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1.发明授权
公开(公告)号：US4403056A
公开(公告)日：1983-09-06
申请号：US228780
申请日：1981-01-30
CPC分类号： C08K5/109
摘要： A carbonate ester of the formula: ##STR1## where n is an integer of from 0 to 4 and m is an integer of from 8 to 14 and carbonate ester compositions containing at least one of such compounds are disclosed. These compounds or compositions can be added to vinyl chloride polymer compositions to plasticize said compositions.
摘要翻译： 一种下式的碳酸酯：其中n为0-4的整数，m为8-14的整数，并且公开了含有至少一种这些化合物的碳酸酯组合物。 这些化合物或组合物可以加入到氯乙烯聚合物组合物中，以塑化所述组合物。
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公开(公告)号：US4378320A
公开(公告)日：1983-03-29
申请号：US204967
申请日：1980-11-07
摘要： Tertiary-butylphenyl diphenyl phosphate esters in which the nominal molar ratio of tertiary-butyl radicals to phenyl radicals ranges from about 1:5 to about 1:2, the meta-tertiary-butylphenyl content ranges from about 25% to about 100 % and the ortho-tertiary-butylphenyl content is less than about 50% are highly effective plasticizers for vinyl chloride polymer compositions.
摘要翻译： 叔丁基苯基二苯基磷酸酯，其中叔丁基与苯基的标称摩尔比为约1:5至约1:2，间叔丁基苯基含量为约25％至约100％， 邻 - 叔丁基苯基含量低于约50％是用于氯乙烯聚合物组合物的高效增塑剂。
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公开(公告)号：US4103096A
公开(公告)日：1978-07-25
申请号：US841626
申请日：1977-10-13
CPC分类号： C07C37/00
摘要： Meta-alkylphenols are prepared by the isomerization of nonmeta-alkylphenols in the presence of trifluoromethane sulfonic acid. Ortho-isomer-containing alkylphenols are isomerized to increase their meta-isomer content and reduce their ortho-isomer content.
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公开(公告)号：US3931365A
公开(公告)日：1976-01-06
申请号：US535887
申请日：1974-12-23
摘要： A method for decolorizing and stabilizing alkylphenyl esters of phosphoric acid which comprises contacting the esters with an effective amount of a water soluble salt of a reduced form of sulfur for a sufficient length of time to decolorize and stabilize the esters against subsequent color formation.
摘要翻译： 一种使磷酸烷基苯基酯脱色和稳定的方法，该方法包括使酯与有效量的还原硫形式的水溶性盐接触足够长的时间以使酯脱色并稳定酯以防止随后的颜色形成。
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公开(公告)号：US4559184A
公开(公告)日：1985-12-17
申请号：US551641
申请日：1983-11-14
CPC分类号： C07F9/12
摘要： Triarylphosphates are prepared by phosphorylation of alkylphenols without use of phosphorylation catalyst. An improved phosphorylation step includes preheating alkylphenol feedstock to 150.degree. C. and completing reaction at 215.degree. C. or above in the presence of a stoichiometric excess of alkylphenol. The absence of phosphorylation catalyst simplifies distillative purification of reaction product by eliminating the need to withdraw purified product as distillate.
摘要翻译： 通过磷酸化烷基酚而不使用磷酸化催化剂制备磷酸三芳基酯。 改进的磷酸化步骤包括将烷基酚原料预热至150℃，并在化学计量过量的烷基酚存在下在215℃或更高温度下完成反应。 缺乏磷酸化催化剂通过消除将纯化产物作为馏出物抽出的需要来简化反应产物的蒸馏净化。
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6.发明授权Vinyl chloride compositions plasticized with meta-tertiary-butylphenyl diphenyl phosphate 失效用叔叔丁基苯基二苯基磷酸酯增塑的氯乙烯组合物
公开(公告)号：US4280945A
公开(公告)日：1981-07-28
申请号：US91633
申请日：1979-11-05
CPC分类号： C08K5/523
摘要： Tertiary-butylphenyl diphenyl phosphate esters in which the nominal molar ratio of tertiary-butyl radicals to phenyl radicals ranges from about 1:5 to about 1:2, the meta-tertiary-butylphenyl content ranges from about 25% to about 100% and the ortho-tertiary-butylphenyl content is less than about 50% are highly effective plasticizers for vinyl chloride polymer compositions.
摘要翻译： 叔丁基苯基二苯基磷酸酯，其中叔丁基与苯基的标称摩尔比为约1:5至约1:2，间叔丁基苯基含量为约25％至约100％， 邻 - 叔丁基苯基含量低于约50％是用于氯乙烯聚合物组合物的高效增塑剂。
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公开(公告)号：US4163767A
公开(公告)日：1979-08-07
申请号：US873468
申请日：1978-01-30
申请人： Silvio L. Giolito
发明人： Silvio L. Giolito
CPC分类号： C08G79/04 , C08G18/5078
摘要： A polyphosphorous mixed phosphite-phosphonate polymer flame retardant having an OH number less than one and containing both alkyl phosphite and haloalkyl phosphonate linkages.
摘要翻译： 具有OH值小于1且含有亚磷酸烷基酯和卤代烷基膦酸酯键的多磷混合亚磷酸酯 - 膦酸酯聚合物阻燃剂。
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8.发明授权Process for producing low temperature stable tert-butylphenyl diphenyl phosphate 失效生产低温稳定性叔丁基苯基二苯基磷酸酯的方法
公开(公告)号：US4414161A
公开(公告)日：1983-11-08
申请号：US279389
申请日：1981-07-01
申请人： Silvio L. Giolito
发明人： Silvio L. Giolito
摘要： A process for producing tert-butylphenyl diphenyl phosphate which is stable at low temperature by a process wherein phenol is butylated to produce tert-butylphenol which is isomerized to produce mixed meta and para isomers thereof, and which thereafter is alkylated with isobutylene to produce tert-butylphenol having a C.sub.4 /.phi. ratio of about 0.62. The tert-butylphenol is then phosphorylated to the tert-butylphenyl diphenyl phosphate meta/para mixture with phosphorus oxychloride. The disclosed process provides a tert-butylphenyl diphenyl phosphate which will not freeze or gel at low temperatures.
摘要翻译： 一种制备叔丁基苯基二苯基磷酸酯的方法，该方法通过以下方法在低温下稳定，其中苯酚被丁基化以产生叔丁基苯酚，其被异构化以产生其混合的间位和对位异构体，然后用异丁烯进行烷基化， C4 / Phi比为约0.62的丁基苯酚。 然后将叔丁基苯酚用磷酰氯磷酸化成叔丁基苯基二苯基磷酸酯/对 - 混合物。 所公开的方法提供了在低温下不会冷冻或凝胶化的叔丁基苯基二苯基磷酸酯。
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公开(公告)号：US3993692A
公开(公告)日：1976-11-23
申请号：US824358
申请日：1969-04-30
IPC分类号： C07C303/16 , C07C309/80 , C07C143/70
CPC分类号： C07C303/16
摘要： A continuous process for preparing methane sulfonyl chloride by the reaction of methyl mercaptan with chlorine in the presence of an aqueous bath of hydrogen chloride at an elevated temperature.
摘要翻译： 在高温下在氯化氢水溶液存在下，通过甲硫醇与氯反应制备甲磺酰氯的连续方法。
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公开(公告)号：US3931366A
公开(公告)日：1976-01-06
申请号：US535888
申请日：1974-12-23
摘要： A method for decolorizing and stabilizing alkylphenyl esters of phosphoric acid which comprises the in situ addition of an effective amount of PCl.sub.3 to the POCL.sub.3 reacted with an alkyl phenol so as to produce a decolorized and stabilized phosphate ester.
摘要翻译： 一种使磷酸烷基苯基酯脱色和稳定的方法，其包括将有效量的PCl 3原位加入到与烷基酚反应的POCl 3中，以产生脱色和稳定的磷酸酯。
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