公开(公告)号：WO2004034047A1

公开(公告)日：2004-04-22

申请号：PCT/EP2003/011044

申请日：2003-10-07

Applicant: UNIVERSITE CATHOLIQUE DE LOUVAIN ,  BOBORODEA, Adrian-Gelu ,  BAILLY, Christian ,  DAOUST, Daniel ,  JONAS, Alain ,  NYSTEN, Bernard

Inventor： BOBORODEA, Adrian-Gelu ,  BAILLY, Christian ,  DAOUST, Daniel ,  JONAS, Alain ,  NYSTEN, Bernard

IPC: G01N30/00

CPC classification number: G01N33/442 ,  G01N25/147 ,  G01N30/52 ,  G01N2030/008 ,  G01N2030/3007 ,  G01N2030/521 ,  G01N33/44

Abstract: The present invention relates to a column for performing analytical temperature rising elution fractionation (ATREF) characterized in that the packing of said column comprises elastic wires having a good elasticity and a good thermal conductivity. The present invention also relates to a device comprising the column according to the invention, a temperature controlling system for controlling the temperature of said column, a sample injector for injecting a polymer sample solution into said column, a pump for eluting the polymer fractions from said column and a detector for detecting eluting fractions of said sample solution. The present invention further relates to a method for performing ATREF analyses using the column according to the invention.

Abstract translation: 本发明涉及一种用于进行分析升温洗脱分馏（ATREF）的色谱柱，其特征在于，所述色谱柱的填料包括具有良好弹性和良好导热性的弹性丝。 本发明还涉及包括根据本发明的塔的装置，用于控制所述塔的温度的温度控制系统，用于将聚合物样品溶液注入所述塔中的样品注射器，用于从所述柱中洗脱聚合物部分的泵 柱和用于检测所述样品溶液的洗脱级分的检测器。 本发明还涉及使用本发明的色谱柱进行ATREF分析的方法。