公开(公告)号：US5290015A

公开(公告)日：1994-03-01

申请号：US842961

申请日：1992-02-28

申请人： Tatsuo Naritomi ,  Yoshinobu Toshida ,  Toshiyuki Ohta ,  Masaji Katsumaru ,  Hisayuki Wada ,  Takashi Banno ,  Tadayuki Choshi

发明人： Tatsuo Naritomi ,  Yoshinobu Toshida ,  Toshiyuki Ohta ,  Masaji Katsumaru ,  Hisayuki Wada ,  Takashi Banno ,  Tadayuki Choshi

IPC分类号： C22B5/04 ,  C22B5/16 ,  C22B34/12 ,  C22B34/14 ,  C22B34/00

CPC分类号： C22B34/1277 ,  C22B34/1263 ,  C22B34/1268 ,  C22B34/1272 ,  C22B34/14 ,  C22B5/04 ,  C22B5/16 ,  Y10S266/905

摘要： A method and apparatus for producing a high-melting-point and high-toughness metal, comprising: reducing a high-melting point and high-toughness metal chloride with an activated metal to form a high-melting-point and high-toughness sponge metal in a reducing vessel arranged sideways relative to a condensing vessel, wherein the condensing vessel is integrally connected to the reducing vessel through a conduit, and at least one of the reducing vessel and/or the condensing vessel is supported so as to move with thermal expansion of said conduit; and measuring a weight-change of the vessel supported so as to move with thermal expansion of the conduit to estimate the degree of progress of a separating and recovering process on the basis of the detected weight-change when nonreacted activated metal and its chloride remaining in the sponge metal formed in the reducing vessel are recovered into the condensing vessel by vacuum separation.

摘要翻译： 一种用于生产高熔点和高韧性金属的方法和设备，包括：用活化金属还原高熔点和高韧性的金属氯化物，以形成高熔点和高韧性的海绵金属 在相对于冷凝容器侧向排列的还原容器中，其中所述冷凝容器通过导管与所述还原容器一体连接，并且所述还原容器和/或冷凝容器中的至少一个被支撑以便随着热膨胀 的管道; 并且测量支撑的容器的重量变化，以便随着管道的热膨胀而移动，以基于检测到的重量变化来估计分离和回收过程的进行程度，当未反应的活化金属及其氯化物保持在 在还原容器中形成的海绵金属通过真空分离回收到冷凝容器中。