Process for the recovery of perfluorinated sulphonic acids from spent acid residue
    2.
    发明授权
    Process for the recovery of perfluorinated sulphonic acids from spent acid residue 失效
    从废酸残渣中回收全氟磺酸的方法

    公开(公告)号:US06891076B2

    公开(公告)日:2005-05-10

    申请号:US10144709

    申请日:2002-05-15

    CPC分类号: C07C303/44 C07C309/06

    摘要: Process for the recovery of perfluorinated sulphonic acid from a hydrocarbon residue, comprising the steps of (a) treating the residue with an alkyl ammonium salt of the perfluorinated sulphonic acid or a mixture of an alkyl ammonium salt of the perfluorinated sulphonic acid and the perfluorinated sulphonic acid in an amount being effective to liquefy the residue at ambient temperature; (b) contacting the liquefied residue with water at conditions to obtaining an aqueous extract containing the perfluorinated sulphonic acid and/or the alkyl ammonium salt of the perfluorinated acid into water; and (c) separating water from the aqueous extract to recover the perfluorinated sulphonic acid or the mixture of the acid and the ammonium salt.

    摘要翻译: 从烃残基中回收全氟磺酸的方法,包括以下步骤:(a)用全氟磺酸的烷基铵盐或全氟磺酸的烷基铵盐与全氟磺酸的混合物处理残余物 酸的量在环境温度下有效液化残留物; (b)在获得含有全氟化磺酸和/或全氟酸的烷基铵盐的水性提取物的水的条件下使液化的残余物与水接触; 和(c)从水提取物中分离水以回收全氟磺酸或酸和铵盐的混合物。