公开(公告)号：US07569106B2

公开(公告)日：2009-08-04

申请号：US11629946

申请日：2005-06-16

申请人： Rainer Heubach ,  Dieter Lieske

发明人： Rainer Heubach ,  Dieter Lieske

IPC分类号： C09B67/04 ,  C09B47/04

CPC分类号： C09B67/0023 ,  C09B67/0021

摘要： The invention relates to a method for producing an aqueous suspension of pure-phase β-copper phtalocyanine blue pigment using an agitator ball mill. According to said method: a) in a preparatory step, a phthalocyanine crude blue is suspended by means of a dissolver in an aqueous medium, said aqueous medium containing in particular lipophilic substances, which are similar to binding agents and are compatible with the final application medium and crystalline-phase controlling and/or pigment-surface conditioning compounds; b) said aqueous suspension of the phthalocyanine crude blue is ground in an agitator ball mill to form a suspension of a β-phtalocyanine blue pigment. The aqueous suspension thus obtained is characterized in that it contains a high-grade β-phtalocyanine blue pigment for producing a conditioned β-phtalocyanine blue pigment. The advantage is that said suspension can also be directly converted into a colour concentrate, in particular by means of a flushing and kneading method.

摘要翻译： 本发明涉及使用搅拌球磨机制备纯相β-铜酞菁蓝颜料的水性悬浮液的方法。 根据所述方法：a）在准备步骤中，通过溶解器在水性介质中悬浮酞菁粗蓝，所述水性介质特别是含有与粘合剂相似并与最终应用相容的亲油性物质 中等和结晶相控制和/或颜料表面调理化合物; b）将所述酞菁粗蓝的所述含水悬浮液在搅拌器球磨机中研磨以形成β-酞菁蓝颜料的悬浮液。 由此获得的水性悬浮液的特征在于其含有用于生产调理的β-酞菁蓝颜料的高级β-酞菁蓝颜料。 优点是所述悬浮液还可以直接转化成浓缩色料，特别是通过冲洗和捏合方法。

公开(公告)号：US07276555B2

公开(公告)日：2007-10-02

申请号：US10441171

申请日：2003-05-19

申请人： Christopher J. Holmes ,  Richard K. Winblad ,  Rudolf Anthonius Maria Venderbosch ,  Richard Hendrikus Gerrit Brinkhuis

发明人： Christopher J. Holmes ,  Richard K. Winblad ,  Rudolf Anthonius Maria Venderbosch ,  Richard Hendrikus Gerrit Brinkhuis

IPC分类号： C08L67/00 ,  C08L33/06 ,  C08L71/00 ,  C08L75/00 ,  C08L77/00

CPC分类号： C09D11/03 ,  B01F17/0042 ,  B01F17/005 ,  C09B67/0021 ,  C09B67/009 ,  C09D7/45 ,  C09D17/00

摘要： A method of dispersing pigment using an amide-modified resin or an amide-modified hydrocarbyl moiety, and the resulting pigment concentrate or coating or ink composition.

摘要翻译： 使用酰胺改性树脂或酰胺改性的烃基部分分散颜料的方法，以及得到的颜料浓缩物或涂料或油墨组合物。

公开(公告)号：US20030188664A1

公开(公告)日：2003-10-09

申请号：US10117469

申请日：2002-04-05

发明人： Kalpathy R. Anantharaman ,  Michael L. Lewis ,  Pat Galioto

IPC分类号： C09B067/00 ,  C09B067/10

CPC分类号： C09B67/0021 ,  C09B67/0003

摘要： Disclosed is a process for the preparation of a pigment dispersion starting with a tank flushed pigment that is continuously fed into a twin screw extruder, washed and dried by vacuum to get a desirable product.

摘要翻译： 公开了一种制备颜料分散体的方法，其开始于槽冲洗颜料，其连续进料到双螺杆挤出机中，通过真空洗涤和干燥以得到所需的产物。

公开(公告)号：US5645636A

公开(公告)日：1997-07-08

申请号：US333886

申请日：1994-11-03

申请人： Manfred Schneider ,  Rainer Schunck ,  Dieter Schnaitmann ,  Udo Brost

发明人： Manfred Schneider ,  Rainer Schunck ,  Dieter Schnaitmann ,  Udo Brost

IPC分类号： C09B67/00 ,  C09B67/20 ,  C09D11/037 ,  C09D17/00 ,  C08K5/16

CPC分类号： C09D11/037 ,  C09B67/0021 ,  C09B67/006

摘要： The deliveries to the printing ink industry of pigment preparations in the form of flushed pastes increasingly take the form of containers. Given the required high pigment content of the pastes and the attendant high viscosity and thixotropy, there are very frequent problems with filling the containers and complaints concerning the emptying of the containers. There is a demand for a homogeneous, pumpable pigment paste having a long shelf life. According to the invention, this demand is met in the case of pigments based on arylpararosanillnesulfonic acids by the use of specific aids of the type of the condensation products of aliphatic amines or ammonium compounds with polyesters of hydroxy fatty acids as part of the flushing process of the pigment using the customary or slightly modified binder systems which for the same pigment contents bring about a distinctly lower viscosity and thixotropy. The printing properties are not adversely affected.

摘要翻译： 以冲洗浆料形式向印刷油墨行业的色素制剂的交付越来越多地以容器的形式出现。 鉴于糊料所需的高颜料含量和伴随的高粘度和触变性，填充容器和关于容器排空的投诉存在非常频繁的问题。 需要具有长的保存期限的均匀的，可泵送的颜料浆料。 根据本发明，在通过使用脂肪族胺或铵化合物与羟基脂肪酸的聚酯的缩合产物类型的特定助剂作为冲洗过程的一部分的情况下，在基于芳基罗拉尼尼亚磺酸的颜料的情况下满足该需求 对于相同的颜料含量，使用常规或稍微改性的粘合剂体系的颜料导致明显较低的粘度和触变性。 印刷性能不会受到不利影响。

公开(公告)号：US20090000512A1

公开(公告)日：2009-01-01

申请号：US11442805

申请日：2006-05-30

申请人： Bjorn Erik Haabegaard Larsen ,  Robert Pedersen ,  Palle Chris Nielsen ,  Steffen Carrock Olsen

发明人： Bjorn Erik Haabegaard Larsen ,  Robert Pedersen ,  Palle Chris Nielsen ,  Steffen Carrock Olsen

IPC分类号： C09D11/02

CPC分类号： C09D11/037 ,  C09B67/0021 ,  C09D11/03

摘要： A printing ink and process for preparing by mixing an aqueous pigment slurry with at least one non-pigment ink component immiscible in water to form a flush cake which is processed to a finished printing ink.

摘要翻译： 一种印刷油墨和通过将水性颜料浆料与不混溶在水中的至少一种非颜料墨水组分混合以形成冲洗饼以制备成印刷油墨的方法，该冲洗饼被加工成成品油墨。

公开(公告)号：US20060037517A1

公开(公告)日：2006-02-23

申请号：US11204083

申请日：2005-08-15

申请人： Christopher Teeley ,  David Kassin ,  Douglas Cochran ,  Christopher Palmer ,  Norman Pratt

发明人： Christopher Teeley ,  David Kassin ,  Douglas Cochran ,  Christopher Palmer ,  Norman Pratt

IPC分类号： C08K5/00

CPC分类号： B01F15/0201 ,  B01F7/082 ,  B01F2015/0221 ,  C09B67/0021

摘要： A method for preparing an organic pigment dispersion, such as a flush pigment or ink product, comprises steps of introducing into a twin screw extruder a stable, water-borne pigment dispersion, an organic medium, and a destabilizing agent; mixing together the stable, water-borne pigment dispersion, the organic medium, and the destabilizing agent to produce a pigment flush phase and a water phase; and removing at least a part of the water phase. A twin-screw extruder for carrying out the flushing method has an addition and flushing zone, a water removal zone, and a zone for rinsing the crude organic pigment dispersion or flush with water and removing the rinse water. Additional materials may be added to form a finished pigmented product such as an ink product, masterbatch, or toner.

摘要翻译： 制备有机颜料分散体如冲洗颜料或油墨产品的方法包括以下步骤：向双螺杆挤出机中引入稳定的水性颜料分散体，有机介质和不稳定剂; 将稳定的水性颜料分散体，有机介质和去稳定剂混合在一起以产生颜料冲洗相和水相; 并除去水相的至少一部分。 用于进行冲洗方法的双螺杆挤出机具有添加和冲洗区域，除水区域和用于漂洗粗有机颜料分散体或与水冲洗并除去冲洗水的区域。 可以添加另外的材料以形成成品着色产品，例如油墨产品，母料或调色剂。

公开(公告)号：US06348091B1

公开(公告)日：2002-02-19

申请号：US09398486

申请日：1999-09-17

申请人： Donald C. Affeldt ,  Mary F. Pardi ,  Christopher M. Teeley

发明人： Donald C. Affeldt ,  Mary F. Pardi ,  Christopher M. Teeley

IPC分类号： C09D1100

CPC分类号： C09B67/0021 ,  B01F7/08 ,  B01F2003/125 ,  B01F2215/0059 ,  B29C47/766

摘要： The present invention provides a process for continuous production of pigment flushes and an apparatus for carrying out the process. In the process of the invention, the pigment press cake is first fluidized. The fluidized press cake and a hydrophobic liquid organic medium are fed into a twin screw extruder. The kneading of the organic medium and press cake between the twin screws flushes the pigment into the organic medium. The water phase and flushed pigment phase are separated by removing at least part of the water phase through a vent in the extruder. An impediment to the flow of material downstream of the water vent causes the flush to accumulate in the vented section for a period of time sufficient to remove the desired amount of the water phase. The flush works over the impediment and passes downstream to where vacuum is applied to remove residual water from the flush. The flush may be further combined with other ink ingredients to form an ink product. The extruder includes at least one monitoring apparatus that continually monitors a property of the material being processed in the extruder and adjusts a process parameter in response to a deviation of the value obtained for the property from a predetermined desired value for the property.

摘要翻译： 本发明提供连续生产颜料冲洗的方法和用于进行该方法的装置。 在本发明的方法中，颜料压饼首先被流化。 将流化的压饼和疏水液体有机介质进料到双螺杆挤出机中。 在双螺杆之间的有机介质和压饼的捏合将颜料冲洗成有机介质。 通过挤出机中的排气口去除至少部分水相，分离水相和冲洗的颜料相。 在水通道下游的材料流动的障碍导致冲洗在通气部分中积聚足够的时间以消除所需量的水相。 冲洗工作在障碍物上，并通过下游进入真空的地方，以从冲洗中除去残留的水。 冲洗可以进一步与其他油墨成分组合以形成油墨产品。 挤出机包括至少一个监测装置，其连续地监测在挤出机中正在处理的材料的性质，并响应于从该特性获得的值与该特性的预定期望值的偏差来调整工艺参数。

公开(公告)号：US5648418A

公开(公告)日：1997-07-15

申请号：US651451

申请日：1996-05-22

申请人： Charles Francis Lences

发明人： Charles Francis Lences

IPC分类号： C08F8/32 ,  C08F8/30 ,  C08G69/00 ,  C08G81/02 ,  C09B67/00 ,  C09B67/46 ,  C09C3/10 ,  C09D17/00 ,  D06P1/52 ,  D06P1/653 ,  C08F20/06 ,  C08K9/04 ,  C08L23/36

CPC分类号： C09B67/0021 ,  C08F8/44 ,  C08G69/00 ,  C08F2800/20

摘要： A low molecular weight copolymer reaction product of a copolymer acid of an .alpha.-olefin and an unsaturated carboxylic acid, preferably an .alpha.,.beta.-ethylenically unsaturated carboxylic acid, and at least one amino acid compound. The present invention includes a method of preparing the copolymer reaction product. The reaction product has excellent compatibility with other polymers, particularly polyamides. The copolymer reaction product is useful in a method to flush water from pigments.

摘要翻译： α-烯烃和不饱和羧酸的共聚酸，优选α，β-烯属不饱和羧酸和至少一种氨基酸化合物的低分子量共聚物反应产物。 本发明包括制备共聚物反应产物的方法。 反应产物与其它聚合物，特别是聚酰胺具有优异的相容性。 共聚物反应产物可用于从颜料中冲洗水的方法。

公开(公告)号：US4990187A

公开(公告)日：1991-02-05

申请号：US419294

申请日：1989-10-10

申请人： Chi K. Dien ,  Daniel J. Carlick

发明人： Chi K. Dien ,  Daniel J. Carlick

IPC分类号： C09B67/00 ,  C09D11/08

CPC分类号： C09B67/0021 ,  C09D11/08

摘要： Gravure base inks are prepared by flushing an aqueous pigment with a hydrocarbon solvent solution of a major amount of calcium resinate or magnesium resinate and a minor amount of zinc resinate in the presence of a C.sub.8 -C.sub.24 fatty acid amine or C.sub.8 -C.sub.24 fatty acid quaternary ammonium salt. The solvent to metal ratio is at least 40:60 and the pH is in the range of 4 to 10.

摘要翻译： 通过在C8-C24脂肪酸胺或C8-C24脂肪酸四季醇的存在下，用大量的树脂酸钙或树脂酸镁和少量的树脂树脂酸盐的烃溶剂溶液冲洗含水颜料来制备凹版油墨 铵盐。 溶剂与金属之比至少为40:60，pH值在4至10的范围内。

公开(公告)号：US4729796A

公开(公告)日：1988-03-08

申请号：US311253

申请日：1981-10-14

申请人： Reinhold Deubel ,  Christa Uhde nee Schilling ,  Werner Marx

发明人： Reinhold Deubel ,  Christa Uhde nee Schilling ,  Werner Marx

IPC分类号： C09C3/00 ,  C09B67/00 ,  C09B67/02 ,  C09B67/08 ,  C09B67/20 ,  C09C3/10 ,  C09D11/10 ,  C09B67/22 ,  C09B67/54

CPC分类号： C09B67/0021 ,  C09B67/001 ,  C09B67/0095

摘要： Easily dispersible dust-free pigment granules of high tinctorial strength are obtained by adding to the aqueous suspension of a finely divided pigment, an alkaline solution of from 25 to 90 weight percent based on the weight of the granules obtained, of colophony or a colophony derivative, acidifying the mixture, subjecting it to a flush process while stirring and heating to a temperature, above the softening point of the resin, up to 100.degree. C. and isolatng the granules obtained. The granules are particularly suitable for preparing printing inks which are distinguished by a very high tinctorial strength, a good transparency and a low viscosity.

摘要翻译： 通过向精细分散的颜料的水性悬浮液中加入基于获得的颗粒的重量，松香或松香衍生物的25至90重量％的碱性溶液，获得高着色强度的易分散无尘颜料颗粒 ，将混合物酸化，同时搅拌并加热到高于树脂软化点的温度至100℃，并分离得到的颗粒。 颗粒特别适用于制备印刷油墨，其特征在于极高的着色强度，良好的透明度和低粘度。