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    Process for preparing a metal-free phthalocyanine
    2.
    发明授权
    Process for preparing a metal-free phthalocyanine 失效
    制备无金属酞菁的方法

    公开(公告)号：US5824800A

    公开(公告)日：1998-10-20

    申请号：US666121

    申请日：1996-06-21

    申请人： Shinichi Tamura ,  Seishi Terasaki ,  Tadashi Mimura ,  Teruaki Kobayashi ,  Youichi Tei

    发明人： Shinichi Tamura ,  Seishi Terasaki ,  Tadashi Mimura ,  Teruaki Kobayashi ,  Youichi Tei

    IPC分类号： C07D487/22 ,  C09B47/30 ,  C09B67/50 ,  G03G5/06

    CPC分类号： C09B67/0026 ,  C09B47/30 ,  G03G5/0696

    摘要： Phthalonitrile, an alkali metal or an alkali metal compound, and a hydrogen donor compound are heated in an organic solvent to synthesize a partially hydrogenated alkali metal phthalocyanine, which is then brought into contact with a dealkalizing agent to effect substitution with hydrogen of the partially hydrogenated alkali metal phthalocyanine to thereby obtain high-purity metal-free phthalocyanine. FX-type metal-free phthalocyanine as obtained according to the foregoing procedure may be used as a charge-generating substance to produce an electrophotographic photoconductor of high image quality which is highly sensitive to near infrared rays.

    摘要翻译： 邻苯二甲腈，碱金属或碱金属化合物和氢供体化合物在有机溶剂中加热，以合成部分氢化的碱金属酞菁，然后与脱碱剂接触，以实现部分氢化的氢取代 碱金属酞菁，由此得到高纯度的无金属酞菁。 根据上述方法获得的FX型无金属酞菁可以用作电荷产生物质，以产生对近红外线高度敏感的高图像质量的电子照相感光体。

    Electrophotographic photoconductor including a metal-free phthalocyanine
    3.
    发明授权
    Electrophotographic photoconductor including a metal-free phthalocyanine 失效
    包括无金属酞菁的电子照相感光体

    公开(公告)号：US5591555A

    公开(公告)日：1997-01-07

    申请号：US370384

    申请日：1995-01-10

    申请人： Shinichi Tamura ,  Seishi Terasaki ,  Tadashi Mimura ,  Teruaki Kobayashi ,  Youichi Tei

    发明人： Shinichi Tamura ,  Seishi Terasaki ,  Tadashi Mimura ,  Teruaki Kobayashi ,  Youichi Tei

    IPC分类号： C07D487/22 ,  C09B47/30 ,  C09B67/50 ,  G03G5/06

    CPC分类号： C09B67/0026 ,  C09B47/30 ,  G03G5/0696

    摘要： An electrophotographic photoconductor, includes metal-free phthalocyanine as a charge-generating substance, wherein the X-ray diffraction spectrum of said metal-free phthalocyanine as measured using CuK.alpha. as a radiation source includes intense diffraction peaks at Bragg angles (2.theta..+-.0.2.degree.) of 7.5.degree., 9.0.degree., 16.6.degree., 17.2.degree., 21.5.degree., 22.2.degree., 23.8.degree., and 28.5.degree., and wherein the infrared absorption spectrum of said metal-free phthalocyanine includes four absorption bands with the maximum absorption intensity at a wavenumber of 716 cm.sup.-1 between a wavenumber of 700 cm.sup.-1 and a wavenumber of 760 cm.sup.-1 and a characteristic absorption band at a wavenumber of 3,291.+-.2 cm.sup.-1.

    摘要翻译： 电子照相感光体包括无金属酞菁作为电荷产生物质，其中使用CuKα作为辐射源测量的所述无金属酞菁的X射线衍射光谱包括在布拉格角（2θ/ -0.2°）为7.5°，9.0°，16.6°，17.2°，21.5°，22.2°，23.8°和28.5°，其中所述无金属酞菁的红外吸收光谱包括具有最大吸收的四个吸收带 波数为700cm -1，波数为760cm -1的波数716cm -1处的波数和波数为3,291 +/- 2cm -1的特征吸收带。

    Photosensitive body for electrophotography
    5.
    发明授权
    Photosensitive body for electrophotography 失效
    电子照相用感光体

    公开(公告)号：US06287736B1

    公开(公告)日：2001-09-11

    申请号：US09641017

    申请日：2000-08-17

    申请人： Ikuo Takaki ,  Seishi Terasaki

    发明人： Ikuo Takaki ,  Seishi Terasaki

    IPC分类号： G03G5047

    CPC分类号： G03G5/0677 ,  G03G5/0618 ,  G03G5/0679

    摘要： The present invention provides an organic photosensitive body having improved stability of the electric property at times of repeated use and at times of changes in conditions of environmental usage. Such a photosensitive body prevents the generation of image defects of memory and the like. The present invention is a function-separated laminated organic photosensitive body equipped with a photosensitive layer, having a charge generating layer and a charge transport layer laminated in sequence on top of a conductive substrate, wherein the charge transport layer contains at least one type of electron transporting compound represented by the following general formulas (I) and (II): wherein R1-R29, A1, B1, and B2 are each as defined in the specification.

    摘要翻译： 本发明提供一种有机感光体，其在反复使用时和环境使用条件变化时具有改善的电性能稳定性。 这样的感光体防止存储器等的图像缺陷的产生。 本发明是一种功能分离的层叠有机感光体，其具有感光层，其具有顺序层叠在导电性基板上的电荷产生层和电荷输送层，其中电荷输送层含有至少一种电子 由以下通式（I）和（II）表示的输送化合物：其中R1-R29，A1，B1和B2各自如说明书中所定义。

    Electrophotographic photoconductor and electrophotographic device using the same
    7.
    发明授权
    Electrophotographic photoconductor and electrophotographic device using the same 失效
    电子照相感光体和使用其的电子照相装置

    公开(公告)号：US6127078A

    公开(公告)日：2000-10-03

    申请号：US477596

    申请日：2000-01-04

    申请人： Shinichi Omokawa ,  Kenichi Ohkura ,  Seishi Terasaki ,  Yoshihiro Ueno ,  Kenji Kawate

    发明人： Shinichi Omokawa ,  Kenichi Ohkura ,  Seishi Terasaki ,  Yoshihiro Ueno ,  Kenji Kawate

    IPC分类号： G03G5/047 ,  G03G5/06

    CPC分类号： G03G5/0696 ,  G03G5/047 ,  G03G5/0614 ,  G03G5/0668

    摘要： An organic electrophotographic photoconductor diminished in an image trouble due to history of a transfer process in a reversal development system is disclosed. The above organic electrophotographic photoconductor is called a separated-function laminated type organic electrophotographic photoconductor, which has an undercoat layer and a photosensitive layer laminated in this order on a conductive substrate, the photosensitive layer comprising a charge generation layer laminated on the undercoat layer and containing an organic compound, and a charge transport layer laminated on the charge generation layer and containing an organic compound. For the charge generation layer, a titanyloxyphthalocyanine compound is used as a charge generation material. The present invention uses the titanyloxyphthalocyanine compound having a clear diffraction peak at a Bragg angle (2.theta.) of 9.6.degree..+-.0.2.degree. or 27.3.degree..+-.0.2.degree. for CuK.alpha. characteristic X-ray (wavelength 1.541 .ANG.). For the charge transport layer, a specific organic compound is used as a charge transport material.

    摘要翻译： 公开了由于反转显影系统中的转印过程的历史而在图像故障中减少的有机电子照相感光体。 上述有机电子照相感光体被称为分离功能层叠型有机电子照相感光体，其具有依次层叠在导电性基板上的底涂层和感光层，该感光层包含层叠在底涂层上的电荷产生层， 有机化合物和层叠在电荷产生层上并含有有机化合物的电荷输送层。 对于电荷产生层，使用钛氧基氧酞菁化合物作为电荷产生材料。 对于CuKα特征X射线（波长1.541ng），本发明使用布拉格角（2θ）为9.6°+/- 0.2°或27.3°±0.2°的具有清晰衍射峰的钛氧基氧酞菁化合物。 对于电荷输送层，使用特定的有机化合物作为电荷输送材料。