公开(公告)号：US07977513B2

公开(公告)日：2011-07-12

申请号：US12438025

申请日：2007-08-06

申请人： Shinya Tachibana ,  Ryuji Yoshiyama ,  Tsuyoshi Oishi ,  Mikiya Sakurai ,  Kazuo Ishida ,  Tatsuya Tsujiuchi ,  Hidehisa Mita ,  Ryosuke Araki ,  Kenji Saito

发明人： Shinya Tachibana ,  Ryuji Yoshiyama ,  Tsuyoshi Oishi ,  Mikiya Sakurai ,  Kazuo Ishida ,  Tatsuya Tsujiuchi ,  Hidehisa Mita ,  Ryosuke Araki ,  Kenji Saito

IPC分类号： C07C213/00 ,  C07C213/04

CPC分类号： C07C213/04 ,  C07C213/10 ,  C07C215/08

摘要： An amine producing apparatus includes a reactor that reacts a mono-lower-alkylamine and an alkylene oxide, an unreacted-raw-material-recovery distillation column that separates unreacted raw materials by distillation from a product including unreacted raw materials obtained in the reactor, a non-aqueous distillation column that removes water and a light component by a distillation method from a reactive product from which unreacted raw material have been separated, and a purification and distillation column that separates by distillation a desired reactive product (mono-lower-alkylmonoalkanolamine) and residue (mono-lower-alkyldialkanolamine which is a dimer) from a reactive product from which the water and the light component have been removed.

摘要翻译： 胺生产装置包括使单低级烷基胺和环氧烷反应的反应器，通过蒸馏将未反应原料与包含反应器中得到的未反应原料的产物分离的未反应原料回收蒸馏塔， 通过蒸馏法从未反应的原料分离出的反应性产物中除去水和轻质成分的非水蒸馏塔和通过蒸馏分离所需的反应性产物（单低级烷基单链烷醇胺）的纯化和蒸馏塔， 和去除水和轻组分的反应产物的残基（单 - 低级 - 烷基二烷醇胺，其是二聚体）。

公开(公告)号：US20100249463A1

公开(公告)日：2010-09-30

申请号：US12438025

申请日：2007-08-06

申请人： Shinya Tachibana ,  Ryuji Yoshiyama ,  Tsuyoshi Oishi ,  Mikiya Sakurai ,  Kazuo Ishida ,  Tatsuya Tsujiuchi ,  Hidehisa Mita ,  Ryosuke Araki ,  Kenji Saito

发明人： Shinya Tachibana ,  Ryuji Yoshiyama ,  Tsuyoshi Oishi ,  Mikiya Sakurai ,  Kazuo Ishida ,  Tatsuya Tsujiuchi ,  Hidehisa Mita ,  Ryosuke Araki ,  Kenji Saito

IPC分类号： C07C215/08 ,  B01J8/00

CPC分类号： C07C213/04 ,  C07C213/10 ,  C07C215/08

摘要： An amine producing apparatus includes a reactor that reacts a mono-lower-alkylamine and an alkylene oxide, an unreacted-raw-material-recovery distillation column that separates unreacted raw materials by distillation from a product including unreacted raw materials obtained in the reactor, a non-aqueous distillation column that removes water and a light component by a distillation method from a reactive product from which unreacted raw material have been separated, and a purification and distillation column that separates by distillation a desired reactive product (mono-lower-alkylmonoalkanolamine) and residue (mono-lower-alkyldialkanolamine which is a dimer) from a reactive product from which the water and the light component have been removed.

摘要翻译： 胺生产装置包括使单低级烷基胺和环氧烷反应的反应器，通过蒸馏将未反应原料与包含反应器中得到的未反应原料的产物分离的未反应原料回收蒸馏塔， 通过蒸馏法从未反应的原料分离出的反应性产物中除去水和轻质成分的非水蒸馏塔和通过蒸馏分离所需的反应性产物（单低级烷基单链烷醇胺）的纯化和蒸馏塔， 和去除水和轻组分的反应产物的残基（单 - 低级 - 烷基二烷醇胺，其是二聚体）。

公开(公告)号：US08415502B2

公开(公告)日：2013-04-09

申请号：US12994599

申请日：2008-10-24

申请人： Tatsuya Tsujiuchi ,  Shinya Tachibana ,  Tsuyoshi Oishi ,  Tomio Mimura ,  Yasuyuki Yagi ,  Hidehisa Mita ,  Ryosuke Araki ,  Kenji Saito

发明人： Tatsuya Tsujiuchi ,  Shinya Tachibana ,  Tsuyoshi Oishi ,  Tomio Mimura ,  Yasuyuki Yagi ,  Hidehisa Mita ,  Ryosuke Araki ,  Kenji Saito

IPC分类号： C07C213/04

CPC分类号： C07C213/10 ,  C07C213/04 ,  C07C215/08

摘要： A reaction column (12) to which a raw material mixture (11) containing a mono-lower-alkylamine (AA: raw material I) and an alkylene oxide (AO: raw material II) is supplied, an unreacted raw material distillation column (14) that separates an unreacted raw material (15) from a reaction product (13a) (containing the unreacted raw material (15), a target reaction product (monomer) (17), and a by-product (dimer) (18)), and a flash drum (16) to which a reaction product (13b) (containing the target reaction product (monomer) (17) and the by-product (dimer) (18)) is supplied, the flash drum (16) separating a mono-lower-alkyl monoalkanolamine (monomer, the target reaction product 17) in a gas state, are provided.

摘要翻译： 将供给含有单低级烷基胺（AA：原料I）和环氧烷（AO：原料II））的原料混合物（11）的反应塔（12），未反应原料蒸馏塔 14），将未反应的原料（15）与反应产物（13a）（含有未反应的原料（15）），目标反应产物（单体）（17）和副产物（二聚体）（18）分离， ）和提供有反应产物（13b）（含有目标反应产物（单体）（17）和副产物（二聚体）（18））的闪蒸筒），闪蒸鼓（16） 分离出气态下的单低级烷基单烷醇胺（单体，目标反应产物17）。

公开(公告)号：US20110071318A1

公开(公告)日：2011-03-24

申请号：US12994599

申请日：2008-10-24

申请人： Tatsuya Tsujiuchi ,  Shinya Tachibana ,  Tsuyoshi Oishi ,  Tomio Mimura ,  Yasuyuki Yagi ,  Hidehisa Mita ,  Ryosuke Araki ,  Kenji Saito

发明人： Tatsuya Tsujiuchi ,  Shinya Tachibana ,  Tsuyoshi Oishi ,  Tomio Mimura ,  Yasuyuki Yagi ,  Hidehisa Mita ,  Ryosuke Araki ,  Kenji Saito

IPC分类号： C07C213/04 ,  B01J19/00

CPC分类号： C07C213/10 ,  C07C213/04 ,  C07C215/08

摘要： A reaction column (12) to which a raw material mixture (11) containing a mono-lower-alkylamine (AA: raw material I) and an alkylene oxide (AO: raw material II) is supplied, an unreacted raw material distillation column (14) that separates an unreacted raw material (15) from a reaction product (13a) (containing the unreacted raw material (15), a target reaction product (monomer) (17), and a by-product (dimer) (18)), and a flash drum (16) to which a reaction product (13b) (containing the target reaction product (monomer) (17) and the by-product (dimer) (18)) is supplied, the flash drum (16) separating a mono-lower-alkyl monoalkanolamine (monomer, the target reaction product 17) in a gas state, are provided.

摘要翻译： 将供给含有单低级烷基胺（AA：原料I）和环氧烷（AO：原料II））的原料混合物（11）的反应塔（12），未反应原料蒸馏塔 14），将未反应的原料（15）与反应产物（13a）（含有未反应的原料（15）），目标反应产物（单体）（17）和副产物（二聚体）（18）分离， ）和提供有反应产物（13b）（含有目标反应产物（单体）（17）和副产物（二聚体）（18））的闪蒸筒），闪蒸鼓（16） 分离出气态下的单低级烷基单烷醇胺（单体，目标反应产物17）。

公开(公告)号：US07732100B2

公开(公告)日：2010-06-08

申请号：US11916873

申请日：2006-06-02

申请人： Masataka Wakihara ,  Masayuki Seki ,  Hidehisa Mita

发明人： Masataka Wakihara ,  Masayuki Seki ,  Hidehisa Mita

IPC分类号： H01M10/40 ,  H01M6/18

CPC分类号： H01M10/0565 ,  H01M6/166 ,  H01M6/168 ,  H01M6/181 ,  H01M10/0525 ,  H01M10/056 ,  H01M2300/0085

摘要： The invention provides a novel lithium-ion battery electrolyte which is produced by adding an aluminate ester compound as a plasticizer in a solid polymer electrolyte. The lithium-ion battery solid polymer electrolyte of the present invention comprises a lithium ion source, an organic polymer compound, and one or more kinds of aluminate ester compounds represented by the general formula where R1, R2, and R3 each independently represent a straight-chain or branched-chain lower alkyl group having one to eight carbon atoms, an alkenyl group having three to six carbon atoms, acryloyl, or methacryloyl; OA1, OA2, and OA3 each independently represent an oxyalkylene group having two to four carbon atoms; l represents a number from 1 to 100; and m and n each independently represent a number from 0 to 100.

摘要翻译： 本发明提供了一种新型的锂离子电池电解质，其通过在固体聚合物电解质中添加铝酸酯化合物作为增塑剂而制备。 本发明的锂离子电池固体聚合物电解质包含锂离子源，有机高分子化合物和由通式表示的一种或多种铝酸酯化合物，其中R 1，R 2和R 3各自独立地表示直链， 具有1-8个碳原子的链或支链低级烷基，具有3-6个碳原子的链烯基，丙烯酰基或甲基丙烯酰基; OA1，OA2和OA3各自独立地表示具有2至4个碳原子的氧化烯基团; l表示1〜100的数; m和n各自独立地表示0〜100的数。

公开(公告)号：US20090104538A1

公开(公告)日：2009-04-23

申请号：US11916873

申请日：2006-06-02

申请人： Masataka Wakihara ,  Masayuki Seki ,  Hidehisa Mita

发明人： Masataka Wakihara ,  Masayuki Seki ,  Hidehisa Mita

IPC分类号： H01M10/40 ,  H01M6/18

CPC分类号： H01M10/0565 ,  H01M6/166 ,  H01M6/168 ,  H01M6/181 ,  H01M10/0525 ,  H01M10/056 ,  H01M2300/0085

摘要： The invention provides a novel lithium-ion battery electrolyte which is produced by adding an aluminate ester compound as a plasticizer in a solid polymer electrolyte. The lithium-ion battery solid polymer electrolyte of the present invention comprises a lithium ion source, an organic polymer compound, and one or more kinds of aluminate ester compounds represented by the general formula where R1, R2, and R3 each independently represent a straight-chain or branched-chain lower alkyl group having one to eight carbon atoms, an alkenyl group having three to six carbon atoms, acryloyl, or methacryloyl; OA1, OA2, and OA3 each independently represent an oxyalkylene group having two to four carbon atoms; l represents a number from 1 to 100; and m and n each independently represent a number from 0 to 100.

摘要翻译： 本发明提供了一种新型锂离子电池电解质，其通过在固体聚合物电解质中添加铝酸酯化合物作为增塑剂而制备。 本发明的锂离子电池固体高分子电解质包含锂离子源，有机高分子化合物以及由通式表示的一种或多种铝酸酯化合物，其中R 1，R 2和R 3各自独立地表示直链， 具有1-8个碳原子的链或支链低级烷基，具有3-6个碳原子的链烯基，丙烯酰基或甲基丙烯酰基; OA1，OA2和OA3各自独立地表示具有2至4个碳原子的氧化烯基团; l表示1〜100的数; m和n各自独立地表示0〜100的数。