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公开(公告)号:US20190144418A1
公开(公告)日:2019-05-16
申请号:US16306970
申请日:2017-07-27
发明人: Haibo YU , Guimin ZHAO , Guosheng ZHANG , Junwu YING , Huibin YANG , Bin LI
IPC分类号: C07D401/04 , A01N43/56
摘要: The present invention provides a polymorph of a benzamide compound and a preparation method and applications thereof. The shown benzamide compound is 3-Bromo-N-[2,4-dichloro-6-[(methylamino)carbonyl]phenyl]-1-(3,5-dichloro-2-pyridinyl)-1H-pyrazole-5-carboxamide. The application of the polymorph of the compound in the preparation of the formulation exhibits excellent effect. The advantages of the polymorph A in aspects such as chemical stability, filterability, solubility, hygroscopicity, melting point, solid density and flowability can have a significant impact on the developments of the production method and a formulation and on the quality and efficacy of a plant treating agent.
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公开(公告)号:US20220400678A1
公开(公告)日:2022-12-22
申请号:US17755625
申请日:2020-11-02
发明人: Xueming CHENG , Haibo YU , Liang CHEN , Hongfei WU , Geng SUN , Chunxiao GUO , Libao XU , Jingbo XU , Ningning SUN
IPC分类号: A01N43/78 , C07D277/46 , C07D277/40 , C07D277/50 , A01P1/00 , A01P3/00
摘要: The present invention discloses an oxime ether compound with novel structure. The structure is shown in general formula I. The definition of each substituent in the formula is provided in the description. The compound of general formula I has excellent microbicidal 1 activity, and has good control effects on plant bacterial diseases and fungal diseases. The present invention comprises an application of the compound of the general formula I as a microbicide in agriculture and other fields.
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公开(公告)号:US20210380530A1
公开(公告)日:2021-12-09
申请号:US17287460
申请日:2019-10-08
发明人: Haibo YU , Hao YANG , Guimin ZHAO , Zhongbao REN , Hongfei WU , Xueling WANG , Zeyong ZHANG
IPC分类号: C07C319/20 , B01J31/24 , B01J23/06
摘要: A preparation method of a sulfur-containing biphenylsulfur-containing biphenyl compound shown by the general formula (I) has a reaction formula as follows: Each substituent in the formula is defined in the description. In the method, halogeno benzene shown by the general formula (II) generates a coupling reaction in a catalytic system composed of a nickel compound and at least one ligand under the combined action of metallic zinc to obtain the sulfur-containing biphenyl compound shown by the general formula (I).
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公开(公告)号:US20230271919A1
公开(公告)日:2023-08-31
申请号:US18005572
申请日:2021-07-13
发明人: Libao XU , Hongfei WU , Xiuhui CHANG , Haibo YU , Yuquan SONG , Jingbo XU , Chunxiao GUO , Xueming CHENG , Ningning SUN
IPC分类号: C07C317/32 , C07C323/65 , A01P7/02
CPC分类号: C07C317/32 , C07C323/65 , A01P7/02
摘要: The present invention belongs to the field of agricultural acaricides, and particularly relates to a substituted phenyl sulfide compound and an application thereof. The substituted phenyl sulfide compound is as represented in general formula I. Definitions of substituted groups in the formula are given in the description. The compound of the general formula I has excellent acaricidal activity and can be used for preventing and controlling various mites.
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公开(公告)号:US20220202011A1
公开(公告)日:2022-06-30
申请号:US17687385
申请日:2022-03-04
发明人: Hongfei WU , Jingbo XU , Shaowu LIU , Haibo YU , Lanfeng BAN , Libao XU , Xueming CHENG , Chunxiao GUO , Ningning SUN
IPC分类号: A01N43/30 , C07D317/46 , A01P7/04
摘要: The present invention belongs to the fields of insecticides and acaricides, and particularly relates to a piperonylic acid derivative and application thereof. The structure is shown in a general formula I, and the definition of each substituent in the formula is described in the description. The compound of the general formula I has excellent insecticidal and acaricidal activity and can be used for controlling various pests and mites.
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公开(公告)号:US20220055996A1
公开(公告)日:2022-02-24
申请号:US17259565
申请日:2019-06-17
发明人: Hongfei WU , Xueming CHENG , Libao XU , Chunxiao GUO , Jingbo XU , Ningning SUN , Haibo YU
IPC分类号: C07D277/24 , C07C255/64 , C07C253/30 , C07C253/20 , C07D213/61 , C07D215/14
摘要: Provided are a method of preparing a malononitrile oxime ether compound and an intermediate compound. The malononitrile oxime ether compound has a structure as shown in formula (VII), wherein W is selected from aryl or heteroaryl. The preparation method comprises steps: reacting a first raw material with a second raw material in the presence of a first solvent and a catalyst to obtain the intermediate compound, wherein the first raw material has a structure as shown in formula (IV), and the second raw material has a structure as shown in formula (V); and subjecting the intermediate compound as shown in formula (VI), and, a dehyclrant to a dehydrantion reaction in the presence of a second solvent to obtain the malononitrile oxime ether compound. In the preparation process for the intermediate, a cheaper cyanoacetamide is used as a raw material, the reaction conditions are mild. Moreover, the yield of the intermediate compound is high and the cost of the process is low. Furthermore, the required malononitrile oxime ether compound, is obtained only through one-step dehydration reaction. Using the preparation method, is advantageous for improving the yield of malononitrile oxime ethers and reducing the cost of the process.
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公开(公告)号:US20210176988A1
公开(公告)日:2021-06-17
申请号:US17187877
申请日:2021-02-28
发明人: Jingyu CHOU , Lu YU , Yuquan SONG , Hongfei WU , Haibo YU
摘要: The present invention belongs to the field of acaricides, and relates to a liquid formulation of a biphenyl-containing compound and an application thereof. A liquid formulation of a biphenyl-containing compound takes compound A as an active component and comprises at least one carrier and at least one auxiliary. The weight percentage of the active component in the liquid formulation is 0.1%-99%. The liquid formulation of the present invention can control the particle size of the liquid formulation through a good auxiliary system, and has the characteristics of good dispersibility, high suspension rate, good biological activity, low dosage, low cost, resistance to rain washing, low residue and low toxicity to people and animals.
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公开(公告)号:US20200181107A1
公开(公告)日:2020-06-11
申请号:US16625296
申请日:2018-06-22
发明人: Hongfei WU , Jingbo XU , Shaowu LIU , Haibo YU , Xiuhui CHANG , Qin SUN , Libao XU , Xueming CHENG , Hao YANG , Ningning SUN
IPC分类号: C07D317/68 , A01N43/30
摘要: The present invention belongs to the fields of insecticides, acaricides and fungicides, and particularly relates to a piperonylic acid derivative, and preparation and application thereof. The structure is shown in a general formula I, and the definition of each substituent in the formula is described in the description. The compound of the general formula I exhibits excellent insecticidal, acaricidal and fungicidal activity and can be used for controlling various harmful insects, mites or fungus.
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