公开(公告)号：US20050022666A1

公开(公告)日：2005-02-03

申请号：US10628509

申请日：2003-07-29

申请人： Wen-Tzong Liu ,  Chia-Chang Lin ,  Sheng Yang ,  Tsung-Jen Ho ,  Hua-Tang Yu

发明人： Wen-Tzong Liu ,  Chia-Chang Lin ,  Sheng Yang ,  Tsung-Jen Ho ,  Hua-Tang Yu

IPC分类号： B01D53/24 ,  B01D57/00

CPC分类号： B01D53/24

摘要： A method is used to remove an unreacted alcohol from an ester product mixture by a gas stripping. The method involves the feeding of the ester product mixture into proximity of an axis of a rotating packed bed, so as to enable the ester product mixture to flow radially to come in contact with a gas which is introduced into the rotating packed bed. The unreacted alcohol and any other volatile component of low molecular weight are thus stripped from the ester product mixture by the gas entrainment, thereby resulting in production of a purified ester product which is collected at the bottom of the rotating packed bed. The unreacted alcohol and the volatile component, which are entrained in the gas, are discharged via an exit located at the top of the rotating packed bed.

摘要翻译： 使用一种方法通过气提从酯产物混合物中除去未反应的醇。 该方法包括将酯产物混合物进料到旋转填充床的轴线附近，以使酯产物混合物径向流动以与引入旋转填充床的气体接触。 因此，未反应的醇和任何其它低分子量的挥发性成分被气体夹带从酯产物混合物中汽提，从而产生在旋转填充床的底部收集的纯化的酯产物。 夹在气体中的未反应的醇和挥发性成分经由位于旋转填充床顶部的出口排出。

公开(公告)号：US06884401B2

公开(公告)日：2005-04-26

申请号：US10196245

申请日：2002-07-17

申请人： Sheng Yang ,  Chia-Chang Lin ,  I-Min Tseng ,  Wen-Tzong Liu ,  Hua-Tang Yu

发明人： Sheng Yang ,  Chia-Chang Lin ,  I-Min Tseng ,  Wen-Tzong Liu ,  Hua-Tang Yu

IPC分类号： C01B7/07 ,  C07F9/02 ,  B01D33/06 ,  B01B7/01 ,  C01F9/02

CPC分类号： C07F9/025 ,  C01B7/0706

摘要： A high viscosity liquid is fed into a rotation pack bed at a position with a distance far enough from a rotation axis, creating a centrifugal force exerted on the high viscosity liquid overwhelming a drag thereof, so that it can flow radially through the rotation pack bed. A high pressure gas is introduced into the rotation pack bed peripherally and/or a suction force source is connected to a position near the rotation axis, so that a volatile component contained in the high viscosity fluid is entrained in the gas counter currently flowing through the rotation pack bed and withdrawn from the position near the rotation axis, or the volatile component exits from the position near the rotation axis in gas phase, and thus the volatile component is removed from the high viscosity liquid. A second fluid can also be fed into the rotation pack bed to react with the high viscosity liquid, so that a reaction product is formed, and a volatile side product is removed at the same time.

摘要翻译： 将高粘度液体输送到离旋转轴距离足够远的位置的旋转包装床中，产生施加在高粘度液体上的离心力，压缩其阻力，使得其可以径向流过旋转包装床 。 将高压气体周向引入旋转包床，和/或吸力源连接到靠近旋转轴的位置，使得包含在高粘度流体中的挥发性成分被夹带在目前流经 旋转包装床并从旋转轴附近的位置取出，或者挥发性成分从气相中的旋转轴附近的位置离开，从高粘度液体除去挥发性成分。 第二流体也可以进料到旋转包装床中以与高粘度液体反应，从而形成反应产物，同时除去挥发性副产物。