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公开(公告)号：US4102749A
公开(公告)日：1978-07-25
申请号：US789380
申请日：1977-04-21
Applicant: Howard V. Hess , William F. Franz , Edward L. Cole
Inventor： Howard V. Hess , William F. Franz , Edward L. Cole
CPC classification number: C10B57/00 , C10B53/00 , C10B53/02 , C10G1/006 , C10G1/08 , C10G3/44 , C10G2300/1003 , C10G2300/1014 , C10G2300/1022 , C10G2300/4006 , C10G2300/4012 , Y02E50/14 , Y02P30/20
Abstract: A process for making low sulfur oil by reacting aqueous reactive sludges and slurries with hot, pressurized carbon monoxide and hydrogen (synthesis gas) wherein the wastes are first concentrated by coking in the liquid phase under a pressure of 300 to 3000 psig at a temperature of 400.degree. to 550.degree. F for from 5 minutes to 2 hours.
Abstract translation: 通过使水性反应性污泥和浆料与热的，加压的一氧化碳和氢气（合成气）反应来制备低硫油的方法，其中废物首先通过在300-3000psig的压力下在液相中焦化而在 400°F至550°F，时间为5分钟至2小时。
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公开(公告)号：US4057399A
公开(公告)日：1977-11-08
申请号：US556516
申请日：1975-03-07
Applicant: Edward L. Cole , Howard V. Hess , William F. Franz
Inventor： Edward L. Cole , Howard V. Hess , William F. Franz
Abstract: Water is removed from carbonaceous materials such as coal by treatment with a hydrocarbon at elevated temperatures and a pressure sufficiently high to maintain the system liquid.
Abstract translation: 通过在高温下用烃处理和足够高的压力以保持系统液体，从碳质材料如煤中除去水。
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3.发明授权Isoparaffin-olefin alkylation utilizing a continuous sulfuric acid phase in a tubular reaction zone 失效在管状反应区中使用连续硫酸相的异链烷烃烯烃烷基化
公开(公告)号：US3956417A
公开(公告)日：1976-05-11
申请号：US515943
申请日：1974-10-18
Applicant: William F. Franz , Edward L. Cole
Inventor： William F. Franz , Edward L. Cole
CPC classification number: C07C2/62 , C07C2527/054 , Y10S585/91
Abstract: A process for alkylating isoparaffin hydrocarbons with olefin hydrocarbons for production of high octane gasoline range alkylate wherein the alkylation reaction is performed in the presence of a sulfuric acid alkylation catalyst containing from about 0.0005 to about 0.5 weight percent of a selected micelle forming amphiphilic compound, and wherein the reaction is carried out in a non-backmixed tubular reactor.
Abstract translation: 用于生产高辛烷值汽油范围烷基化物的烯烃烃烷基化异构烷烃的方法，其中烷基化反应在含有约0.0005-约0.5重量％选择的胶束形成两亲化合物的硫酸烷基化催化剂存在下进行，以及 其中反应在非反混合管式反应器中进行。
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公开(公告)号：US4052169A
公开(公告)日：1977-10-04
申请号：US551484
申请日：1975-02-20
Applicant: Edward L. Cole , Howard V. Hess , William F. Franz
Inventor： Edward L. Cole , Howard V. Hess , William F. Franz
CPC classification number: C10L5/00
Abstract: The heating value of solid fuel is increased and the particle size decreased by passing a slurry of the fuel in liquid water at a temperature between 400.degree. F. and the critical temperature of water through a tubular attrition under conditions of turbulent flow. The product slurry is suitable for pipelining.
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公开(公告)号：US4030981A
公开(公告)日：1977-06-21
申请号：US532967
申请日：1974-12-16
Applicant: Howard V. Hess , William F. Franz , Edward L. Cole
Inventor： Howard V. Hess , William F. Franz , Edward L. Cole
CPC classification number: C10B57/00 , C10B53/00 , C10B53/02 , C10G1/006 , C10G1/08 , C10G3/44 , C10G2300/1003 , C10G2300/1014 , C10G2300/1022 , C10G2300/4006 , C10G2300/4012 , Y02E50/14 , Y02P30/20
Abstract: Process for making low sulfur oil by reacting aqueous reactive sludges and slurries with hot, pressurized carbon monoxide and hydrogen (synthesis gas) wherein the wastes are first concentrated by coking in the liquid phase under a pressure of 300 to 3000 psig at a temperature of 400.degree. to 550.degree. F for from 5 minutes to 2 hours.
Abstract translation: 通过使水性反应性污泥和浆料与热的，加压的一氧化碳和氢气（合成气）反应制备低硫油的方法，其中首先通过在300-3000psig的压力下在液相中在400℃的温度下焦化而将废物浓缩 DEG至550°F，时间为5分钟至2小时。
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Patent Agency Ranking
公开(公告)号：US4017263A
公开(公告)日：1977-04-12
申请号：US515942
申请日：1974-10-18
Applicant: Jeffrey W. Holmes , Bruce K. Purcell , William F. Franz , Edward L. Cole
Inventor： Jeffrey W. Holmes , Bruce K. Purcell , William F. Franz , Edward L. Cole
CPC classification number: C07C2/62 , C07C2527/054 , Y10S585/921
Abstract: Improved alkylation reactor and reaction emulsion phase separation apparatus is described. Such apparatus is particularly useful in sulfuric acid catalyzed alkylation of isoparaffin with olefins for production of high octane value alkylate.
Abstract translation: 描述了改进的烷基化反应器和反应乳液相分离装置。 这种装置特别可用于异构烷烃与烯烃的硫酸催化烷基化以生产高辛烷值的烷基化物。
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公开(公告)号：US3962076A
公开(公告)日：1976-06-08
申请号：US505127
申请日：1974-09-11
Applicant: Howard V. Hess , William F. Franz , Edward L. Cole
Inventor： Howard V. Hess , William F. Franz , Edward L. Cole
CPC classification number: B01D11/0426 , B01D11/0488 , C02F1/025 , C02F11/002
Abstract: Disclosed herein is a process for disposing of aqueous sewage and for producing fresh water by coking the sewage in the liquid phase to form gases, coke and an effluent which is extracted with a hot liquid hydrocarbon to form a hydrocarbon-water solution and a hot concentrated brine. The hot brine is injected into the sewage sludge to heat same to coking temperature. Hot water is removed from the hydrocarbon-water solution, used for space heating or the like and thereby cooled. The cool water then is passed through a carbon absorber to remove traces of hydrocarbon dissolved therein, and chlorinated to give potable water.
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公开(公告)号：US3944462A
公开(公告)日：1976-03-16
申请号：US384672
申请日：1973-08-01
Applicant: Howard V. Hess , Edward L. Cole , William F. Franz
Inventor： Howard V. Hess , Edward L. Cole , William F. Franz
CPC classification number: D21C11/04 , Y10S423/03
Abstract: The liquid phase coking of waste kraft pulping liquors can be effected with a shorter residence time in the coking means at lower temperature, and lower pressure by reducing the pH of such liquors by at least one pH unit before coking. Products are lower in malodorous organic sulfur components than those produced at a higher pH.The lowering of the pH is achieved by adding sulfur dioxide to the liquor either as free SO.sub.2 or as an aqueous solution of SO.sub.2.
Abstract translation: 废硫酸盐制浆液的液相焦化可以在较低温度下在焦化装置中具有更短的停留时间，并且可以在焦化之前通过将这些液体的pH降低至少一个pH单位而降低压力。 恶臭有机硫成分的产物比在较高pH下产生的产物要低。
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公开(公告)号：US4014661A
公开(公告)日：1977-03-29
申请号：US558870
申请日：1975-03-17
Applicant: Howard V. Hess , William F. Franz , Edward L. Cole
Inventor： Howard V. Hess , William F. Franz , Edward L. Cole
Abstract: Disclosed is a process for making a hydrocarbon coke slurry fuel by coking carbonaceous materials in the liquid phase under autogenous pressure to form coke which is then extracted with a combustible hydrocarbon at high temperatures and pressures to produce a dense slurry of coke in the hydrocarbon suitable for use as a fuel.
Abstract translation: 公开了一种通过在自生压力下在液相中焦化碳质材料来形成碳氢焦炭浆料燃料的方法，以形成焦炭，然后在高温和高压下用可燃性烃萃取，从而在适于 用作燃料。
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公开(公告)号：US4382895A
公开(公告)日：1983-05-10
申请号：US284710
申请日：1981-07-20
Applicant: Edward L. Cole , Robert M. Suggitt
Inventor： Edward L. Cole , Robert M. Suggitt
IPC: C07C309/62 , C07C143/24
CPC classification number: C07C309/62
Abstract: A process for the production of petroleum sulfonates from lubricating oil extract fractions wherein a primary extract-solvent mixture, preferably substantially free from water, is cooled to a temperature at least 25.degree. C. below the extraction temperature to form two immiscible liquid phases comprising a secondary extract phase which is richer in aromatic hydrocarbons than the primary extract and a secondary raffinate phase which is poorer in aromatics than the primary extract. The secondary raffinate is sulfonated and the unsulfonated fraction returned to the separations process.The process results in improved yields of petroleum sulfonates with lowered SO.sub.3 consumption and less by-product sludge than conventional processes in which the entire extract fraction is sulfonated.
Abstract translation: 从润滑油提取物馏分中生产石油磺酸盐的方法，其中将优选基本上不含水的初级萃取 - 溶剂混合物冷却至低于提取温度至少25℃的温度，以形成两个不混溶的液相，其包含 二级萃取相，其比一级提取物富含芳族烃，二级萃余相比芳族化合物比初级萃取物差。 二次萃余液被磺化，未磺化的馏分返回到分离过程。 与其中整个萃取馏分磺化的常规方法相比，该方法可以提高石油磺酸盐的产率，降低SO 3消耗量和较少的副产物污泥。
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