度范围内的温度，以将第一金属前体转化为第一金属，然后加热至第二温度范围内的温度，从而形成 金属间化合物通过第一和第二金属之间的固态反应。 金属间化合物可以用作螯合剂中的催化剂和/或香烟的过滤器。
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6.发明授权Nanoscale particles of iron aluminide and iron aluminum carbide by the reduction of iron salts 有权通过铁盐的还原，铝铁铝和铁铝碳化物的纳米级颗粒公开(公告)号：US07677255B2
公开(公告)日：2010-03-16
申请号：US11300586
申请日：2005-12-15
CPC分类号： C04B35/117 , A24B15/28 , A24B15/286 , A24B15/287 , A24D3/16 , B22F1/0018 , B22F9/20 , B22F9/24 , B82Y30/00 , C01G49/00 , C01G49/009 , C01P2002/50 , C01P2002/72 , C01P2002/85 , C01P2004/03 , C01P2004/04 , C01P2004/30 , C01P2004/64 , C01P2006/42 , C04B35/56 , C04B35/628 , C04B35/62813 , C04B2235/3217 , C04B2235/3817 , C04B2235/402 , C04B2235/5454 , C04B2235/549 , C04B2235/80 , C22C1/0491 , C22C1/053
摘要： A method of making intermetallic nanoscale particles comprising iron aluminide and/or iron aluminum carbide comprising the steps of preparing a mixture of a solvent, an iron salt and LiAlH4, and heating the mixture to form the intermetallic nanoscale particles. The intermetallic nanoscale particles, which can comprise intermetallic nanoscale particles of iron aluminide and/or iron aluminum carbide in an alumina matrix, are capable of reducing the amount of 1,3-butadiene in the mainstream smoke of a cigarette.
摘要翻译： 制备包含铁铝化物和/或碳化铝铁的金属间纳米级颗粒的方法包括以下步骤：制备溶剂，铁盐和LiAlH 4的混合物，并加热混合物以形成金属间纳米级颗粒。 可以在氧化铝基质中包含铁铝化物和/或铁铝碳化物的金属间纳米级颗粒的金属间纳米尺寸颗粒能够减少香烟主流烟气中的1,3-丁二烯的量。
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7.发明授权公开(公告)号：US07004993B2
公开(公告)日：2006-02-28
申请号：US10460318
申请日：2003-06-13
CPC分类号： C04B35/117 , A24B15/28 , A24B15/286 , A24B15/287 , A24D3/16 , B22F1/0018 , B22F9/20 , B22F9/24 , B82Y30/00 , C01G49/00 , C01G49/009 , C01P2002/50 , C01P2002/72 , C01P2002/85 , C01P2004/03 , C01P2004/04 , C01P2004/30 , C01P2004/64 , C01P2006/42 , C04B35/56 , C04B35/628 , C04B35/62813 , C04B2235/3217 , C04B2235/3817 , C04B2235/402 , C04B2235/5454 , C04B2235/549 , C04B2235/80 , C22C1/0491 , C22C1/053
摘要： A method of making intermetallic nanoscale particles comprising iron aluminide and/or iron aluminum carbide comprising the steps of preparing a mixture of a solvent, an iron salt and LiAlH4, and heating the mixture to form the intermetallic nanoscale particles. The intermetallic nanoscale particles, which can comprise intermetallic nanoscale particles of iron aluminide and/or iron aluminum carbide in an alumina matrix, are capable of reducing the amount of 1,3-butadiene in the mainstream smoke of a cigarette.
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8.发明授权Copper and/or zinc alloy nanopowders made by laser vaporization and condensation 有权通过激光蒸发和冷凝制成的铜和/或锌合金纳米粉末公开(公告)号：US07413725B2
公开(公告)日：2008-08-19
申请号：US10915693
申请日：2004-08-11
申请人： M. Samy El-Shall , Sarojini Deevi , Yezdi B. Pithawalla , Seetharama C. Deevi , A. Clifton Lilly, Jr.
发明人： M. Samy El-Shall , Sarojini Deevi , Yezdi B. Pithawalla , Seetharama C. Deevi , A. Clifton Lilly, Jr.
CPC分类号： B82Y30/00 , B01J23/80 , B01J35/0013 , B22F9/12 , B22F2999/00 , C23C14/14 , C23C14/28 , B22F2202/11
摘要： A method of making Cu, Zn, and/or Cu/Zn alloy nanoparticles subjects one or more targets to laser energy to form a vapor and condenses the vapor to form nanoparticles having an average particle size of less than 20 nm. The optional application of an electric field results in nanoparticles with aspect ratios greater than 1.0. The target(s) can be a single target or separate targets comprising a mixture of copper, zinc, and/or copper/zinc. When separate targets are used, the laser beam can be split to form two separate beams each of which is made incident upon one of the targets. The nanoparticles can be formed in a chamber having an inert atmosphere or a reactive atmosphere and a convection current is created in the chamber by maintaining the top plate at a lower temperature than the bottom plate.
摘要翻译： 一种制备Cu，Zn和/或Cu / Zn合金纳米颗粒的方法使一个或多个靶发生激光能量以形成蒸气并使蒸气冷凝以形成平均粒度小于20nm的纳米颗粒。 电场的可选应用导致长宽比大于1.0的纳米颗粒。 靶可以是单个靶或包含铜，锌和/或铜/锌的混合物的单独靶。 当使用单独的目标时，激光束可以被分割以形成两个单独的光束，每个光束入射到其中一个目标上。 纳米颗粒可以在具有惰性气氛或反应性气氛的室中形成，并且通过将顶板保持在低于底板的温度下而在室中产生对流。
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9.发明授权Silver and silver oxide catalysts for the oxidation of carbon monoxide in cigarette smoke 有权用于氧化香烟烟雾中一氧化碳的银和氧化银催化剂公开(公告)号：US08360073B2
公开(公告)日：2013-01-29
申请号：US12782427
申请日：2010-05-18
申请人： Rangaraj S. Sundar , Sarojini Deevi
发明人： Rangaraj S. Sundar , Sarojini Deevi
IPC分类号： A24B15/18
CPC分类号： A24B15/288 , A24B15/28 , A24B15/286 , A24B15/287 , A24D1/002 , A24D1/02 , A24D3/16 , B01D53/865 , B01D2255/104 , B01J23/50 , B01J23/66 , B01J35/0013 , Y02P70/66
摘要： A component of a cigarette comprises a silver-based catalyst for the conversion of carbon monoxide to carbon dioxide. The silver-based catalyst comprises particles (e.g., nanoscale or larger sized particles) of metallic silver and/or silver oxide supported in and/or on metal oxide support particles. The silver-based catalyst can be incorporated into a cigarette component such as tobacco cut filler, cigarette paper and cigarette filter material to reduce the concentration of carbon monoxide in the mainstream smoke of a cigarette during smoking. The catalyst can also be used in non-cigarette applications.
摘要翻译： 香烟的组分包括用于将一氧化碳转化为二氧化碳的银基催化剂。 银基催化剂包含负载在金属氧化物载体颗粒中和/或上的金属银和/或氧化银的颗粒（例如，纳米级或更大尺寸的颗粒）。 可以将银基催化剂掺入烟草成分如烟草切片填料，卷烟纸和卷烟过滤材料中，以减少吸烟期间卷烟主流烟雾中的一氧化碳浓度。 该催化剂也可用于非卷烟应用中。
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10.发明授权Silver and silver oxide catalysts for the oxidation of carbon monoxide in cigarette smoke 有权用于氧化香烟烟雾中一氧化碳的银和氧化银催化剂公开(公告)号：US07743772B2
公开(公告)日：2010-06-29
申请号：US10868015
申请日：2004-06-16
申请人： Rangaraj S. Sundar , Sarojini Deevi
发明人： Rangaraj S. Sundar , Sarojini Deevi
CPC分类号： A24B15/288 , A24B15/28 , A24B15/286 , A24B15/287 , A24D1/002 , A24D1/02 , A24D3/16 , B01D53/865 , B01D2255/104 , B01J23/50 , B01J23/66 , B01J35/0013 , Y02P70/66
摘要： A component of a cigarette comprises a silver-based catalyst for the conversion of carbon monoxide to carbon dioxide. The silver-based catalyst comprises particles (e.g., nanoscale or larger sized particles) of metallic silver and/or silver oxide supported in and/or on metal oxide support particles. The silver-based catalyst can be incorporated into a cigarette component such as tobacco cut filler, cigarette paper and cigarette filter material to reduce the concentration of carbon monoxide in the mainstream smoke of a cigarette during smoking. The catalyst can also be used in non-cigarette applications.
摘要翻译： 香烟的组分包括用于将一氧化碳转化为二氧化碳的银基催化剂。 银基催化剂包含负载在金属氧化物载体颗粒中和/或上的金属银和/或氧化银的颗粒（例如，纳米级或更大尺寸的颗粒）。 可以将银基催化剂掺入烟草成分如烟草切片填料，卷烟纸和卷烟过滤材料中，以减少吸烟期间卷烟主流烟雾中的一氧化碳浓度。 该催化剂也可用于非卷烟应用中。
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