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公开(公告)号：US3790562A
公开(公告)日：1974-02-05
申请号：US3790562D
申请日：1972-05-23
申请人： US AGRICULTURE
摘要： THIS INVENTION RELATES TO A METHOD FOR PREPARING CARBOHYDRATE-BORON ALKOXIDE COMPOUNDS. UNDER ANHYDROUS CONDITIONS, STABLE COMPOUNDS OF METHYL CELLULOSE AND BORON ALKOXIDES, SUCH AS BORON ETHOXIDE, BORON PROPOXIDE, AND BORON ISOPROPOXIDE, WERE PREPARED IN NEAT BORON ALKOXIDE, THE PARENT ALCOHOL, BENZENE, PYRIDINE, AND/OR ETHYLENEDIAMINE. THE METHOD OF THIX INVENTION HAS AS ITS OBJECTIVE INCREASING THE REACTIVITY OF METHYL CELLULOSE WITH BORON ALKOXIDES BY TREATMENT IN SOLUTIONS OF STRONG BASES, SUCH AS PYRIDINE AND ETHYLENEDIAMINE. FORMATION OF METHYL CELLULOSE-BORON ALKOXIDE COMPOUNDS MODIFIES THE RATE OF OXIDATION OF METHYL CELLULOSE AND IS RELATED TO PREPARING FLAME-RESISTANT PRODUCTS.
摘要翻译： 本发明涉及一种制备碳水化合物 - 硼醇盐化合物的方法。 在无水条件下，制备稳定的甲基-α-D-葡萄糖苷，甲基-α-甘露糖苷，蔗糖，纤维二糖，甲基纤维素和纤维素和硼醇的化合物，例如乙醇硼，硼氧化物和异丙醇硼 醇醇，母体醇，苯，吡啶和/或乙二胺。 本发明的方法的目的是通过在强碱如吡啶和乙二胺的溶液中处理来提高碳水化合物的反应性，因为它们的分子量增加。 碳水化合物 - 硼醇盐化合物的形成改变了碳水化合物的氧化速率，并且与制备阻燃产品有关。
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公开(公告)号：US3821196A
公开(公告)日：1974-06-28
申请号：US40640773
申请日：1973-10-15
申请人： US AGRICULTURE
摘要： Fibrous cotton cellulose boron isoproxide or boron propoxide. Under anhydrous conditions, stable compounds of cotton cellulose and boron isopropoxide or boron propoxide were prepared in the neat boron alkoxide, the parent alcohol, benzene, pyridine, and/or ethylenediamine. The method of this invention has as its objective increasing the reactivity of the cotton cellulose with boron isopropoxide or boron propoxide by treatment in solutions of strong bases, such as pyridine and ethylene diamine. Formation of the fibrous cotton cellulose-boron isopropoxide or boron propoxide modifies the rate of oxidation of the cotton cellulose and is related to preparing flame resistant products.
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