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    Synthesis method of organometallic complex, synthesis method of pyrazine derivative, 5,6-diaryl-2-pyrazyl triflate, light-emitting element, light-emitting device, electronic device, and lighting device
    3.
    发明授权
    Synthesis method of organometallic complex, synthesis method of pyrazine derivative, 5,6-diaryl-2-pyrazyl triflate, light-emitting element, light-emitting device, electronic device, and lighting device 有权
    有机金属配合物的合成方法，吡嗪衍生物的合成方法，三氟甲磺酸5,6-二芳基-2-吡唑酯，发光元件，发光元件，电子器件及照明装置

    公开(公告)号：US09231217B2

    公开(公告)日：2016-01-05

    申请号：US14551712

    申请日：2014-11-24

    Applicant: Semiconductor Energy Laboratory Co., Ltd.

    Inventor： Hideko Inoue ,  Tomohiro Kubota ,  Miki Kanamoto

    IPC: H01L21/76 ,  H01L51/00 ,  C07F15/00 ,  C07D241/12 ,  C09K11/06 ,  H01L51/50

    CPC classification number: C07D241/18 ,  C07D241/12 ,  C07F15/0033 ,  C09K11/06 ,  C09K2211/185 ,  H01L51/0085 ,  H01L51/5016 ,  H01L2251/308

    Abstract: Provided is a 5,6-diaryl-2-pyrazyl triflate, its synthetic method, and a method for synthesizing an organometallic complex having a triarylpyrazine ligand from the 5,6-diaryl-2-pyrazyl triflate. The triflate is readily obtained from the corresponding 5,6-diarylpyrazin-2-ol, and the palladium-catalyzed coupling of the 5,6-diaryl-2-pyrazyl triflate with an arylboronic acid derivative leads to a high yield of a triarylpyrazine derivative having high purity. The use of the triarylpyrazine derivative in the reaction with a metal compound such as a metal chloride results in an ortho-metallated organometallic complex with high purity. The high purity of the organometallic complex contributes to the extremely high durability of a light-emitting element.

    Abstract translation: 提供三氟甲磺酸5,6-二芳基-2-吡唑酯，其合成方法以及由5,6-二芳基-2-吡唑基三氟甲磺酸酯合成具有三芳基吡嗪配体的有机金属络合物的方法。 三氟甲磺酸酯很容易从相应的5,6-二芳基吡嗪-2-醇中获得，并且5,6-二芳基-2-吡唑基三氟甲磺酸酯与芳基硼酸衍生物的钯催化偶联导致高产率的三芳基吡嗪衍生物 具有高纯度。 在与金属化合物如金属氯化物的反应中使用三芳基吡嗪衍生物导致具有高纯度的邻近金属化的有机金属络合物。 有机金属配合物的高纯度有助于发光元件的极高耐久性。

    Organometallic Complex, Light-Emitting Element, Light-Emitting Device, Electronic Device, and Lighting Device
    4.
    发明申请
    Organometallic Complex, Light-Emitting Element, Light-Emitting Device, Electronic Device, and Lighting Device 审中-公开
    有机金属配合物，发光元件，发光装置，电子装置和照明装置

    公开(公告)号：US20140246656A1

    公开(公告)日：2014-09-04

    申请号：US14193415

    申请日：2014-02-28

    Applicant: Semiconductor Energy Laboratory Co., Ltd.

    Inventor： Hideko Inoue ,  Miki Kanamoto ,  Hiromi Seo ,  Satoshi Seo ,  Tatsuyoshi Takahashi ,  Tomoya Yamaguchi

    IPC: H01L51/00 ,  H01L51/50

    CPC classification number: H01L51/0085 ,  C07F15/0033 ,  C09K11/06 ,  C09K2211/185 ,  H01L51/5016

    Abstract: As a novel substance having a novel skeleton, an organometallic complex having high emission efficiency and improved color purity is provided. The color purity is improved by reducing the half width of an emission spectrum. The organometallic complex is represented by General Formula (G1). In General Formula (G1), at least one of R1 to R4 represents a substituted or unsubstituted alkyl group having 1 to 4 carbon atoms, and the others each independently represent hydrogen or a substituted or unsubstituted alkyl group having 1 to 4 carbon atoms. Note that the case where all of R1 to R4 represent alkyl groups each having 1 carbon atom is excluded. Further, R5 to R9 each independently represent hydrogen or a substituted or unsubstituted alkyl group having 1 to 6 carbon atoms.

    Abstract translation: 作为具有新骨架的新型物质，提供了发光效率高，颜色纯度提高的有机金属配合物。 通过减小发射光谱的半宽度来提高色纯度。 有机金属络合物由通式（G1）表示。 在通式（G1）中，R 1至R 4中的至少一个表示取代或未取代的具有1至4个碳原子的烷基，其余各自独立地表示氢或取代或未取代的碳原子数1〜4的烷基。 注意，除了所有R 1至R 4表示各自具有1个碳原子的烷基的情况。 此外，R 5至R 9各自独立地表示氢或取代或未取代的具有1至6个碳原子的烷基。

    Organometallic complex, light-emitting element, light-emitting device, electronic device, and lighting device
    7.
    发明授权
    Organometallic complex, light-emitting element, light-emitting device, electronic device, and lighting device 有权

    公开(公告)号：US10115912B2

    公开(公告)日：2018-10-30

    申请号：US15137460

    申请日：2016-04-25

    Applicant: Semiconductor Energy Laboratory Co., Ltd.

    Inventor： Hideko Inoue ,  Miki Kanamoto ,  Satoshi Seo

    IPC: H01L51/00 ,  H01L27/32 ,  C07F15/00 ,  C09K11/06

    Abstract: An object is to provide a novel organometallic complex. Another object is to provide an organometallic complex that can exhibit yellow to blue phosphorescence. A platinum complex with a tetracoordinate ligand including a phenothiazine skeleton or a phenoxazine skeleton is provided. In the ligand, nitrogen at the 10-position and carbon at the 2-position of the phenothiazine skeleton or the phenoxazine skeleton have a pyridyl group and a phenoxy group, respectively. A five-membered heteroaromatic residue is present at the 3-position of the phenoxy group. The five-membered heteroaromatic residue has two or three nitrogen atoms in its skeleton. Carbon at the 1-position of the phenothiazine skeleton or the phenoxazine skeleton and carbon at the 2-position of the phenoxy group are bonded to platinum, and nitrogen of the pyridyl group and nitrogen or carbene carbon of the five-membered heteroaromatic residue are coordinated to platinum.

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