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19 条记录 (耗时 0.01 秒)

    Process for making a 1,3,5,7-tetraalkanoyl-1,3,5,7-tetraazacyclooctane
    2.
    发明授权
    Process for making a 1,3,5,7-tetraalkanoyl-1,3,5,7-tetraazacyclooctane 失效
    制备1,3,5,7-四烷酰基-1,3,5,7-四氮杂环辛烷的方法

    公开(公告)号：US06201117B1

    公开(公告)日：2001-03-13

    申请号：US09476699

    申请日：2000-01-03

    申请人： William J. Lukasavage

    发明人： William J. Lukasavage

    IPC分类号： C07D25702

    CPC分类号： C06B45/20 ,  C06B21/0066 ,  C06B25/34

    摘要： A process for making a 1,3,5,7-tetraalkanoyl-1,3,5,7-tetraazacyclooctane comprises the steps of: (a) reacting a compound having the formula wherein R is straight chain or branched alkyl having 1-5 carbon atoms, with an alkanoic acid anhydride having the formula (RCO)2O, where R is as defined above, thereby producing a compound having the formula: wherein R is as defined above; and (b) reacting the compound having the formula (II) with the alkanoic acid anhydride in the presence of water and a catalytic amount of at least one transition metal oxide, thereby producing a compound having the formula where R is as defined above.

    摘要翻译： 制备1,3,5,7-四烷酰基-1,3,5,7-四氮杂环辛烷的方法包括以下步骤：（a）使具有糠醛的化合物R是具有1-5个碳原子的直链或支链烷基 原子与具有式（RCO）2 O的链烷酸酐反应，其中R如上定义，由此制备具有下式的化合物：其中R如上定义; 和（b）在水和催化量的至少一种过渡金属氧化物的存在下使具有式（II）的化合物与链烷酸酐反应，由此制备具有式R的化合物如上定义。

    Granulation process
    5.
    发明授权
    Granulation process 失效
    造粒工艺

    公开(公告)号：US06428724B1

    公开(公告)日：2002-08-06

    申请号：US09476894

    申请日：2000-01-03

    申请人： William J. Lukasavage ,  Karri A. Brock ,  Lawrence A. Behrmann ,  Wallace E. Voreck

    发明人： William J. Lukasavage ,  Karri A. Brock ,  Lawrence A. Behrmann ,  Wallace E. Voreck

    IPC分类号： C06B2506

    CPC分类号： C06B25/34 ,  B01J2/10 ,  B01J2/16 ,  C06B21/0066 ,  C06B21/0091 ,  C06B45/20

    摘要： A process for forming granules (e.g., alpha-HMX containing granules) from at least one particulate material comprises the steps of: (a) selecting particulates (e.g., alpha-HMX particulates) having a particle size distribution; and (b) fluidizing the particulates, whereby particulates agglomerate to form granules. Optionally, the particulates can be coated with one or more second materials, such as energetic materials or fuels. If one or more of the second materials comprise polymerizable monomers, the process can optionally further comprise the step of polymerizing those monomers in situ, either before or after the granule is formed.

    摘要翻译： 从至少一种颗粒材料形成颗粒（例如含有α-HMX的颗粒）的方法包括以下步骤：（a）选择具有粒度分布的颗粒（例如，α-HMX颗粒）; 和（b）使颗粒流化，由此颗粒聚集形成颗粒。可选地，颗粒可以涂覆有一种或多种第二材料，例如高能材料或燃料。 如果一种或多种第二种材料包含可聚合单体，则该方法可以任选地进一步包括在颗粒形成之前或之后原位聚合那些单体的步骤。

    HMX compositions and processes for their preparation
    8.
    发明授权
    HMX compositions and processes for their preparation 失效
    HMX组合物及其制备方法

    公开(公告)号：US06194571B1

    公开(公告)日：2001-02-27

    申请号：US09476279

    申请日：2000-01-03

    申请人： William J. Lukasavage

    发明人： William J. Lukasavage

    IPC分类号： C07D25504

    CPC分类号： C06B21/0066 ,  B01J2/10 ,  B01J2/16 ,  C06B21/0091 ,  C06B25/34 ,  C06B45/20

    摘要： A process for making alpha-HMX comprises the steps of: (a) combining phosphorus pentoxide and nitric acid at a temperature of about 0-25° C., forming a reaction mixture; and (b) adding a compound having the formula: wherein R is straight chain or branched alkyl having 1-5 carbon atoms, to the reaction mixture, whereby a product comprising alpha-HMX is produced.

    摘要翻译： 制备α-HMX的方法包括以下步骤：（a）在约0-25℃的温度下混合五氧化二磷和硝酸，形成反应混合物; 和（b）向反应混合物中加入具有下式的化合物：其中R是具有1-5个碳原子的直链或支链烷基，由此产生包含α-HMX的产物。

    Deterrent coating for propellent grains
    9.
    发明授权
    Deterrent coating for propellent grains 失效
    消毒颗粒的防腐涂料

    公开(公告)号：US3636882A

    公开(公告)日：1972-01-25

    申请号：US38327064

    申请日：1964-07-14

    申请人： US ARMY

    发明人： AARONSON HENRY A ,  SCHWARTZ FRANK R ,  SUKORNICK BERNARD

    IPC分类号： C06B45/20

    CPC分类号： C06B45/20

    摘要： 1. A method of preparing progressive-burning, multiple-base propellants comprising tumbling grains of propellant having a perforation through the length of the grain with a powder mixture consisting essentially of about 65 percent copper resinate and about 35 percent lead naphthenate by weight and then applying heat to said grains and powder mixture during tumbling to soften said powder mixture sufficiently to form a continuous, adherent coating on said grains.

    摘要翻译： {PG，11。一种制备逐步燃烧的多基础推进剂的方法，其包括具有通过所述颗粒长度的穿孔的推进剂的滚动颗粒，所述推进剂基本上由约65％的树脂树脂和约35％的环烷酸铅组成的粉末混合物 ，然后在翻滚期间向所述颗粒和粉末混合物施加热量以充分软化所述粉末混合物，以在所述颗粒上形成连续的粘附涂层。