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1.发明授权Organic matrix composite structures and thermal oxidative barrier coating therefor 有权有机基质复合结构及其热氧化屏障涂层公开(公告)号：US07776434B2
公开(公告)日：2010-08-17
申请号：US11965964
申请日：2007-12-28
CPC分类号： B32B27/08 , Y10T428/25 , Y10T428/254 , Y10T428/259 , Y10T428/31663 , Y10T428/31667 , Y10T428/31721
摘要： A tailorable polyimide resin system may be used to form an organic matrix composite (OMC) structure for use in high temperature applications. A thermal oxidative barrier coating on the OMC may include a bond coat comprising a tailorable polyimide resin system. The bond coat may include nano-particles such as clay platelets, graphite flakes or a polyhedral oligomeric silsesquioxane. The coating system may include a thermal barrier layer including a silsesquioxane or an inorganic polymer. The tailorable polyimide resin system includes first and second independent prepolymer components able to impart desired properties in the prepolymer blend or the crosslinked polyimide matrix.
摘要翻译： 可以使用可调节的聚酰亚胺树脂体系形成用于高温应用的有机基质复合（OMC）结构。 OMC上的热氧化屏障涂层可以包括包含可调节的聚酰亚胺树脂体系的粘合涂层。 粘合涂层可以包括纳米颗粒，例如粘土片晶，石墨薄片或多面体低聚倍半硅氧烷。 涂层系统可以包括包含硅倍半氧烷或无机聚合物的热障层。 可调节的聚酰亚胺树脂体系包括能够在预聚物共混物或交联的聚酰亚胺基质中赋予所需性质的第一和第二独立的预聚物组分。
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2.发明授权RTM and RI processible tailorable polyimide resin systems and composite articles formed therefrom 有权RTM和RI可加工的可定制的聚酰亚胺树脂体系和由其形成的复合制品公开(公告)号：US08030433B2
公开(公告)日：2011-10-04
申请号：US11965071
申请日：2007-12-27
IPC分类号： C08G69/02
CPC分类号： C08G73/00 , C08L79/08 , C08L2205/02 , C08L2666/20
摘要： Tailorable polyimide resin systems suitable for processing by resin transfer molding (RTM) and resin infusion (RI) methods. An exemplary resin system includes first and second prepolymer components present in respective amounts to provide the desired processibility. The cured polyimide system exhibits high glass transition temperature and other properties required for gas turbine engine applications. The first and second prepolymer components independently comprise a monomeric mixture or a reaction product of a diamine component, a dianhydride component, and an end group component.
摘要翻译： 适用于通过树脂传递模塑（RTM）和树脂注入（RI）方法加工的可聚酰亚胺树脂体系。 示例性树脂体系包括以各自量存在的第一和第二预聚物组分以提供所需的加工性。 固化的聚酰亚胺系统表现出高的玻璃化转变温度和燃气涡轮发动机应用所需的其它性能。 第一和第二预聚物组分独立地包含单体混合物或二胺组分，二酐组分和端基组分的反应产物。
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3.发明申请RTM and RI Processible Tailorable Polyimide Resin Systems and Composite Articles Formed Therefrom 有权RTM和RI可加工的可折叠聚酰亚胺树脂体系和复合制品公开(公告)号：US20080146769A1
公开(公告)日：2008-06-19
申请号：US11965071
申请日：2007-12-27
CPC分类号： C08G73/00 , C08L79/08 , C08L2205/02 , C08L2666/20
摘要： Tailorable polyimide resin systems suitable for processing by resin transfer molding (RTM) and resin infusion (RI) methods. An exemplary resin system includes first and second prepolymer components present in respective amounts to provide the desired processibility. The cured polyimide system exhibits high glass transition temperature and other properties required for gas turbine engine applications. The first and second prepolymer components independently comprise a monomeric mixture or a reaction product of a diamine component, a dianhydride component, and an end group component.
摘要翻译： 适用于通过树脂传递模塑（RTM）和树脂注入（RI）方法加工的可聚酰亚胺树脂体系。 示例性树脂体系包括以各自量存在的第一和第二预聚物组分以提供所需的加工性。 固化的聚酰亚胺系统表现出高的玻璃化转变温度和燃气涡轮发动机应用所需的其它性能。 第一和第二预聚物组分独立地包含单体混合物或二胺组分，二酐组分和端基组分的反应产物。
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4.发明申请Methods For Forming Composite Articles From Tailorable Polyimide Resin Systems using RTM and RI Techniques 有权使用RTM和RI技术形成可折叠聚酰亚胺树脂体系的复合制品的方法公开(公告)号：US20080154015A1
公开(公告)日：2008-06-26
申请号：US11965083
申请日：2007-12-27
IPC分类号： C08G73/00
CPC分类号： B29C70/48 , B29C70/543 , B29K2079/08 , B29K2105/243 , C08L79/08 , C08L2205/02 , C08L2666/20
摘要： A method for forming a polyimide composite article utilizes a polyimide resin system including at least a first prepolymer component and a second prepolymer component. A preform structure is tackified with the first prepolymer component. Using resin infusion or resin transfer molding techniques, the tackified preform structure is contacted with the second prepolymer component. The polyimide resin system is cured under suitable cure conditions so that the first and second prepolymer components mix and react to produce the polyimide composite structure.
摘要翻译： 一种形成聚酰亚胺复合制品的方法是使用至少包含第一预聚物组分和第二预聚物组分的聚酰亚胺树脂体系。 预成型结构用第一预聚物组分增粘。 使用树脂浸渍或树脂传递模塑技术，使增粘的预成型结构与第二预聚物组分接触。 聚酰亚胺树脂体系在合适的固化条件下固化，使得第一和第二预聚物组分混合并反应以产生聚酰亚胺复合结构。
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5.发明授权Methods for forming composite articles from tailorable polyimide resin systems using RTM and RI techniques 有权使用RTM和RI技术从可裁剪的聚酰亚胺树脂体系形成复合制品的方法公开(公告)号：US08030437B2
公开(公告)日：2011-10-04
申请号：US11965083
申请日：2007-12-27
IPC分类号： C08G73/00
CPC分类号： B29C70/48 , B29C70/543 , B29K2079/08 , B29K2105/243 , C08L79/08 , C08L2205/02 , C08L2666/20
摘要： A method for forming a polyimide composite article utilizes a polyimide resin system including at least a first prepolymer component and a second prepolymer component. A preform structure is tackified with the first prepolymer component. Using resin infusion or resin transfer molding techniques, the tackified preform structure is contacted with the second prepolymer component. The polyimide resin system is cured under suitable cure conditions so that the first and second prepolymer components mix and react to produce the polyimide composite structure.
摘要翻译： 一种形成聚酰亚胺复合制品的方法是使用至少包含第一预聚物组分和第二预聚物组分的聚酰亚胺树脂体系。 预成型结构用第一预聚物组分增粘。 使用树脂浸渍或树脂传递模塑技术，使增粘的预成型结构与第二预聚物组分接触。 聚酰亚胺树脂体系在合适的固化条件下固化，使得第一和第二预聚物组分混合并反应以产生聚酰亚胺复合结构。
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公开(公告)号：US20100196729A1
公开(公告)日：2010-08-05
申请号：US12363741
申请日：2009-01-31
申请人： Stephen Mark Whiteker , Lisa Vinciguerra Shafer , Warren Rosal Ronk , William Evan McCormack , Joseph Thomas Begovich, JR.
发明人： Stephen Mark Whiteker , Lisa Vinciguerra Shafer , Warren Rosal Ronk , William Evan McCormack , Joseph Thomas Begovich, JR.
CPC分类号： C08G73/1014 , B29C35/0227 , B29C35/0288 , B29C70/44 , B29K2079/08 , B29L2031/08 , C08G73/1007 , C08G73/1042 , C08J5/04 , C08J5/24 , C08J2379/08 , C08K7/02 , C08L79/08 , Y10T428/31721
摘要： Method includes forming a preform utilizing a polyimide resin-impregnated fiber-reinforced layers; removing solvent from the system at initial vacuum, pressure, and temperature conditions for an initial time interval sufficient to remove substantially all the solvent; imidizing the polyimide resin system under second vacuum, pressure, and temperature conditions for a second time interval sufficient to substantially completely imidize the polyimide resin; consolidating the preform following imidization under third vacuum, pressure, and temperature conditions and including applying pressure to the preform when the preform is at a predetermined temperature; and solidifying the preform under fourth vacuum, pressure, and temperature conditions to provide a cured laminate structure having a shape of a turbine engine component. A method is provided for designing the polyimide resin overall cure cycle dependent on the desired outcome at the solvent removal stage, the imidization stage, the consolidation stage, and the solidification stage.
摘要翻译： 方法包括使用聚酰亚胺树脂浸渍的纤维增强层来形成预制件; 在初始真空，压力和温度条件下从系统中除去溶剂，初始时间间隔足以除去基本上所有的溶剂; 在第二真空，压力和温度条件下将聚酰亚胺树脂体系酰亚胺化第二时间间隔，足以基本上完全酰亚胺化聚酰亚胺树脂; 在第三真空，压力和温度条件下，在酰亚胺化之后固化预成型件，并且包括当预制件处于预定温度时对预成型件施加压力; 并在第四真空，压力和温度条件下固化预成型件，以提供具有涡轮发动机部件形状的固化层压结构。 提供了一种用于根据在溶剂去除阶段，酰亚胺化阶段，固结阶段和凝固阶段期望结果来设计聚酰亚胺树脂整体固化周期的方法。
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7.发明申请Organic Matrix Composite Structures and Thermal Oxidative Barrier Coating Therefor 有权有机矩阵复合结构及其热氧化阻挡涂层公开(公告)号：US20080213604A1
公开(公告)日：2008-09-04
申请号：US11965964
申请日：2007-12-28
IPC分类号： B32B13/12
CPC分类号： B32B27/08 , Y10T428/25 , Y10T428/254 , Y10T428/259 , Y10T428/31663 , Y10T428/31667 , Y10T428/31721
摘要： A tailorable polyimide resin system may be used to form an organic matrix composite (OMC) structure for use in high temperature applications. A thermal oxidative barrier coating on the OMC may include a bond coat comprising a tailorable polyimide resin system. The bond coat may include nano-particles such as clay platelets, graphite flakes or a polyhedral oligomeric silsesquioxane. The coating system may include a thermal barrier layer including a silsesquioxane or an inorganic polymer. The tailorable polyimide resin system includes first and second independent prepolymer components able to impart desired properties in the prepolymer blend or the crosslinked polyimide matrix.
摘要翻译： 可以使用可调节的聚酰亚胺树脂体系形成用于高温应用的有机基质复合（OMC）结构。 OMC上的热氧化屏障涂层可以包括包含可调节的聚酰亚胺树脂体系的粘合涂层。 粘合涂层可以包括纳米颗粒，例如粘土片晶，石墨薄片或多面体低聚倍半硅氧烷。 涂层系统可以包括包含硅倍半氧烷或无机聚合物的热障层。 可调节的聚酰亚胺树脂体系包括能够在预聚物共混物或交联的聚酰亚胺基质中赋予所需性质的第一和第二独立的预聚物组分。
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