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    THERMAL EXTRACTION GEOCHEMICAL METHOD FOR MEASUREMENT OF OIL IN PLACE AND MOVABLE OIL
    4.
    发明申请
    THERMAL EXTRACTION GEOCHEMICAL METHOD FOR MEASUREMENT OF OIL IN PLACE AND MOVABLE OIL 审中-公开
    用于测量地表和可移动油中的油的热提取地球化学方法

    公开(公告)号：WO2015153465A3

    公开(公告)日：2015-11-26

    申请号：PCT/US2015023355

    申请日：2015-03-30

    Applicant: APACHE CORP

    Inventor： ABRAMS MICHAEL A

    IPC: E21B49/08 ,  G01K17/00 ,  G01N30/68

    CPC classification number: E21B49/08 ,  G01K17/00 ,  G01N30/00 ,  G01N30/68 ,  G01N33/241 ,  G01N2030/008 ,  G01N2030/8854

    Abstract: A method for analyzing total oil in place and fraction that is movable oil in a fine grain rock formation includes monitoring thermal extraction of hydrocarbon and non- hydrocarbon compounds from a sample of a subsurface formation by heating the sample. The heating has a selected initial temperature, and a temperature increase at a selected rate to a final temperature. The extracted hydrocarbon and non-hydrocarbon compounds are passed through a capillary column to a flame ionization detector. Types of hydrocarbon and non-hydrocarbon compounds and relative fractional amounts of each type thereof are determined from the sample by analyzing a chemical thermogram generated by the flame ionization detector.

    Abstract translation: 在细粒岩层中可动油分析总油的分析方法，是通过加热样品来监测来自地下地层样品的烃类和非碳氢化合物的热萃取。 加热具有选择的初始温度，并且以选定的速率升温至最终温度。 提取的烃和非烃化合物通过毛细管柱进入火焰离子化检测器。 通过分析由火焰离子化检测器产生的化学热分析图，从样品中确定烃类和非烃类化合物的类型及其各自类型的相对分数。

    COLUMN FOR ANALYTICAL TEMPERATURE RISING ELUTION FRACTIONATION (ATREF)
    5.
    发明申请
    COLUMN FOR ANALYTICAL TEMPERATURE RISING ELUTION FRACTIONATION (ATREF) 审中-公开
    分析温度升高分辨率（ATREF）

    公开(公告)号：WO2004034047A1

    公开(公告)日：2004-04-22

    申请号：PCT/EP2003/011044

    申请日：2003-10-07

    Applicant: UNIVERSITE CATHOLIQUE DE LOUVAIN ,  BOBORODEA, Adrian-Gelu ,  BAILLY, Christian ,  DAOUST, Daniel ,  JONAS, Alain ,  NYSTEN, Bernard

    Inventor： BOBORODEA, Adrian-Gelu ,  BAILLY, Christian ,  DAOUST, Daniel ,  JONAS, Alain ,  NYSTEN, Bernard

    IPC: G01N30/00

    CPC classification number: G01N33/442 ,  G01N25/147 ,  G01N30/52 ,  G01N2030/008 ,  G01N2030/3007 ,  G01N2030/521 ,  G01N33/44

    Abstract: The present invention relates to a column for performing analytical temperature rising elution fractionation (ATREF) characterized in that the packing of said column comprises elastic wires having a good elasticity and a good thermal conductivity. The present invention also relates to a device comprising the column according to the invention, a temperature controlling system for controlling the temperature of said column, a sample injector for injecting a polymer sample solution into said column, a pump for eluting the polymer fractions from said column and a detector for detecting eluting fractions of said sample solution. The present invention further relates to a method for performing ATREF analyses using the column according to the invention.

    Abstract translation: 本发明涉及一种用于进行分析升温洗脱分馏（ATREF）的色谱柱，其特征在于，所述色谱柱的填料包括具有良好弹性和良好导热性的弹性丝。 本发明还涉及包括根据本发明的塔的装置，用于控制所述塔的温度的温度控制系统，用于将聚合物样品溶液注入所述塔中的样品注射器，用于从所述柱中洗脱聚合物部分的泵 柱和用于检测所述样品溶液的洗脱级分的检测器。 本发明还涉及使用本发明的色谱柱进行ATREF分析的方法。

    THERMAL EXTRACTION GEOCHEMICAL METHOD FOR MEASUREMENT OF OIL IN PLACE AND MOVABLE OIL IN LIQUID RICH FINE GRAIN ROCKS
    7.
    发明申请
    THERMAL EXTRACTION GEOCHEMICAL METHOD FOR MEASUREMENT OF OIL IN PLACE AND MOVABLE OIL IN LIQUID RICH FINE GRAIN ROCKS 审中-公开
    用于测量液体油中的油的热提取地球化学方法

    公开(公告)号：WO2015153465A2

    公开(公告)日：2015-10-08

    申请号：PCT/US2015/023355

    申请日：2015-03-30

    Applicant: APACHE CORPORATION

    Inventor： ABRAMS, Michael, A.

    IPC: G01N30/68

    CPC classification number: E21B49/08 ,  G01K17/00 ,  G01N30/00 ,  G01N30/68 ,  G01N33/241 ,  G01N2030/008 ,  G01N2030/8854

    Abstract: A method for analyzing total oil in place and fraction that is movable oil in a fine grain rock formation includes monitoring thermal extraction of hydrocarbon and non- hydrocarbon compounds from a sample of a subsurface formation by heating the sample. The heating has a selected initial temperature, and a temperature increase at a selected rate to a final temperature. The extracted hydrocarbon and non-hydrocarbon compounds are passed through a capillary column to a flame ionization detector. Types of hydrocarbon and non-hydrocarbon compounds and relative fractional amounts of each type thereof are determined from the sample by analyzing a chemical thermogram generated by the flame ionization detector.

    Abstract translation: 在细粒岩层中可动油分析总油的分析方法，是通过加热样品来监测来自地下地层样品的烃类和非碳氢化合物的热萃取。 加热具有选择的初始温度，并且以选定的速率升温至最终温度。 提取的烃和非烃化合物通过毛细管柱进入火焰离子化检测器。 通过分析由火焰离子化检测器产生的化学热分析图，从样品中确定烃类和非烃类化合物的类型及其各自类型的相对分数。

    "> PROCEDIMIENTO PARA EL MUESTREO PASIVO DE CONTAMINANTES ATMOSFÉRICOS MEDIANTE EL DISPOSITIVO
    8.
    发明申请
    PROCEDIMIENTO PARA EL MUESTREO PASIVO DE CONTAMINANTES ATMOSFÉRICOS MEDIANTE EL DISPOSITIVO "VERAM" 审中-公开
    “VERAM”设备无害抽取大气污染物的程序

    公开(公告)号：WO2010109049A1

    公开(公告)日：2010-09-30

    申请号：PCT/ES2010/070169

    申请日：2010-03-24

    Applicant: UNIVERSITAT DE VALENCIA ,  PASTOR GARCÍA, Agustín ,  DE LA GUARDIA CIRUGEDA, Miguel ,  ESTEVE TURRILLAS, Francesc

    Inventor： PASTOR GARCÍA, Agustín ,  DE LA GUARDIA CIRUGEDA, Miguel ,  ESTEVE TURRILLAS, Francesc

    IPC: G01N1/22 ,  B01D53/04

    CPC classification number: G01N1/2202 ,  B01D53/04 ,  G01N1/4005 ,  G01N30/7206 ,  G01N2030/008 ,  G01N2030/009

    Abstract: Procedimiento para el muestreo pasivo de contaminantes atmosféricos mediante el dispositivo VERAM. En la presente invención se describe un procedimiento versátil, fácil y de manejo rápido para la determinación de contaminantes orgánicos en aire mediante un dispositivo de muestreo pasivo formado por una membrana semipermeable plana de tipo tubo polimérico de tamaño variable rellena de una fase sólida o mezcla de fases sólidas (VERAM). La utilización de este dispositivo garantiza una determinación directa de los contaminantes adsorbidos mediante la aplicación de la técnica de desorción térmica seguida de la técnica de inyección de espacio de cabeza con cromatografía de gases y espectrometría de masas. (HS-GC- MS). Además, la presente invención describe el desarrollo de modelos matemáticos que correlacionen la cantidad absorbida por el muestreador con la concentración promedio del contaminante en el aire durante el periodo de muestreo.

    Abstract translation: 通过“VERAM”装置对大气污染物进行被动采样的程序。 本发明描述了一种用于通过无源采样装置测定空气中的有机污染物的通用，容易和快速的方法，该无源采样装置包括填充有固相或固相混合物（VERAM）的可变尺寸的聚合物管类型的平坦半透膜 ）。 所述装置的利用确保通过应用热解吸附技术，随后通过气相色谱和质谱法（HS-GC-MS）注入顶部空间的技术直接测定污染物。 此外，本发明描述了将采样器吸收的量与采样期间空气中的污染物的平均浓度相关联的数学模型的发展。

    CARBON PARTICULATE MONITOR
    10.
    发明申请
    CARBON PARTICULATE MONITOR 审中-公开
    碳颗粒监测仪

    公开(公告)号：WO1993022654A1

    公开(公告)日：1993-11-11

    申请号：PCT/US1992011252

    申请日：1992-12-17

    Applicant: RUPPRECHT & PATASHNICK COMPANY, INC.

    Inventor： RUPPRECHT & PATASHNICK COMPANY, INC. ,  PATASHNICK, Harvey ,  RUPPRECHT, Georg

    IPC: G01N15/06

    CPC classification number: G01N31/12 ,  F02B3/06 ,  G01N1/2208 ,  G01N15/0618 ,  G01N31/005 ,  G01N2015/0261 ,  G01N2030/008

    Abstract: Carbon particulate concentration of diesel exhaust or other sampled gas is measured by collecting the particulate on a high efficiency filter (18) while measuring the amount of sampled gas passing through the filter (18). The filtered particulate is then heated in an oxygen rich environment (16) to oxidize carbon within the particulate to carbon dioxide. The amount of resulting carbon dioxide is measured with a closed measurement loop (30) to derive a corresponding measurement of the amount of filtered particulate. Particulate concentration is calculated by comparing the amount of carbon particulate with the measured amount of sampled gas passed through the filter. Filtered particulate can be heated incrementally to obtain a measurement of volatile carbon components within the particulate prior to the oxidation of the non-volatile carbon component. The filter (18) employed to collect the carbon particulate is of a high temperature resistant type making it reusable and can be either integral with or inserted into the oxidation chamber (16) of the instrument. Oxidation of the particulate inherently concurrently cleans the filter (18) for reuse. An upstream preseparator (15) can extend the life of the high efficiency filter (18). Particulate can also be collected for analysis by using an accelerating impaction nozzle (68) in conjunction with a heatable impaction plate (70).

    Abstract translation: 通过在测量通过过滤器（18）的取样气体的量的同时将颗粒收集在高效过滤器（18）上来测量柴油机废气或其它采样气体的碳颗粒浓度。 然后将过滤的颗粒在富氧环境（16）中加热以将颗粒内的碳氧化成二氧化碳。 用闭合的测量回路（30）测量所得二氧化碳的量，以得出过滤颗粒的量的相应测量值。 通过比较碳颗粒的量与通过过滤器的取样气体的测量量来计算颗粒浓度。 过滤的颗粒可以被递增地加热以获得在非挥发性碳组分氧化之前颗粒内的挥发性碳组分的测量。 用于收集碳颗粒的过滤器（18）具有耐高温型，使得其可重复使用，并且可以与仪器的氧化室（16）成一体或插入到该氧化室中。 颗粒的氧化固有地同时清洁过滤器（18）以便重新使用。 上游预分离器（15）可以延长高效过滤器（18）的寿命。 还可以通过使用加速冲击喷嘴（68）与可加热冲击板（70）结合来收集颗粒以用于分析。

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