Apparatus and method for calibration of spectrophotometers
    1.
    发明授权
    Apparatus and method for calibration of spectrophotometers 有权
    用于校准分光光度计的装置和方法

    公开(公告)号:US07061608B2

    公开(公告)日:2006-06-13

    申请号:US10768644

    申请日:2004-01-30

    Abstract: An apparatus and related method for optical calibration of spectrophotometers is described. The apparatus is a calibration plate including one or more cuvettes filled with solutions of interest. The cuvettes are sealed to prevent evaporation. The cuvettes also possess a compressible component to allow for expansion of the solution and a bubble control apparatus to ensure that the compressible component does not intersect the beam path. A piece of neutral density glass is optionally included in the apparatus to track optical changes of the solutions over time.

    Abstract translation: 描述了用于分光光度计的光学校准的装置和相关方法。 该装置是包括一个或多个充满感兴趣的溶液的比色杯的校准板。 试管被密封以防止蒸发。 试管还具有允许溶液膨胀的可压缩部件和气泡控制装置,以确保可压缩部件不与光束路径相交。 装置中可选地包括一片中性密度玻璃,以跟踪溶液随时间的光学变化。

    METHOD FOR DETERMINING THE PATH LENGTH OF A SAMPLE AND VALIDATING THE MEASUREMENT OBTAINED
    2.
    发明申请
    METHOD FOR DETERMINING THE PATH LENGTH OF A SAMPLE AND VALIDATING THE MEASUREMENT OBTAINED 有权
    确定样品路径长度并确定获得的测量值的方法

    公开(公告)号:US20130070236A1

    公开(公告)日:2013-03-21

    申请号:US13617478

    申请日:2012-09-14

    Abstract: A for traceably determining an unknown optical path length of a sample in an optical measuring device comprises the steps of: providing a drop analyser connected to a standard spectrophotometer; providing a certified reference material contained in first and second closed high accuracy cuvettes; measuring absorbance of the certified reference material to obtain a first absorbance measurement for the first specified path length; measuring absorbance of the certified reference material for a second path length to obtain a second absorbance measurement; using a dropping device to drop a specified volume of the solvent on an optical surface so that the path length of the specified volume can be determined by reference to the first and second absorbance measurement; and using the dropping device to drop the same volume of sample as the specified volume of solvent on the optical measuring device.

    Abstract translation: A,用于在光学测量装置中用于可追溯性地确定样品的未知光程长度包括以下步骤:提供连接到标准分光光度计的液滴分析仪; 提供包含在第一和第二封闭高精度比色杯中的认证参考材料; 测量认证参考材料的吸光度,以获得第一指定路径长度的第一吸光度测量; 测量第二路径长度的认证参考材料的吸光度以获得第二吸光度测量; 使用滴下装置将特定体积的溶剂落在光学表面上,使得可以参照第一和第二吸光度测量来确定指定体积的路径长度; 并且使用滴液装置将相同体积的样品与特定体积的溶剂一起放在光学测量装置上。

    Gas Analyzer for Measuring the Mercury Content of a Gas
    3.
    发明申请
    Gas Analyzer for Measuring the Mercury Content of a Gas 审中-公开
    用于测量气体汞含量的气体分析仪

    公开(公告)号:US20120194818A1

    公开(公告)日:2012-08-02

    申请号:US13356151

    申请日:2012-01-23

    Applicant: Rolf DISCH

    Inventor: Rolf DISCH

    Abstract: The invention relates to a gas analyzer for measuring the mercury content of a gas having an Hg light source which transmits transmitted light having wavelengths of at least one spectral line of the mercury, a measuring cell in which the gas to be measured is present, a light receiver, an evaluation unit and a test cuvette which can be introduced into the beam path for checking the operability. To provide an improved gas analyzer which can be calibrated in a simple manner as well as a corresponding improved calibration method, provision is made that the test cuvette contains benzol as a test gas.

    Abstract translation: 本发明涉及一种气体分析仪,用于测量具有Hg光源的气体的汞含量,该Hg光源透射具有至少一条汞谱的波长的透射光,其中存在待测气体的测量池, 光接收器,评估单元和可以被引入光束路径中以检查可操作性的测试比色皿。 为了提供可以以简单的方式校准的改进的气体分析仪以及相应的改进的校准方法,提供了测试试管含有作为测试气体的苯酚。

    Pollution monitor with self-contained calibration and cell-block therefor
    4.
    发明授权
    Pollution monitor with self-contained calibration and cell-block therefor 失效
    污染监测器,具有独立校准和电池阻挡

    公开(公告)号:US3944834A

    公开(公告)日:1976-03-16

    申请号:US512338

    申请日:1974-10-04

    Abstract: The embodiment of the pollution monitor described in the specification uses the principle of ultraviolet-induced fluorescence to detect and measure gaseous pollution in air, smokestack exhaust and other fluids. Improved calibration or standardization is effected by the use of one or more calibration cells in which a non-gaseous material simulates the fluorescence of the gaseous species under investigation, by scattering the incident ultraviolet light into a spectral region similar to that of the fluorescence of the gaseous species. Examples of suitable materials have been found to be aluminum, gold, platinum and molybdenum, all of which scatter light in the appropriate spectral region at a level which stays substantially constant with time.In the preferred embodiment, the sample cell and the calibration cells are all formed in a single cell block by drilling holes into solid bar material which holes function as the individual cell cavities. The sample cell has ports for the flow of sample gas therethrough, while in each of the calibration cells, the metallic material is mounted to intercept and scatter the incident ultraviolet light energy. The cell block is constructed to rotate so that the several cells can be individually aligned in the light path between the ultraviolet source and fluorescence detector.

    Abstract translation: 本说明书中描述的污染监测器的实施例使用紫外线诱发荧光的原理来检测和测量空气,烟囱排气和其它流体中的气体污染。 通过使用一种或多种校准单元来实现改进的校准或标准化,其中非气态材料通过将入射的紫外光散射到类似于荧光的光谱区域中来模拟所研究的气态物质的荧光, 气态物种。 已经发现合适的材料的实例是铝,金,铂和钼,所有这些材料都以适当的光谱区域中的光散射在与时间基本恒定的水平上。

    Method for determining the path length of a sample and validating the measurement obtained
    5.
    发明授权
    Method for determining the path length of a sample and validating the measurement obtained 有权
    用于确定样品的路径长度并验证获得的测量的方法

    公开(公告)号:US08947668B2

    公开(公告)日:2015-02-03

    申请号:US13617478

    申请日:2012-09-14

    Abstract: A for traceably determining an unknown optical path length of a sample in an optical measuring device comprises the steps of: providing a drop analyzer connected to a standard spectrophotometer; providing a certified reference material contained in first and second closed high accuracy cuvettes; measuring absorbance of the certified reference material to obtain a first absorbance measurement for the first specified path length; measuring absorbance of the certified reference material for a second path length to obtain a second absorbance measurement; using a dropping device to drop a specified volume of the solvent on an optical surface so that the path length of the specified volume can be determined by reference to the first and second absorbance measurement; and using the dropping device to drop the same volume of sample as the specified volume of solvent on the optical measuring device.

    Abstract translation: A,用于在光学测量装置中用于可追溯性地确定样品的未知光程长度包括以下步骤:提供连接到标准分光光度计的液滴分析仪; 提供包含在第一和第二封闭高精度比色杯中的认证参考材料; 测量认证参考材料的吸光度,以获得第一指定路径长度的第一吸光度测量; 测量第二路径长度的认证参考材料的吸光度以获得第二吸光度测量; 使用滴下装置将特定体积的溶剂落在光学表面上,使得可以参照第一和第二吸光度测量来确定指定体积的路径长度; 并使用滴液装置将相同体积的样品与特定体积的溶剂一起放在光学测量装置上。

    Apparatus and method for calibration of spectrophotometers
    6.
    发明申请
    Apparatus and method for calibration of spectrophotometers 有权
    用于校准分光光度计的装置和方法

    公开(公告)号:US20050168737A1

    公开(公告)日:2005-08-04

    申请号:US10768644

    申请日:2004-01-30

    Abstract: An apparatus and related method for optical calibration of spectrophotometers is described. The apparatus is a calibration plate including one or more cuvettes filled with solutions of interest. The cuvettes are sealed to prevent evaporation. The cuvettes also possess a compressible component to allow for expansion of the solution and a bubble control apparatus to ensure that the compressible component does not intersect the beam path. A piece of neutral density glass is optionally included in the apparatus to track optical changes of the solutions over time.

    Abstract translation: 描述了用于分光光度计的光学校准的装置和相关方法。 该装置是包括一个或多个充满感兴趣的溶液的比色杯的校准板。 试管被密封以防止蒸发。 试管还具有允许溶液膨胀的可压缩部件和气泡控制装置,以确保可压缩部件不与光束路径相交。 装置中可选地包括一片中性密度玻璃,以跟踪溶液随时间的光学变化。

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