公开(公告)号：US08308979B2

公开(公告)日：2012-11-13

申请号：US13217559

申请日：2011-08-25

申请人： Shinichiro Ishino ,  Tomoki Masuda ,  Hirotaka Nanno ,  Yuko Kawanami ,  Noriyuki Matsusue ,  Mituru Harada

发明人： Shinichiro Ishino ,  Tomoki Masuda ,  Hirotaka Nanno ,  Yuko Kawanami ,  Noriyuki Matsusue ,  Mituru Harada

IPC分类号： H05B33/10 ,  H01L51/50

CPC分类号： H05B33/14 ,  C09D5/22 ,  H01L27/3244 ,  H01L51/0007 ,  H01L51/5012 ,  H01L51/56

摘要： An ink for an organic electroluminescent device includes a functional material, a first solvent, a second solvent, and a third solvent. The functional material is for forming a functional layer of the organic electroluminescent device. The first solvent is for dissolving the functional material. The second solvent has a diester backbone and a second boiling point that is at most equal to a first boiling point of the first solvent or greater than the first boiling point of the first solvent by at most 20° C. The third solvent is an aliphatic alcohol and has a third boiling point that is less than the first boiling point of the first solvent and less than the second boiling point of the second solvent.

摘要翻译： 用于有机电致发光器件的油墨包括功能材料，第一溶剂，第二溶剂和第三溶剂。 功能材料用于形成有机电致发光器件的功能层。 第一溶剂用于溶解功能材料。 第二溶剂具有二酯主链和第二沸点，其最多等于第一溶剂的第一沸点或大于第一溶剂的第一沸点至多20℃。第三溶剂是脂族 并且具有小于第一溶剂的第一沸点且小于第二溶剂的第二沸点的第三沸点。

公开(公告)号：US09318722B2

公开(公告)日：2016-04-19

申请号：US13976681

申请日：2011-01-19

申请人： Hirotaka Nanno ,  Shinichiro Ishino ,  Tomoki Masuda ,  Yuko Kawanami ,  Noriyuki Matsusue

发明人： Hirotaka Nanno ,  Shinichiro Ishino ,  Tomoki Masuda ,  Yuko Kawanami ,  Noriyuki Matsusue

IPC分类号： H01L51/56 ,  H01L51/52 ,  H01L51/00 ,  C09D11/36 ,  C09D11/30 ,  C09D11/50 ,  H05B33/10 ,  H01L51/50

CPC分类号： H01L51/52 ,  C09D11/30 ,  C09D11/36 ,  C09D11/50 ,  H01L51/0005 ,  H01L51/50 ,  H01L51/56 ,  H05B33/10

摘要： A method of efficiently manufacturing an organic light-emitting element with excellent light-emitting characteristics is provided. The method includes: preparing ink and filling an inkjet device having an ink ejection nozzle with the ink; preparing a substrate having a base layer including a first electrode; positioning the inkjet device above the substrate; and causing the inkjet device to eject a drop of the ink onto the base layer. In the preparation of the ink, a value Z denoting a reciprocal of the Ohnesorge number Oh determined by density ρ (g/dm3), surface tension γ (mN/m), and viscosity η (mPa·s) of the ink and a diameter r (mm) of the ink ejection nozzle satisfies Formula 1, in the ejection of the drop of the ink, speed V (m/s) of the ejected drop satisfies Formula 2, and the value Z and the speed V (m/s) satisfy Formula 3.

摘要翻译： 提供了一种有效地制造具有优异的发光特性的有机发光元件的方法。 该方法包括：准备墨水并将具有墨水喷射嘴的喷墨装置填充到墨水中; 制备具有包括第一电极的基层的基板; 将喷墨设备定位在基板上方; 并使喷墨装置将一滴墨水喷射到基底层上。 在油墨的制备中，表示Ohnesorge数的倒数的值Z表示为密度＆rgr; （g / dm3），表面张力γ（mN / m）和粘度＆ （mPa·s）和喷墨嘴的直径r（mm）满足式1，在喷墨滴下时，喷射液滴的速度V（m / s）满足式2，并且 值Z和速度V（m / s）满足公式3。

公开(公告)号：US20130292661A1

公开(公告)日：2013-11-07

申请号：US13978018

申请日：2011-01-19

申请人： Hirotaka Nanno ,  Shinichiro Ishino ,  Tomoki Masuda ,  Yuko Kawanami ,  Noriyuki Matsusue

发明人： Hirotaka Nanno ,  Shinichiro Ishino ,  Tomoki Masuda ,  Yuko Kawanami ,  Noriyuki Matsusue

IPC分类号： H01L51/56 ,  H01L51/50

CPC分类号： H01L51/56 ,  H01L51/0005 ,  H01L51/0007 ,  H01L51/50 ,  H01L51/5012 ,  H05B33/10

摘要： To provide a method of efficiently manufacturing an organic light-emitting element with excellent light-emitting characteristics by application, the method includes: preparing ink and filling an inkjet device having an ink ejection nozzle with the ink; preparing a substrate having a base layer including a first electrode; and positioning the inkjet device above the substrate, and causing the inkjet device to eject a drop of the ink onto the base layer, wherein, in the preparation of the ink, a value Z denoting a reciprocal of the Ohnesorge number Oh determined by density ρ (g/m3), surface tension γ (mN·m), and viscosity η (mPa·s) of the ink and a diameter r (mm) of the ink ejection nozzle satisfies Formula 1, in the ejection of the drop of the ink, speed V (m/s) of the ejected drop satisfies Formula 2, and the value Z and the speed V (m/s) satisfy Formula 3.

公开(公告)号：US20130139720A1

公开(公告)日：2013-06-06

申请号：US13641892

申请日：2011-09-28

申请人： Yuko Kawanami ,  Shinichiro Ishino ,  Tomoki Masuda ,  Hirotaka Nanno ,  Noriyuki Matsusue

发明人： Yuko Kawanami ,  Shinichiro Ishino ,  Tomoki Masuda ,  Hirotaka Nanno ,  Noriyuki Matsusue

IPC分类号： C09D11/02

CPC分类号： C09D11/02 ,  H01L27/3246 ,  H01L51/0005 ,  H01L51/5012 ,  H01L2251/55

摘要： An ink for an organic light-emitting element includes a first solvent, a second solvent, and a functional material. The first and second solvents have equal or similar boiling points. The first solvent is such that an imitatively formed functional layer formed by replacing the second solvent with the first solvent, in a light-emitting region of an organic light-emitting element, is thicker at both end portions than at a central portion and the top surfaces of the end portions are positioned higher than the top surface of the central portion. The second solvent is such that an imitatively formed functional layer formed by replacing the first solvent with the second solvent, in a light-emitting region of an organic light-emitting element, is thicker at a central portion than at both end portions and the top surface of the central portion is positioned higher than the top surfaces of the end portions.

摘要翻译： 用于有机发光元件的墨包括第一溶剂，第二溶剂和功能材料。 第一和第二溶剂具有相同或相似的沸点。 第一溶剂使得在有机发光元件的发光区域中通过用第一溶剂置换第二溶剂而形成的模仿功能层在两个端部处比在中心部分更厚，并且顶部 端部的表面定位成高于中心部分的顶表面。 第二溶剂使得在有机发光元件的发光区域中通过用第二溶剂替换第一溶剂而形成的模仿功能层在中心部分比在两个端部处和顶部的顶部更厚 中心部分的表面定位成高于端部的顶表面。

公开(公告)号：US09153782B2

公开(公告)日：2015-10-06

申请号：US13978013

申请日：2011-01-19

申请人： Hirotaka Nanno ,  Shinichiro Ishino ,  Tomoki Masuda ,  Yuko Kawanami ,  Noriyuki Matsusue

发明人： Hirotaka Nanno ,  Shinichiro Ishino ,  Tomoki Masuda ,  Yuko Kawanami ,  Noriyuki Matsusue

IPC分类号： H01L51/50 ,  H01L51/00 ,  H01L51/56 ,  H05B33/10

CPC分类号： H01L51/0005 ,  H01L51/0007 ,  H01L51/5012 ,  H01L51/56 ,  H05B33/10

摘要： To provide a method of efficiently manufacturing an organic light-emitting element with excellent light-emitting characteristics by application, the method includes: preparing ink and filling an inkjet device having an ink ejection nozzle with ink; preparing a substrate having a base layer including a first electrode; and positioning the inkjet device above the substrate, and causing the inkjet device to eject a drop of the ink onto the base layer, wherein, in the preparation of the ink, a value Z denoting a reciprocal of the Ohnesorge number Oh determined by density ρ (g/dm3), surface tension γ (mN/m), and viscosity η (mPa·s) of the ink and a diameter r (mm) of the ink ejection nozzle satisfies Formula 1, in the ejection of the drop of the ink, speed V (m/s) of the ejected drop satisfies Formula 2, and the value Z and the speed V (m/s) satisfy Formula 3.

摘要翻译： 为了提供一种通过应用有效地制造具有优异的发光特性的有机发光元件的方法，该方法包括：制备墨水并用具有墨水的具有喷墨嘴的喷墨装置进行填充; 制备具有包括第一电极的基层的基板; 并将喷墨装置定位在基板上方，并使喷墨装置将一滴墨喷射到基层上，其中，在制备墨时，表示由密度＆rgr确定的Ohnesorge数的倒数的值Z ; （g / dm3），表面张力γ（mN / m）和粘度＆ （mPa·s）和喷墨嘴的直径r（mm）满足式1，在喷墨滴下时，喷射液滴的速度V（m / s）满足式2，并且 值Z和速度V（m / s）满足公式3。

公开(公告)号：US08980678B2

公开(公告)日：2015-03-17

申请号：US13996132

申请日：2011-01-19

申请人： Hirotaka Nanno ,  Shinichiro Ishino ,  Tomoki Masuda ,  Yuko Kawanami ,  Noriyuki Matsusue

发明人： Hirotaka Nanno ,  Shinichiro Ishino ,  Tomoki Masuda ,  Yuko Kawanami ,  Noriyuki Matsusue

IPC分类号： H01L21/00 ,  H01L51/56 ,  H01L51/00 ,  B41J2/17 ,  H01L51/52 ,  B41J2/145

CPC分类号： H01L51/56 ,  B41J2/145 ,  B41J2/17 ,  B41J2202/09 ,  H01L51/0005 ,  H01L51/0007 ,  H01L51/52 ,  H05B33/10

摘要： To provide a method of efficiently manufacturing an organic light-emitting element with excellent light-emitting characteristics by application, the method includes: preparing ink and filling an inkjet device having an ink ejection nozzle with the ink; preparing a substrate having a base layer including a first electrode; and positioning the inkjet device above the substrate, and causing the inkjet device to eject a drop of the ink onto the base layer, wherein, in the preparation of the ink, a value Z denoting a reciprocal of the Ohnesorge number Oh determined by density ρ (g/m3), surface tension γ (mN·m), and viscosity η (mPa·s) of the ink and a diameter r (mm) of the ink ejection nozzle satisfies Formula 1, in the ejection of the drop of the ink, speed V (m/s) of the ejected drop satisfies Formula 2, and the value Z and the speed V (m/s) satisfy Formula 3.

摘要翻译： 为了提供一种通过应用有效地制造具有优异发光特性的有机发光元件的方法，该方法包括：制备油墨并用具有油墨的具有喷墨嘴的喷墨装置进行填充; 制备具有包括第一电极的基层的基板; 并将喷墨装置定位在基板上方，并使喷墨装置将一滴墨喷射到基层上，其中，在制备墨时，表示由密度＆rgr确定的Ohnesorge数的倒数的值Z ; （g / m 3），表面张力γ（mN·m），粘度＆ （mPa·s）和喷墨嘴的直径r（mm）满足式1，在喷墨滴下时，喷射液滴的速度V（m / s）满足式2，并且 值Z和速度V（m / s）满足公式3。

公开(公告)号：US09373822B2

公开(公告)日：2016-06-21

申请号：US13978018

申请日：2011-01-19

申请人： Hirotaka Nanno ,  Shinichiro Ishino ,  Tomoki Masuda ,  Yuko Kawanami ,  Noriyuki Matsusue

发明人： Hirotaka Nanno ,  Shinichiro Ishino ,  Tomoki Masuda ,  Yuko Kawanami ,  Noriyuki Matsusue

IPC分类号： H01L21/00 ,  H01L51/56 ,  H01L51/00 ,  H01L51/50 ,  H05B33/10

CPC分类号： H01L51/56 ,  H01L51/0005 ,  H01L51/0007 ,  H01L51/50 ,  H01L51/5012 ,  H05B33/10

摘要： To provide a method of efficiently manufacturing an organic light-emitting element with excellent light-emitting characteristics by application, the method includes: preparing ink and filling an inkjet device having an ink ejection nozzle with the ink; preparing a substrate having a base layer including a first electrode; and positioning the inkjet device above the substrate, and causing the inkjet device to eject a drop of the ink onto the base layer, wherein, in the preparation of the ink, a value Z denoting a reciprocal of the Ohnesorge number Oh determined by density ρ (g/dm3), surface tension γ (mN/m), and viscosity η (mPa·s) of the ink and a diameter r (mm) of the ink ejection nozzle satisfies Formula 1, in the ejection of the drop of the ink, speed V (m/s) of the ejected drop satisfies Formula 2, and the value Z and the speed V (m/s) satisfy Formula 3.

摘要翻译： 为了提供一种通过应用有效地制造具有优异发光特性的有机发光元件的方法，该方法包括：制备油墨并用具有油墨的具有喷墨嘴的喷墨装置进行填充; 制备具有包括第一电极的基层的基板; 并将喷墨装置定位在基板上方，并使喷墨装置将一滴墨喷射到基层上，其中，在制备墨时，表示由密度＆rgr确定的Ohnesorge数的倒数的值Z ; （g / dm3），表面张力γ（mN / m）和粘度＆ （mPa·s）和喷墨嘴的直径r（mm）满足式1，在喷墨滴下时，喷射液滴的速度V（m / s）满足式2，并且 值Z和速度V（m / s）满足公式3。

公开(公告)号：US09023239B2

公开(公告)日：2015-05-05

申请号：US13641892

申请日：2011-09-28

申请人： Yuko Kawanami ,  Shinichiro Ishino ,  Tomoki Masuda ,  Hirotaka Nanno ,  Noriyuki Matsusue

发明人： Yuko Kawanami ,  Shinichiro Ishino ,  Tomoki Masuda ,  Hirotaka Nanno ,  Noriyuki Matsusue

IPC分类号： H01L51/50 ,  H05B33/10 ,  H05B33/12 ,  H05B33/22 ,  C09D11/02 ,  H01L51/00 ,  H01L27/32

CPC分类号： C09D11/02 ,  H01L27/3246 ,  H01L51/0005 ,  H01L51/5012 ,  H01L2251/55

摘要： An ink for an organic light-emitting element includes a first solvent, a second solvent, and a functional material. The first and second solvents have equal or similar boiling points. The first solvent is such that an imitatively formed functional layer formed by replacing the second solvent with the first solvent, in a light-emitting region of an organic light-emitting element, is thicker at both end portions than at a central portion and the top surfaces of the end portions are positioned higher than the top surface of the central portion. The second solvent is such that an imitatively formed functional layer formed by replacing the first solvent with the second solvent, in a light-emitting region of an organic light-emitting element, is thicker at a central portion than at both end portions and the top surface of the central portion is positioned higher than the top surfaces of the end portions.

摘要翻译： 用于有机发光元件的墨包括第一溶剂，第二溶剂和功能材料。 第一和第二溶剂具有相同或相似的沸点。 第一溶剂使得在有机发光元件的发光区域中通过用第一溶剂置换第二溶剂而形成的模仿功能层在两个端部处比在中心部分更厚，并且顶部 端部的表面定位成高于中心部分的顶表面。 第二溶剂使得在有机发光元件的发光区域中通过用第二溶剂置换第一溶剂而形成的模仿功能层在中心部分比在两个端部处和顶部的顶部更厚 中心部分的表面定位成高于端部的顶表面。

公开(公告)号：US20130292667A1

公开(公告)日：2013-11-07

申请号：US13996132

申请日：2011-01-19

申请人： Hirotaka Nanno ,  Shinichiro Ishino ,  Tomoki Masuda ,  Yuko Kawanami ,  Noriyuki Matsusue

发明人： Hirotaka Nanno ,  Shinichiro Ishino ,  Tomoki Masuda ,  Yuko Kawanami ,  Noriyuki Matsusue

IPC分类号： H01L51/56 ,  B41J2/17 ,  H01L51/52

CPC分类号： H01L51/56 ,  B41J2/145 ,  B41J2/17 ,  B41J2202/09 ,  H01L51/0005 ,  H01L51/0007 ,  H01L51/52 ,  H05B33/10

摘要： To provide a method of efficiently manufacturing an organic light-emitting element with excellent light-emitting characteristics by application, the method includes: preparing ink and filling an inkjet device having an ink ejection nozzle with the ink; preparing a substrate having a base layer including a first electrode; and positioning the inkjet device above the substrate, and causing the inkjet device to eject a drop of the ink onto the base layer, wherein, in the preparation of the ink, a value Z denoting a reciprocal of the Ohnesorge number Oh determined by density ρ (g/m3), surface tension γ (mN·m), and viscosity η (mPa·s) of the ink and a diameter r (mm) of the ink ejection nozzle satisfies Formula 1, in the ejection of the drop of the ink, speed V (m/s) of the ejected drop satisfies Formula 2, and the value Z and the speed V (m/s) satisfy Formula 3.

摘要翻译： 为了提供一种通过应用有效地制造具有优异发光特性的有机发光元件的方法，该方法包括：制备油墨并用具有油墨的具有喷墨嘴的喷墨装置进行填充; 制备具有包括第一电极的基层的基板; 并将喷墨装置定位在基板上方，并使喷墨装置将一滴墨喷射到基层上，其中，在制备墨时，表示由密度rho确定的Ohnesorge数Oh的倒数的值Z （g / m 3），表面张力γ（mN·m）和粘度η（mPa·s）和墨喷射嘴的直径r（mm）满足式1，在喷出液滴 墨水，喷射液滴的速度V（m / s）满足式2，并且值Z和速度V（m / s）满足公式3。

公开(公告)号：US20130285032A1

公开(公告)日：2013-10-31

申请号：US13978013

申请日：2011-01-19

申请人： Hirotaka Nanno ,  Shinichiro Ishino ,  Tomoki Masuda ,  Yuko Kawanami ,  Noriyuki Matsusue

发明人： Hirotaka Nanno ,  Shinichiro Ishino ,  Tomoki Masuda ,  Yuko Kawanami ,  Noriyuki Matsusue

IPC分类号： H01L51/00 ,  H01L51/50

CPC分类号： H01L51/0005 ,  H01L51/0007 ,  H01L51/5012 ,  H01L51/56 ,  H05B33/10

摘要： To provide a method of efficiently manufacturing an organic light-emitting element with excellent light-emitting characteristics by application, the method includes: preparing ink and filling an inkjet device having an ink ejection nozzle with ink; preparing a substrate having a base layer including a first electrode; and positioning the inkjet device above the substrate, and causing the inkjet device to eject a drop of the ink onto the base layer, wherein, in the preparation of the ink, a value Z denoting a reciprocal of the Ohnesorge number Oh determined by density ρ (g/m3), surface tension γ (mN·m), and viscosity η (mPa·s) of the ink and a diameter r (mm) of the ink ejection nozzle satisfies Formula 1, in the ejection of the drop of the ink, speed V (m/s) of the ejected drop satisfies Formula 2, and the value Z and the speed V (m/s) satisfy Formula 3.

摘要翻译： 为了提供一种通过应用有效地制造具有优异的发光特性的有机发光元件的方法，该方法包括：制备墨水并用具有墨水的具有喷墨嘴的喷墨装置进行填充; 制备具有包括第一电极的基层的基板; 并将喷墨装置定位在基板上方，并使喷墨装置将一滴墨喷射到基层上，其中，在制备墨时，表示由密度rho确定的Ohnesorge数Oh的倒数的值Z （g / m 3），表面张力γ（mN·m）和粘度η（mPa·s）和墨喷射嘴的直径r（mm）满足式1，在喷出液滴 墨水，喷射液滴的速度V（m / s）满足式2，并且值Z和速度V（m / s）满足公式3。