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公开(公告)号：US20060144715A1
公开(公告)日：2006-07-06
申请号：US11367193
申请日：2006-03-03
申请人： Lawrence Becnel
发明人： Lawrence Becnel
摘要： This invention relates to the methods and installations for producing ultra pure sodium chloride salt crystals primarily for use in saturating depleted brine resulting from the electrolytic decomposition of saturated brine in chlor alkali membrane cells for the production of chlorine, caustic soda and hydrogen. More particularly, this invention related to the production of ultra pure sodium chloride salt crystals by processing primary treated brine by first acidifying the primary treated brine, then stripping the carbonic acid produced by acidification as carbon dioxide, and then returning the brine to a pH of about 6 or higher which is sufficient for processing it in evaporation equipment where the ultra pure salt crystals are produced.
摘要翻译： 本发明涉及用于生产超纯氯化钠盐晶体的方法和装置，其主要用于饱和由氯碱膜细胞中的饱和盐水电解分解产生氯，苛性钠和氢气的贫化盐水。 更具体地，本发明涉及通过首先酸化初级处理的盐水，然后将由酸化产生的碳酸作为二氧化碳，然后将盐水返回至pH为 约6或更高，这足以在制造超纯盐晶体的蒸发设备中进行处理。
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公开(公告)号：US4243503A
公开(公告)日：1981-01-06
申请号：US937724
申请日：1978-08-29
申请人： Donald F. Lieb , Mary R. Suchanski
发明人： Donald F. Lieb , Mary R. Suchanski
CPC分类号： C25C7/02 , C25B11/0478
摘要： Disclosed is an electrode for use in electrochemical processes wherein a metal substrate made of a valve metal such as titanium carries an electrocatalytically active coating such as an oxide selected from the group consisting of manganese, iron, cobalt, or nickel applied in a series of layers wherein particles of fibers of various filler materials such as titanium, other valve metals, tin oxide, titanium oxides, manganese oxide, quartz, silica, and alumina were admixed with the top coating material.
摘要翻译： 公开了一种用于电化学过程的电极，其中由诸如钛的阀金属制成的金属基底载有电催化活性涂层，其选自由一系列层中施加的锰，铁，钴或镍组成的组中的氧化物 其中各种填料材料如钛，其它阀金属，氧化锡，氧化钛，氧化锰，石英，二氧化硅和氧化铝的纤维颗粒与顶部涂层材料混合。
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公开(公告)号：US4209370A
公开(公告)日：1980-06-24
申请号：US840224
申请日：1977-10-07
CPC分类号： C25B1/36
摘要： The present invention refers to a process for electrolysis of brine by mercury cathodes, being the latter cathode separated from the anode by a porous diaphragm or membrane with diameter of pore such that mercury cannot pass through it.
摘要翻译： 本发明涉及一种通过汞阴极电解盐水的方法，后一种阴极通过多孔隔膜或孔直径从阳极分离，孔直径使得汞不能通过。
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公开(公告)号：US4199418A
公开(公告)日：1980-04-22
申请号：US37327
申请日：1979-05-08
申请人： Frank Boggs, Jr.
发明人： Frank Boggs, Jr.
CPC分类号： C25B1/36 , C25B9/142 , Y02P20/132
摘要： A process for making alkali hydroxide and chlorine in a plurality of electrolytic cells of the amalgam type, wherein a decomposer is provided for each cell and wherein alkali metal amalgam formed in the cell is reacted with water in a companion decomposer to form alkali hydroxide, the improvement comprising utilizing for each cell and corresponding decomposer a condenser and a separator component between the condenser and decomposer in the hydrogen outlet line of the decomposer to separate mercury vapor and water vapor initially liquefied in the condenser and divert the condensed mercury back into the decomposer.
摘要翻译： 一种在汞齐型多个电解槽中制造碱金属氢氧化物和氯的方法，其中为每个电池提供分解器，并且其中在电池中形成的碱金属汞齐与伴侣分解器中的水反应形成碱金属氢氧化物， 改进包括在分解器的氢出口管线中的每个电池和相应的分解器之间在冷凝器和分解器之间使用冷凝器和分离器部件，以分离最初在冷凝器中液化的汞蒸气和水蒸汽，并将冷凝的汞转移回分解器。
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公开(公告)号：US4166780A
公开(公告)日：1979-09-04
申请号：US906656
申请日：1978-05-16
摘要： An improved process for the production of halogens and alkali metal hydroxide by electrolysis of aqueous solution of alkali metal halides in a flowing mercury electrolysis cell wherein the salt solutions do not have to purified and to novel amalgam denuders and a mercury electrolytic cell plant without a salt purification step.
摘要翻译： 通过在流动的水银电解池中电解碱金属卤化物的水溶液来生产卤素和碱金属氢氧化物的改进方法，其中盐溶液不需要纯化和新的汞齐溶解剂和没有盐的汞电解池设备 净化步骤。
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公开(公告)号：US4115219A
公开(公告)日：1978-09-19
申请号：US822016
申请日：1977-08-05
申请人： Alan B. Gancy , Chester J. Kaminski
发明人： Alan B. Gancy , Chester J. Kaminski
CPC分类号： C01F11/18 , C01D3/16 , C01F11/181 , C01F11/187 , C01F11/188 , C01F5/14
摘要： In a process for purifying raw brine containing dissolved strontium, calcium and magnesium impurities wherein the raw brine is treated by contacting the brine with sodium carbonate for precipitation of strontium and calcium carbonate, contacting the brine containing the strontium and calcium carbonate solids with sodium hydroxide for precipitation of magnesium hydroxide, and removing strontium carbonate, calcium carbonate and magnesium hydroxide solids from the sodium chloride brine, the improvement which comprises passing at least a portion of said removed solids to the zone wherein the raw brine is contacted with sodium carbonate.
摘要翻译： 在用于净化含有溶解锶，钙和镁杂质的原盐水的方法中，其中通过使盐水与碳酸钠接触以将沉淀的锶和碳酸钙接触来处理生盐水，使含有锶和碳酸钙固体的盐水与氢氧化钠接触 沉淀氢氧化镁，以及从氯化钠盐水中除去碳酸锶，碳酸钙和氢氧化镁固体，其改进之处在于将至少一部分所述去除的固体送至其中生盐水与碳酸钠接触的区域。
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7.发明授权
公开(公告)号：US4003808A
公开(公告)日：1977-01-18
申请号：US573367
申请日：1975-04-30
申请人： Karl-Heinz Sieberer
发明人： Karl-Heinz Sieberer
CPC分类号： C25B15/06
摘要： A method for regulating and controlling the anode current and for avoiding short-circuits between the adjustable anodes and the cathode of an electrolysis cell, wherein by means of an apparatus controlled by a field plate (magnetically controllable resistance), a magnetic diode or a magnetic transistor as sensor, the electrical resistance of which constitutes a measure for the current flowing to an anode or an anode group and, thus, having a nominal value of the resistance for a nominal value of the current, in case there is a deviation of the current from the nominal value the deviation of the electrical resistance of the sensor from the nominal value serves to reset the electrical resistance of the sensor and, thus, also the current of the anode or anode group to the nominal value by adjusting the anode or anode group.
摘要翻译： 一种用于调节和控制阳极电流并避免可调节阳极与电解槽的阴极之间的短路的方法，其中通过由场板（可磁阻的电阻）控制的装置，磁二极管或磁 晶体管作为传感器，其电阻构成流过阳极或阳极组的电流的量度，因此具有电流额定值的电阻的标称值，如果存在偏差 从标称值的电流，传感器的电阻与标称值的偏差用于通过调节阳极或阳极来重置传感器的电阻，从而将阳极或阳极组的电流调整到标称值 组。
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公开(公告)号：US3905880A
公开(公告)日：1975-09-16
申请号：US46541674
申请日：1974-04-29
申请人： ICI LTD
发明人： LEE DENIS , NORBURN LESLIE
摘要： A process for the reduction of thick mercury on the baseplate of a mercury cell which comprises dispersing water or an aqueous medium (preferably brine) continuously or intermittently at one or more stations along the line of amalgam flow without interruption of the electrolysis. It is preferred to inject water or brine in part or whole of the stream of amalgam returning from the denuder to the cell, for example by means of an emulsifier located between the denuder and the cell or by injecting water into the amalgam pump.
摘要翻译： 一种用于减少汞电池底板上的厚汞的方法，该方法包括沿着汞齐流动线连续地或间歇地分散水或水介质（优选盐水）而不中断电解。
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公开(公告)号：US3895938A
公开(公告)日：1975-07-22
申请号：US43332474
申请日：1974-01-14
申请人： BAYER AG
发明人： KLOTZ HELMUT
CPC分类号： C25B1/36 , C22B43/00 , Y02P10/234
摘要： In the electrolysis of an alkali metal chloride in a cell containing mercury there is produced an alkali metal amalgam which is withdrawn and decomposed to regenerate mercury containing impurities introduced from the alkali metal chloride. The impure mercury is mixed turbulently with an aqueous solution of sulfuric acid having mercury (I) sulfate dissolved or suspended therein whereupon the impurities are extracted into the solution and the purified mercury is recycled.
摘要翻译： 在含有汞的电池中的碱金属氯化物的电解中，产生碱金属汞齐，其被排出并分解以再生含有从碱金属氯化物引入的杂质的汞。 将不纯的汞与溶解或悬浮在其中的硫酸汞（I）硫酸的硫酸水溶液混合混合，随后将杂质萃取到溶液中，纯化的汞被再循环。
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公开(公告)号：US3849267A
公开(公告)日：1974-11-19
申请号：US33819373
申请日：1973-03-05
申请人： AKZO NV
CPC分类号： C01G13/04
摘要： A process for recovering mercury from a mercury-containing gas which includes mixing chlorine with the gas, then passing the mixture through a gas-permeable bed of a non-porous solid material which has a large surface area in relation to the bed volume to collect necessary chloride thereon and thereafter recovering the mercury by either washing the bed with chlorine containing brine and passing the resulting mercury-containing brine to an electrolysis cell with a mercury cathode or dissolving the bed material in an aqueous process stream and passing the stream to an electrolysis cell with a mercury cathode.
摘要翻译： 一种从含汞气体中回收汞的方法，包括将氯与气体混合，然后将混合物通过相对于床体积具有大表面积的无孔固体材料的透气床，以收集 其后必要的氯化物，然后通过用含氯盐水洗涤床层并将所得含汞盐水转移到具有汞阴极的电解池或溶解t
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