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    Processes for low melt crosslinked toner resins and toner
    1.
    发明授权
    Processes for low melt crosslinked toner resins and toner 失效
    低熔点交联调色剂树脂和调色剂的方法

    公开(公告)号：US5601960A

    公开(公告)日：1997-02-11

    申请号：US555954

    申请日：1995-11-13

    申请人： Hadi K. Mahabadi ,  Enno E. Agur ,  T. Brian McAneney ,  Sheau V. Kao ,  Gerald R. Allison ,  Michael S. Hawkins ,  Bernard Grushkin ,  J. Stephen Kittelberger ,  Joo T. Chung ,  William H. Hollenbaugh, Jr.

    发明人： Hadi K. Mahabadi ,  Enno E. Agur ,  T. Brian McAneney ,  Sheau V. Kao ,  Gerald R. Allison ,  Michael S. Hawkins ,  Bernard Grushkin ,  J. Stephen Kittelberger ,  Joo T. Chung ,  William H. Hollenbaugh, Jr.

    IPC分类号： G03G9/087 ,  G03G9/08 ,  C08G63/20

    CPC分类号： G03G9/081

    摘要： A process comprising:(a) reactive melt mixing of a base resin with a chemical initiator and crosslinking of said base resin to enable a highly crosslinked precursor resin, said highly crosslinked precursor resin being substantially free of sol, and comprising uncrosslinked portions and crosslinked portions, said crosslinked portions comprised of high density crosslinked microgel particles; and(b) accomplishing dilution by melt mixing said highly crosslinked precursor resin of (a) with a base resin to form a partially crosslinked toner resin, said toner resin being substantially free of sol, and comprising linear uncrosslinked portions and crosslinked portions, said crosslinked portions comprised essentially of high density crosslinked microgel particles, wherein said microgel particles are present in an amount of from about 1 to about 45 percent by weight of said toner resin.

    摘要翻译： 一种方法，包括：（a）基础树脂与化学引发剂的反应性熔融混合和所述基础树脂的交联以使得能够高度交联的前体树脂，所述高度交联的前体树脂基本上不含溶胶，并且包含未交联部分和交联部分 所述交联部分由高密度交联微凝胶颗粒构成; （b）通过将（a）的高度交联的前体树脂与基础树脂熔融混合以形成部分交联的调色剂树脂来实现稀释，所述调色剂树脂基本上不含溶胶，并且包含线性未交联部分和交联部分，所述交联 基本上由高密度交联微凝胶颗粒组成的部分，其中所述微粒凝胶颗粒以所述调色剂树脂重量的约1至约45％的量存在。

    Processes for low melt crosslinked toner resins and toner
    2.
    发明授权
    Processes for low melt crosslinked toner resins and toner 失效
    低熔点交联调色剂树脂和调色剂的方法

    公开(公告)号：US5500324A

    公开(公告)日：1996-03-19

    申请号：US332315

    申请日：1994-10-31

    申请人： Hadi K. Mahabadi ,  Enno E. Agur ,  T. Brian McAneney ,  Sheau V. Kao ,  Gerald R. Allison ,  Michael S. Hawkins ,  Bernard Grushkin ,  J. Stephen Kittelberger ,  Joo T. Chung ,  William H. Hollenbaugh, Jr.

    发明人： Hadi K. Mahabadi ,  Enno E. Agur ,  T. Brian McAneney ,  Sheau V. Kao ,  Gerald R. Allison ,  Michael S. Hawkins ,  Bernard Grushkin ,  J. Stephen Kittelberger ,  Joo T. Chung ,  William H. Hollenbaugh, Jr.

    IPC分类号： G03G9/087 ,  G03G9/08

    CPC分类号： G03G9/081

    摘要： A process comprising:(a) reactive melt mixing of a base resin with a chemical initiator and crosslinking of said base resin to enable a highly crosslinked precursor resin, said highly crosslinked precursor resin being substantially free of sol, and comprising uncrosslinked portions and crosslinked portions, said crosslinked portions comprised of high density crosslinked microgel particles; and(b) accomplishing dilution by melt mixing said highly crosslinked precursor resin of (a) with a base resin to form a partially crosslinked toner resin, said toner resin being substantially free of sol, and comprising linear uncrosslinked portions and crosslinked portions, said crosslinked portions comprised essentially of high density crosslinked microgel particles, wherein said microgel particles are present in an amount of from about 1 to about 45 percent by weight of said toner resin.

    摘要翻译： 一种方法，包括：（a）基础树脂与化学引发剂的反应性熔融混合和所述基础树脂的交联以使得能够高度交联的前体树脂，所述高度交联的前体树脂基本上不含溶胶，并且包含未交联部分和交联部分 所述交联部分由高密度交联微凝胶颗粒构成; （b）通过将（a）的高度交联的前体树脂与基础树脂熔融混合以形成部分交联的调色剂树脂来实现稀释，所述调色剂树脂基本上不含溶胶，并且包含线性未交联部分和交联部分，所述交联 基本上由高密度交联微凝胶颗粒组成的部分，其中所述微粒凝胶颗粒以所述调色剂树脂的约1至约45重量％的量存在。

    Processes for encapsulated toners
    6.
    发明授权
    Processes for encapsulated toners 失效
    封装调色剂的方法

    公开(公告)号：US5153092A

    公开(公告)日：1992-10-06

    申请号：US646914

    申请日：1991-01-28

    申请人： Sheau V. Kao ,  Gerald R. Allison ,  Michael S. Hawkins ,  Hadi K. Mahabadi

    发明人： Sheau V. Kao ,  Gerald R. Allison ,  Michael S. Hawkins ,  Hadi K. Mahabadi

    IPC分类号： G03G9/08 ,  G03G9/087 ,  G03G9/093

    CPC分类号： G03G9/09335 ,  G03G9/09364 ,  G03G9/09392

    摘要： A process for the preparation of encapsulated toners which comprises blending core momomer or monomers, free radical initiator, pigment, and an oil soluble shell monomer; dispersing the resulting mixture in a stabilized aqueous suspension; thereafter subjecting the stabilized droplets to a shell forming interfacial polycondensation reaction by adding a water soluble shell monomer or monomers; subsequently forming the core resin binder by heat induced free radical polymerization within the newly formed capsules; washing the toner suspension; subsequently removing water therefrom in a fluidized bed dryer to obtain a dry encapsulated toner with a surface moisture content of about 0.3 percent by weight to about 0.8 percent by weight; and thereafter blending the encapsulated toner with surface additives.

    摘要翻译： 一种制备包封的调色剂的方法，包括混合核心单体或单体，自由基引发剂，颜料和油溶性壳单体; 将所得混合物分散在稳定的水性悬浮液中; 然后通过加入水溶性壳单体或单体使稳定的液滴经壳形成界面缩聚反应; 随后在新形成的胶囊内通过热诱导的自由基聚合形成核心树脂粘合剂; 清洗调色剂悬浮液; 随后在流化床干燥器中从其中除去水，得到表面含水量为约0.3重量％至约0.8重量％的干燥包封调色剂; 然后将包封的调色剂与表面添加剂混合。

    Processes for preparing phase change inks
    8.
    发明授权
    Processes for preparing phase change inks 有权
    制备相变油墨的方法

    公开(公告)号：US07186762B2

    公开(公告)日：2007-03-06

    申请号：US10721851

    申请日：2003-11-25

    申请人： Raymond W. Wong ,  Hadi K. Mahabadi ,  Paul F. Smith ,  Sheau V. Kao ,  Michael S. Hawkins ,  Caroline M. Turek

    发明人： Raymond W. Wong ,  Hadi K. Mahabadi ,  Paul F. Smith ,  Sheau V. Kao ,  Michael S. Hawkins ,  Caroline M. Turek

    IPC分类号： C09D11/02 ,  C09D11/10 ,  C08L39/04 ,  B29C47/00 ,  B29C47/38

    CPC分类号： C09D11/34 ,  B29C47/6087

    摘要： Disclosed is a process for preparing a phase change ink composition which comprises (a) a phase change ink carrier, said carrier comprising at least one nonpolar component and at least one polar component, and (b) pigment particles, said process comprising (1) selecting at least one of the polar carrier components to be a pigment particle dispersant; (2) admixing the pigment particles with the dispersant; (3) extruding the mixture of pigment particles and dispersant in an extruder at a temperature that is at or above about the peak crystallization temperature of the dispersant and below about the peak melting temperature of the dispersant, thereby forming a pigment dispersion; (4) subsequent to extrusion of the pigment dispersion, adding to the pigment dispersion any remaining polar components and the nonpolar component; and (5) subjecting the resulting mixture of pigment dispersion, polar component, and nonpolar component to high shear mixing to form an ink.

    摘要翻译： 公开了一种制备相变油墨组合物的方法，其包括（a）相变油墨载体，所述载体包含至少一种非极性组分和至少一种极性组分，和（b）颜料颗粒，所述方法包括（1） 选择至少一种极性载体成分为颜料颗粒分散剂; （2）将颜料颗粒与分散剂混合; （3）将挤出机中的颜料颗粒和分散剂的混合物在分散剂的峰值结晶温度以下并且低于分散剂的峰值熔融温度的温度下挤出，从而形成颜料分散体; （4）在颜料分散体挤出之后，向颜料分散体中加入剩余的极性组分和非极性组分; 和（5）将颜料分散体，极性组分和非极性组分的所得混合物进行高剪切混合以形成油墨。