摘要:
The present invention provides a method of producing 2,4,6-tris(hydroxyphenyl)-1,3,5-triazine compound in which no rapid solidification or the like occurs and generation of by-products is suppressed, thereby enabling to reduce decrease in the yield.Particularly, the present invention is a method of producing 2,4,6-tris(hydroxyphenyl)-1,3,5-triazine compound represented by the following Formula (1): wherein the reaction between cyanuric halide compound represented by the following Formula (2): and hydroxyphenyl compound represented by the following Formula (3): is carried out by using, as the reaction solvent, a solvent containing sulfolane as the main component in the presence of a Lewis acid at an amount of 0.3 to 0.7 equivalent with respect to 1 equivalent of halogen atom of the cyanuric halide compound represented by the Formula (2), or by using a mixed solvent of inert solvent and cycloalkyl alkyl ether represented by the following Formula (4): Z1—O—Z2. (4)
摘要:
The present invention provides a method of producing 2,4,6-tris(hydroxyphenyl)-1,3,5-triazine compound in which no rapid solidification or the like occurs and generation of by-products is suppressed, thereby enabling to reduce decrease in the yield.Particularly, the present invention is a method of producing 2,4,6-tris(hydroxyphenyl)-1,3,5-triazine compound represented by the following Formula (1): wherein the reaction between cyanuric halide compound represented by the following Formula (2): and hydroxyphenyl compound represented by the following Formula (3): is carried out by using, as the reaction solvent, a solvent containing sulfolane as the main component in the presence of a Lewis acid at an amount of 0.3 to 0.7 equivalent with respect to 1 equivalent of halogen atom of the cyanuric halide compound represented by the Formula (2), or by using a mixed solvent of inert solvent and cycloalkyl alkyl ether represented by the following Formula (4): z1-0-z2 (4)
摘要:
A producing method of a high-purity pyrophosphate comprising a calcination of the orthophosphate under the condition of 120° C.-350° C.; and a producing method suitable for manufacturing effectively the high-purity melamine pyrophosphate.
摘要:
A sunscreen cosmetic composition contains an ultraviolet absorber composed of a triazine compound (a) represented by the general formula (1) below and a triazine compound (b) represented by chemical formula (2) below. In the general formula (I) below, R1 represents a linear or branched C1-12 alkyl group, a C3-8 cycloalkyl group, a C3-8 alkenyl group, a C6-18 aryl group, a C7-18 alkylaryl group, or a C7-18 arylalkyl group (with the proviso that these groups may be substituted by a hydroxy group, a halogen atom or a C1-12 alkyl or alkoxy group, and may be interrupted by an oxygen atom, a sulfur atom, a carbonyl group, an ester group, an amide group or an imino group, and further that the substitution and the interruption may be combined); and R2 represents a C1-8 alkyl group, or a C3-8 alkenyl group.
摘要:
A producing method of a high-purity pyrophosphate comprising a calcination of the orthophosphate under the condition of 120° C.-350° C.; and a producing method suitable for manufacturing effectively the high-purity melamine pyrophosphate.
摘要:
The present invention provides piperazine pyrophosphate represented by chemical formula (I) which has a sodium content of 10 ppm or lower and a process of producing the same. The piperazine pyrophosphate has high purity and provides a flame retardant composition exhibiting excellent flame retardancy. The process includes dehydration condensation of piperazine diphosphate and is able to produce the piperazine pyrophosphate at low cost.
摘要:
The process for producing a low acid value phosphoric ester of the present invention is characterized by comprising treating a phosphoric ester having an acid value with an organic ortho-acid ester. The phosphoric ester preferably has a specific structure. The organic ortho-acid ester is preferably an ester of orthoformic acid, orthoacetic acid or orthopropionic acid with an alkyl group having 1 to 4 carbon atoms.
摘要:
Disclosed is an optical film or optical sheet which is used for a polarizing plate using iodine as a dye or a liquid crystal display device using the polarizing plate. The optical film or optical sheet is made from a resin containing a triazine compound represented by general formula (1). [In the formula, R1 represents a linear or branched alkyl group having 1-12 carbon atoms, a cycloalkyl group having 3-8 carbon atoms, an alkenyl group having 3-8 carbon atoms, an aryl group having 6-18 carbon atoms, an alkylaryl group having 7-18 carbon atoms, or an arylalkyl group having 7-18 carbon atoms; and R2 represents an alkyl group having 1-8 carbon atoms or an alkenyl group having 3-8 carbon atoms.]
摘要:
The present invention provides piperazine pyrophosphate represented by chemical formula (I) which has a sodium content of 10 ppm or lower and a process of producing the same. The piperazine pyrophosphate has high purity and provides a flame retardant composition exhibiting excellent flame retardancy. The process includes dehydration condensation of piperazine diphosphate and is able to produce the piperazine pyrophosphate at low cost.
摘要:
A sunscreen cosmetic composition contains an ultraviolet absorber composed of a triazine compound (a) represented by the general formula (1) below and a triazine compound (b) represented by chemical formula (2) below. In the general formula (I) below, R1 represents a linear or branched C1-12 alkyl group, a C3-8 cycloalkyl group, a C3-8 alkenyl group, a C6-18 aryl group, a C7-18 alkylaryl group, or a C7-18 arylalkyl group (with the proviso that these groups may be substituted by a hydroxy group, a halogen atom or a C1-12 alkyl or alkoxy group, and may be interrupted by an oxygen atom, a sulfur atom, a carbonyl group, an ester group, an amide group or an imino group, and further that the substitution and the interruption may be combined); and R2 represents a C1-8 alkyl group, or a C3-8 alkenyl group.