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公开(公告)号：WO2007149881A3
公开(公告)日：2007-12-27
申请号：PCT/US2007/071597
申请日：2007-06-19
Applicant: CABOT CORPORATION , KODAS, Toivo, T. , OLJACA, Miodrag , HAMPDEN-SMITH, Mark, J. , FOTOU, George, P. , KORNBREKKE, Ralph, E. , SHEN, Jiang-Ping
Inventor： KODAS, Toivo, T. , OLJACA, Miodrag , HAMPDEN-SMITH, Mark, J. , FOTOU, George, P. , KORNBREKKE, Ralph, E. , SHEN, Jiang-Ping
Abstract: A powder batch is described comprising single crystal metal-containing particles having a crystal size of less than 50nm as measured by X-ray diffraction and having a weight average particle size of from about 10 nanometers to less than 100 nanometers as measured by transmission electron microscopy and including a continuous or non-continuous coating of a ceramic material. The powder batch is preferably produced by flame spraying.
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公开(公告)号：WO2006078826A3
公开(公告)日：2007-04-19
申请号：PCT/US2006001910
申请日：2006-01-20
Applicant: CABOT CORP , KODAS TOIVO T , FOTOU GEORGE P , OLJACA MIODRAG , HARDMAN NED JAY , KUMAR PRAKASH
Inventor： KODAS TOIVO T , FOTOU GEORGE P , OLJACA MIODRAG , HARDMAN NED JAY , KUMAR PRAKASH
CPC classification number: C01G1/00 , B01J23/42 , B01J23/745 , B01J35/006 , B01J37/086 , B01J37/349 , B22F1/0018 , B22F9/026 , B82Y25/00 , B82Y30/00 , C01B33/18 , C01B33/26 , C01G1/02 , C01G23/07 , C01G49/0018 , C01P2004/03 , C01P2004/04 , C01P2004/62 , C01P2004/64 , C01P2006/12 , C01P2006/13 , C23C4/123 , C23C4/129 , C23C18/02 , C23C18/1216 , C23C18/1258 , C23C18/1295 , F23D91/02 , F23D2900/21007 , H01F1/0054 , H01M4/8621 , H01M4/8652 , H01M4/8832 , H01M4/8835 , H01M4/8885 , H01M4/9016 , H01M2008/1293
Abstract: In one aspect, the process includes providing a precursor medium comprising a liquid vehicle and a precursor to a component, and flame spraying the precursor medium under conditions effective to form a population of nanoparticles, wherein the nanoparticles include the component. The population of nanoparticles, as formed, comprises less than about 5 percent by volume particles having a particle size greater than 1.0 µm. A size distribution of the population of nanoparticles may have a d50 value less than about 500 nm, and it may be unimodal. The size distribution may have a geometric standard deviation of less than about 2. The process may occur continuously for at least four hours or more. Greater than about 90 percent by weight of the precursor to the component in the precursor medium may be converted to the component in the nanoparticles. The process typically occurs in an enclosed flame spray reactor.
Abstract translation: 在一个方面，该方法包括提供包含液体载体和组分的前体的前体介质，以及在有效形成纳米颗粒群的条件下火焰喷涂前体介质，其中纳米颗粒包括该组分。 形成的纳米颗粒群包含小于约5体积％的粒径大于1.0μm的粒子。 纳米颗粒群的尺寸分布可以具有小于约500nm的d 50值，并且其可以是单峰的。 尺寸分布可以具有小于约2的几何标准偏差。该过程可以连续发生至少四个小时或更长时间。 前体介质中的组分的前体的大于约90重量％可以转化成纳米颗粒中的组分。 该方法通常发生在封闭的火焰喷雾反应器中。
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公开(公告)号：WO2007149885A3
公开(公告)日：2007-12-27
申请号：PCT/US2007/071601
申请日：2007-06-19
Applicant: CABOT CORPORATION , KODAS, Toivo, T. , OLJACA, Miodrag , HAMPDEN-SMITH, Mark, J. , FOTOU, George, P. , KORNBREKKE, Ralph, E. , SHEN, Jiang-Ping
Inventor： KODAS, Toivo, T. , OLJACA, Miodrag , HAMPDEN-SMITH, Mark, J. , FOTOU, George, P. , KORNBREKKE, Ralph, E. , SHEN, Jiang-Ping
Abstract: Security features, e.g., reflective security features, and processes for forming security features are described. The security features comprise crystalline metal-containing particles having a primary particle size of from about 10 nanometers to less than 500 nanometers and including a continuous or non-continuous coating of a ceramic material. Inks comprising such crystalline metal-containing particles are also described. The crystalline metal-containing particles are preferably produced by flame spraying.
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公开(公告)号：WO2006078827A3
公开(公告)日：2007-04-19
申请号：PCT/US2006001911
申请日：2006-01-20
Applicant: CABOT CORP , KODAS TOIVO T , FOTOU GEORGE P , OLJACA MIODRAG , HARDMAN NED JAY , KUMAR PRAKASH
Inventor： KODAS TOIVO T , FOTOU GEORGE P , OLJACA MIODRAG , HARDMAN NED JAY , KUMAR PRAKASH
CPC classification number: C01G1/00 , B01J23/42 , B01J23/745 , B01J35/006 , B01J37/086 , B01J37/349 , B22F1/0018 , B22F9/026 , B82Y25/00 , B82Y30/00 , C01B33/18 , C01B33/26 , C01G1/02 , C01G23/07 , C01G49/0018 , C01P2004/03 , C01P2004/04 , C01P2004/62 , C01P2004/64 , C01P2006/12 , C01P2006/13 , C23C4/123 , C23C4/129 , C23C18/02 , C23C18/1216 , C23C18/1258 , C23C18/1295 , F23D91/02 , F23D2900/21007 , H01F1/0054 , H01M4/8621 , H01M4/8652 , H01M4/8832 , H01M4/8835 , H01M4/8885 , H01M4/9016 , H01M2008/1293
Abstract: The invention relates to a process for decreasing flame temperature in a flame spray reaction system, the process comprising the steps of providing a precursor medium comprising a precursor to a component; flame spraying the precursor medium under conditions effective to form a population of product particles; and decreasing the flame temperature by contacting the flame with a cooling medium. The process of the present invention allows for the control of the size, composition and morphology of the nanoparticles made using the process. The invention also relates to a nozzle assembly that comprises a substantially longitudinally extending atomizing feed nozzle that comprises an atomizing medium conduit and one or more substantially longitudinally extending precursor medium feed conduits. The nozzle assembly of the present invention is used in a flame spray system to produce nanoparticles using the processes described herein.
Abstract translation: 本发明涉及一种降低火焰喷雾反应体系中火焰温度的方法，该方法包括以下步骤：提供包含组分前体的前体介质; 在有效形成产品颗粒群的条件下，火焰喷涂前体介质; 并通过使火焰与冷却介质接触来降低火焰温度。 本发明的方法允许控制使用该方法制备的纳米颗粒的尺寸，组成和形态。 本发明还涉及一种喷嘴组件，其包括基本纵向延伸的雾化进料喷嘴，其包括雾化介质导管和一个或多个基本上纵向延伸的前体介质进料导管。 本发明的喷嘴组件用于火焰喷射系统中以使用本文所述的方法制备纳米颗粒。
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公开(公告)号：WO2007149883A1
公开(公告)日：2007-12-27
申请号：PCT/US2007/071599
申请日：2007-06-19
Applicant: CABOT CORPORATION , KODAS, Toivo, T. , OLJACA, Miodrag , HAMPDEN-SMITH, Mark, J. , FOTOU, George, P. , KIM, Hyungrak , KOWALSKI, Mark, H.
Inventor： KODAS, Toivo, T. , OLJACA, Miodrag , HAMPDEN-SMITH, Mark, J. , FOTOU, George, P. , KIM, Hyungrak , KOWALSKI, Mark, H.
IPC: H01L31/0224
CPC classification number: B42D25/373 , B22F1/0018 , B22F1/02 , B22F9/28 , B22F9/30 , B42D2033/10 , B82Y30/00 , C03C12/00 , H01L31/022425 , Y02E10/50 , Y10T428/12181 , Y10T428/256 , Y10T428/2991 , Y10T428/2995 , Y10T428/2998
Abstract: Photovoltaic conductive features and processes for forming photovoltaic conductive features are described. The process comprises (a) depositing a composition onto at least a portion of a substrate, wherein the composition comprises metal-containing particles having a primary particle size of from about 10 nanometers to less than 500 nanometers and including a continuous or non-continuous coating of a ceramic material; and (b) heating the composition such that the precursor composition forms at least a portion of a photovoltaic conductive feature. The metal-containing particles are preferably produced by flame spraying.
Abstract translation: 描述了用于形成光伏导电特征的光伏导电特征和工艺。 该方法包括（a）将组合物沉积在基材的至少一部分上，其中所述组合物包含一次粒径为约10纳米至小于500纳米的含金属颗粒，并且包括连续或非连续涂层 的陶瓷材料; 和（b）加热组合物，使得前体组合物形成光伏导电特征的至少一部分。 含金属颗粒优选通过火焰喷涂制成。
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Patent Agency Ranking
公开(公告)号：WO2007149881A2
公开(公告)日：2007-12-27
申请号：PCT/US2007071597
申请日：2007-06-19
Applicant: CABOT CORP , KODAS TOIVO T , OLJACA MIODRAG , HAMPDEN-SMITH MARK J , FOTOU GEORGE P , KORNBREKKE RALPH E , SHEN JIANG-PING
Inventor： KODAS TOIVO T , OLJACA MIODRAG , HAMPDEN-SMITH MARK J , FOTOU GEORGE P , KORNBREKKE RALPH E , SHEN JIANG-PING
CPC classification number: B42D25/373 , B22F1/0018 , B22F1/02 , B22F9/28 , B22F9/30 , B42D2033/10 , B82Y30/00 , C03C12/00 , H01L31/022425 , Y02E10/50 , Y10T428/12181 , Y10T428/256 , Y10T428/2991 , Y10T428/2995 , Y10T428/2998
Abstract: A powder batch is described comprising single crystal metal-containing particles having a crystal size of less than 50nm as measured by X-ray diffraction and having a weight average particle size of from about 10 nanometers to less than 100 nanometers as measured by transmission electron microscopy and including a continuous or non-continuous coating of a ceramic material. The powder batch is preferably produced by flame spraying.
Abstract translation: 描述了一种粉末批料，其包括通过X射线衍射测量的具有小于50nm的晶体尺寸的单晶金属颗粒，并且通过透射电子显微镜测量的重均粒径为约10纳米至小于100纳米 并且包括陶瓷材料的连续或非连续涂层。 粉末批料优选通过火焰喷涂制备。
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公开(公告)号：WO2006078826A2
公开(公告)日：2006-07-27
申请号：PCT/US2006/001910
申请日：2006-01-20
Applicant: CABOT CORPORATION , KODAS, Toivo, T. , FOTOU, George, P. , OLJACA, Miodrag , HARDMAN, Ned, Jay , KUMAR, Prakash
Inventor： KODAS, Toivo, T. , FOTOU, George, P. , OLJACA, Miodrag , HARDMAN, Ned, Jay , KUMAR, Prakash
CPC classification number: C01G1/00 , B01J23/42 , B01J23/745 , B01J35/006 , B01J37/086 , B01J37/349 , B22F1/0018 , B22F9/026 , B82Y25/00 , B82Y30/00 , C01B33/18 , C01B33/26 , C01G1/02 , C01G23/07 , C01G49/0018 , C01P2004/03 , C01P2004/04 , C01P2004/62 , C01P2004/64 , C01P2006/12 , C01P2006/13 , C23C4/123 , C23C4/129 , C23C18/02 , C23C18/1216 , C23C18/1258 , C23C18/1295 , F23D91/02 , F23D2900/21007 , H01F1/0054 , H01M4/8621 , H01M4/8652 , H01M4/8832 , H01M4/8835 , H01M4/8885 , H01M4/9016 , H01M2008/1293
Abstract: In one aspect, the process includes providing a precursor medium comprising a liquid vehicle and a precursor to a component, and flame spraying the precursor medium under conditions effective to form a population of nanoparticles, wherein the nanoparticles include the component. The population of nanoparticles, as formed, comprises less than about 5 percent by volume particles having a particle size greater than 1.0 µm. A size distribution of the population of nanoparticles may have a d50 value less than about 500 nm, and it may be unimodal. The size distribution may have a geometric standard deviation of less than about 2. The process may occur continuously for at least four hours or more. Greater than about 90 percent by weight of the precursor to the component in the precursor medium may be converted to the component in the nanoparticles. The process typically occurs in an enclosed flame spray reactor.
Abstract translation: 在一个方面，该方法包括提供包含液体载体和组分的前体的前体介质，以及在有效形成纳米颗粒群的条件下火焰喷涂前体介质，其中纳米颗粒包括该组分。 形成的纳米颗粒群包含小于约5体积％的粒径大于1.0μm的粒子。 纳米颗粒群的尺寸分布可以具有小于约500nm的d 50值，并且其可以是单峰的。 尺寸分布可以具有小于约2的几何标准偏差。该过程可以连续发生至少四个小时或更长时间。 前体介质中的组分的前体的大于约90重量％可以转化成纳米颗粒中的组分。 该方法通常发生在封闭的火焰喷雾反应器中。
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公开(公告)号：WO2007127232A3
公开(公告)日：2009-10-01
申请号：PCT/US2007009993
申请日：2007-04-25
Applicant: CABOT CORP , LIU JOANNE , FOTOU GEORGE P , KUTSOVSKY YAKOV E
Inventor： LIU JOANNE , FOTOU GEORGE P , KUTSOVSKY YAKOV E
IPC: C01B33/18
CPC classification number: C01B33/183
Abstract: The invention provides a process for the production of fumed silica. The process comprises providing a silicon halide feedstock comprising about 80% to 100% methyltrichlorosilane, combining the silicon halide feedstock with hydrogen gas and oxygen gas to form a reactant mixture, discharging the reactant mixture out of a burner, and combusting the hydrogen gas and the oxygen gas of the reactant mixture so as to hydrolyze the silicon halide feedstock to produce fumed silica. Hydrogen (H2) is present in a mole fraction of about 0.11 or less based on the reactant mixture, and/or the velocity of the reactant mixture upon exiting the burner is about 25 m/s or more.
Abstract translation: 本发明提供一种生产热解二氧化硅的方法。 该方法包括提供包含约80％至100％甲基三氯硅烷的卤化硅原料，将卤化硅原料与氢气和氧气组合以形成反应物混合物，将反应物混合物排出燃烧器，并将氢气和 氧化反应混合物的氧气，以便将卤化硅原料水解以产生热解二氧化硅。 氢（H 2）以基于反应物混合物的约0.11或更小的摩尔分数存在，和/或离开燃烧器时的反应物混合物的速度为约25m / s或更高。
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公开(公告)号：WO2007127232A2
公开(公告)日：2007-11-08
申请号：PCT/US2007/009993
申请日：2007-04-25
Applicant: CABOT CORPORATION , LIU, Joanne , FOTOU, George, P. , KUTSOVSKY, Yakov, E.
Inventor： LIU, Joanne , FOTOU, George, P. , KUTSOVSKY, Yakov, E.
CPC classification number: C01B33/183
Abstract: The invention provides a process for the production of fumed silica. The process comprises providing a silicon halide feedstock comprising about 80% to 100% methyltrichlorosilane, combining the silicon halide feedstock with hydrogen gas and oxygen gas to form a reactant mixture, discharging the reactant mixture out of a burner, and combusting the hydrogen gas and the oxygen gas of the reactant mixture so as to hydrolyze the silicon halide feedstock to produce fumed silica. Hydrogen (H 2 ) is present in a mole fraction of about 0.11 or less based on the reactant mixture, and/or the velocity of the reactant mixture upon exiting the burner is about 25 m/s or more.
Abstract translation: 本发明提供一种生产热解二氧化硅的方法。 该方法包括提供包含约80％至100％甲基三氯硅烷的卤化硅原料，将卤化硅原料与氢气和氧气组合以形成反应物混合物，将反应物混合物排出燃烧器，并将氢气和 氧化反应混合物的氧气，以便将卤化硅原料水解以产生热解二氧化硅。 氢（H 2 H 2）以基于反应物混合物的约0.11或更低的摩尔分数存在，和/或离开燃烧器时反应物混合物的速度为约25m / s或更高 。
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公开(公告)号：WO2007149885A2
公开(公告)日：2007-12-27
申请号：PCT/US2007071601
申请日：2007-06-19
Applicant: CABOT CORP , KODAS TOIVO T , OLJACA MIODRAG , HAMPDEN-SMITH MARK J , FOTOU GEORGE P , KORNBREKKE RALPH E , SHEN JIANG-PING
Inventor： KODAS TOIVO T , OLJACA MIODRAG , HAMPDEN-SMITH MARK J , FOTOU GEORGE P , KORNBREKKE RALPH E , SHEN JIANG-PING
CPC classification number: B42D25/373 , B22F1/0018 , B22F1/02 , B22F9/28 , B22F9/30 , B42D2033/10 , B82Y30/00 , C03C12/00 , H01L31/022425 , Y02E10/50 , Y10T428/12181 , Y10T428/256 , Y10T428/2991 , Y10T428/2995 , Y10T428/2998
Abstract: Security features, e.g., reflective security features, and processes for forming security features are described. The security features comprise crystalline metal-containing particles having a primary particle size of from about 10 nanometers to less than 500 nanometers and including a continuous or non-continuous coating of a ceramic material. Inks comprising such crystalline metal-containing particles are also described. The crystalline metal-containing particles are preferably produced by flame spraying.
Abstract translation: 描述了安全特征，例如反射安全特征以及用于形成安全特征的过程。 安全特征包括具有约10纳米至小于500纳米的初级粒度的含结晶金属的颗粒，并且包括陶瓷材料的连续或非连续涂层。 还描述了包含这种含结晶金属的颗粒的油墨。 含结晶金属的颗粒优选通过火焰喷涂制成。
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